CN104909551B - Preparation technology for the safety glass of electric four-wheel vehicle - Google Patents
Preparation technology for the safety glass of electric four-wheel vehicle Download PDFInfo
- Publication number
- CN104909551B CN104909551B CN201510291613.XA CN201510291613A CN104909551B CN 104909551 B CN104909551 B CN 104909551B CN 201510291613 A CN201510291613 A CN 201510291613A CN 104909551 B CN104909551 B CN 104909551B
- Authority
- CN
- China
- Prior art keywords
- parts
- glass plate
- glass
- prepare
- safety glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Glass Compositions (AREA)
Abstract
The invention belongs to vehicle glass technical field, disclose in the preparation technology of the safety glass of electric four-wheel vehicle, it comprises the following steps：Step 1）Weigh raw material, step 2）Prepare material A, step 3）Prepare material B, step 4）Prepare glass plate, and step 5）Prepare safety glass.Safety glass preparation technology simple possible of the present invention, the product various aspects of performance of preparation preferably, can be applied to electric four-wheel vehicle.
Description
Technical field
The invention belongs to vehicle glass manufacture field, and in particular to the preparation work for the safety glass of electric four-wheel vehicle
Skill.
Background technology
Electric four-wheel vehicle is lightly convenient, and uses electric energy, with low cost, environment friendly and pollution-free, firmly gets liking for people, closely
Develop over year swift and violent.At present, not only there is mechanical performance and preventing ultraviolet effect in the electric automobile vehicle glass occurred on the market
, also there is fracture phenomena under cold and hot extreme temperature in difference, the traffic safety to people brings larger hidden danger.
The content of the invention
Present invention aim to address many defects of electric four-wheel vehicle in the prior art, by lot of experiments and exploration,
Changing existing raw material composition and preparation technology, there is provided a kind of preparation technology of the safety glass for electric four-wheel vehicle, the work
Safety glass prepared by skill possesses preferable mechanical performance, cold and hot stability and corrosion resistance.
To achieve these goals, technical scheme is realized in the following way：
For the preparation technology of the safety glass of electric four-wheel vehicle, it comprises the following steps：
Step 1）Weigh raw material：The raw material for standby of following parts by weight is weighed, wherein,
1-2 parts of aluminium nitride, 1-2 parts of silica white, 1-2 parts of antimony oxide, 2-3 parts of titanium dioxide, zirconium dioxide 3-
4 parts, 3-4 parts of potassium chloride, 5-6 parts of montmorillonite, 5-6 parts of diatomite, 7-8 parts of lithia, 7-8 parts of palygorskite, boron oxide
10-15 parts, 40-50 parts of aluminum oxide, 180-200 parts of quartz sand；
Step 2）Prepare material A：Diatomite is added in stirred reactor, the 1M hydrochloric acid of phase homogenous quantities is then added,
500 turns/min stirs 3min, and 80 DEG C of drying are ground to particle diameter for 100 mesh, produce material A；
Step 3）Prepare material B：Montmorillonite and palygorskite are added in disintegrating machine successively and crushed, is then ground
Mill, acquisition particle diameter is 100 mesh powders, as material B；
Step 4）Prepare glass plate：Corundum crucible is placed in Si-Mo rod stove, 1300 DEG C are warming up to, then by aluminium nitride,
Silica white, antimony oxide, titanium dioxide, zirconium dioxide, potassium chloride, lithia, boron oxide, aluminum oxide, quartz sand, material A
And material B is added in corundum crucible successively, then insulation reaction 30min is warming up to 1650 DEG C with 20 DEG C/min speed,
20min is incubated, the glass metal melted is cast in graphite jig, is transferred in chamber type electric resistance furnace and anneals immediately after shaping, move back
Fiery temperature is 600 DEG C, and then cool natural cooling, produces glass plate；
Step 5）Prepare safety glass：Glass plate is put into 10%（Mass fraction）Soaked in sodium-chloride water solution
30min, is then boiled, and glass plate is taken out after 30min, naturally cools to room temperature；Glass plate is then preheated into 1- at 300-350 DEG C
2 hours, it is heat-treated into annealing furnace, processing time is 60min, treatment temperature is 600 DEG C；Then glass plate is put into
Temperature in 300-350 DEG C of radiating stove, temperature takes out glass plate when being down to 50 DEG C, be put into 80 DEG C 5%（Mass fraction）'s
2-3 hours are stood in sodium-chloride water solution, taking-up produces safety glass.
Preferably, the thickness of safety glass of the present invention is 3-5mm.
The present invention, which obtains beneficial effect, mainly to be included：
Rationally, the safety glass prepared is in anti-impact force, flexibility, degree of the temper and self-destruction for material combination of the present invention
The indexs such as rate are greatly improved；Safety glass of the present invention can obstruct most of infrared ray and ultraviolet, with it is excellent every
Hot heat-insulating property；Safety glass preparation method of the present invention is simple, is adapted to large-scale industrial production.
Embodiment
In order that those skilled in the art more fully understand the technical scheme in the application, have below in conjunction with the application
Body embodiment, is more clearly and completely described, it is clear that described embodiment is only the application one to the present invention
Divide embodiment, rather than whole embodiments.Based on the embodiment in the application, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, should all belong to the scope of protection of the invention.
Embodiment 1
For the preparation technology of the safety glass of electric four-wheel vehicle, it comprises the following steps：
Step 1）Weigh raw material：The raw material for standby of following parts by weight is weighed, wherein,
1 part of aluminium nitride, 1 part of silica white, 1 part of antimony oxide, 2 parts of titanium dioxide, 3 parts of zirconium dioxide, 3 parts of potassium chloride,
5 parts of montmorillonite, 5 parts of diatomite, 7 parts of lithia, 7 parts of palygorskite, 10 parts of boron oxide, 40 parts of aluminum oxide, 180 parts of quartz sand；
Step 2）Prepare material A：Diatomite is added in stirred reactor, the 1M hydrochloric acid of phase homogenous quantities is then added,
500 turns/min stirs 3min, and 80 DEG C of drying are ground to particle diameter for 100 mesh, produce material A；
Step 3）Prepare material B：Montmorillonite and palygorskite are added in disintegrating machine successively and crushed, is then ground
Mill, acquisition particle diameter is 100 mesh powders, as material B；
Step 4）Prepare glass plate：Corundum crucible is placed in Si-Mo rod stove, 1300 DEG C are warming up to, then by aluminium nitride,
Silica white, antimony oxide, titanium dioxide, zirconium dioxide, potassium chloride, lithia, boron oxide, aluminum oxide, quartz sand, material A
And material B is added in corundum crucible successively, then insulation reaction 30min is warming up to 1650 DEG C with 20 DEG C/min speed,
20min is incubated, the glass metal melted is cast in graphite jig, is transferred in chamber type electric resistance furnace and anneals immediately after shaping, move back
Fiery temperature is 600 DEG C, and then cool natural cooling, produces glass plate；
Step 5）Prepare safety glass：Glass plate is put into 10%（Mass fraction）30min is soaked in sodium-chloride water solution,
Then boil, glass plate is taken out after 30min, naturally cool to room temperature；Then glass plate is preheated 2 hours at 350 DEG C, into steel
Change and be heat-treated in stove, processing time is 60min, treatment temperature is 600 DEG C；Then glass plate is put into temperature for 350 DEG C
Radiating stove in, temperature takes out glass plate when being down to 50 DEG C, be put into 80 DEG C 5%（Mass fraction）Sodium-chloride water solution in it is quiet
Put 2 hours, taking-up produces safety glass.
Embodiment 2
For the preparation technology of the safety glass of electric four-wheel vehicle, it comprises the following steps：
Step 1）Weigh raw material：The raw material for standby of following parts by weight is weighed, wherein,
2 parts of aluminium nitride, 2 parts of silica white, 2 parts of antimony oxide, 3 parts of titanium dioxide, 4 parts of zirconium dioxide, 4 parts of potassium chloride,
6 parts of montmorillonite, 6 parts of diatomite, 8 parts of lithia, 8 parts of palygorskite, 15 parts of boron oxide, 50 parts of aluminum oxide, 200 parts of quartz sand；
Step 2）Prepare material A：Diatomite is added in stirred reactor, the 1M hydrochloric acid of phase homogenous quantities is then added,
500 turns/min stirs 3min, and 80 DEG C of drying are ground to particle diameter for 100 mesh, produce material A；
Step 3）Prepare material B：Montmorillonite and palygorskite are added in disintegrating machine successively and crushed, is then ground
Mill, acquisition particle diameter is 100 mesh powders, as material B；
Step 4）Prepare glass plate：Corundum crucible is placed in Si-Mo rod stove, 1300 DEG C are warming up to, then by aluminium nitride,
Silica white, antimony oxide, titanium dioxide, zirconium dioxide, potassium chloride, lithia, boron oxide, aluminum oxide, quartz sand, material A
And material B is added in corundum crucible successively, then insulation reaction 30min is warming up to 1650 DEG C with 20 DEG C/min speed,
20min is incubated, the glass metal melted is cast in graphite jig, is transferred in chamber type electric resistance furnace and anneals immediately after shaping, move back
Fiery temperature is 600 DEG C, and then cool natural cooling, produces glass plate；
Step 5）Prepare safety glass：Glass plate is put into 10%（Mass fraction）Soaked in sodium-chloride water solution
30min, is then boiled, and glass plate is taken out after 30min, naturally cools to room temperature；Then glass plate is preheated 1 hour at 300 DEG C,
It is heat-treated into annealing furnace, processing time is 60min, treatment temperature is 600 DEG C；Then glass plate is put into temperature is
In 350 DEG C of radiating stove, temperature takes out glass plate when being down to 50 DEG C, be put into 80 DEG C 5%（Mass fraction）Aqueous sodium chloride
2 hours are stood in liquid, taking-up produces safety glass.
Embodiment 3
The performance test of safety glass of the present invention, by taking 3mm thickness safety glass prepared by embodiment 1 as an example：
Anti-high and low-temp impact is tested：
Safety glass is placed in high/low temperature circulating box, -20 DEG C of placement 15h of low temperature are maintained at normal temperature 2h in case, then turn high
55 DEG C of experiment 15h of temperature, during by above-mentioned conversion order alternating test to 96h, without any spalling, Fragmentation Phenomena.
Impact resistance test：
Safety glass from glass surface geometric center 2.5m height at free-falling, crack-free.
Fragmentation test：
Fragment 59 in broken rear 50 × 50mm of safety glass thick 3mm, meets national standard；
Light transmission performance test：
Visible light transmissivity is more than 73%
Infrared ray rejection rate is more than 80%
Ultraviolet isolating rate is more than 95%.
The present invention also have detected other indexs：Wherein, flexibility reaches 0.5 ‰, and self-destruction rate is 1.6 ‰.
Although above having made detailed explanation to this case with generality explanation and embodiment, at this
On the basis of invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Therefore,
The modification or improvement made without departing from theon the basis of the spirit of the present invention, belong to the scope of protection of present invention.
Claims (1)
1. the preparation technology of the safety glass for electric four-wheel vehicle, it is characterised in that the technique comprises the following steps：
Step 1）Weigh raw material：The raw material for standby of following parts by weight is weighed, wherein,
1-2 parts of aluminium nitride, 1-2 parts of silica white, 1-2 parts of antimony oxide, 2-3 parts of titanium dioxide, 3-4 parts of zirconium dioxide,
3-4 parts of potassium chloride, 5-6 parts of montmorillonite, 5-6 parts of diatomite, 7-8 parts of lithia, 7-8 parts of palygorskite, boron oxide 10-15
Part, 40-50 parts of aluminum oxide, 180-200 parts of quartz sand；
Step 2）Prepare material A：Diatomite is added in stirred reactor, the 1M hydrochloric acid of phase homogenous quantities, 500 is then added
Turn/min stirrings 3min, 80 DEG C of drying are ground to particle diameter for 100 mesh, produce material A；
Step 3）Prepare material B：Montmorillonite and palygorskite are added in disintegrating machine successively and crushed, is then ground,
Acquisition particle diameter is 100 mesh powders, as material B；
Step 4）Prepare glass plate：Corundum crucible is placed in Si-Mo rod stove, 1300 DEG C are warming up to, then by aluminium nitride, silica gel
Powder, antimony oxide, titanium dioxide, zirconium dioxide, potassium chloride, lithia, boron oxide, aluminum oxide, quartz sand, material A and
Material B is added in corundum crucible successively, insulation reaction 30min, is then warming up to 1650 DEG C, insulation with 20 DEG C/min speed
20min, the glass metal melted is cast in graphite jig, is transferred in chamber type electric resistance furnace and is annealed immediately after shaping, annealing temperature
Spend for 600 DEG C, then cool natural cooling, produces glass plate；
Step 5）Prepare safety glass：30min is soaked in the sodium-chloride water solution that glass plate is put into 10%, is then boiled,
Glass plate is taken out after 30min, room temperature is naturally cooled to；Then glass plate is preheated 1-2 hours at 300-350 DEG C, into tempering
It is heat-treated in stove, processing time is 60min, treatment temperature is 600 DEG C；Then glass plate is put into temperature for 300-350
DEG C radiating stove in, temperature takes out glass plate when being down to 50 DEG C, be put into 80 DEG C of 5% sodium-chloride water solution stand 2-3 it is small
When, taking-up produces safety glass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510291613.XA CN104909551B (en) | 2015-06-01 | 2015-06-01 | Preparation technology for the safety glass of electric four-wheel vehicle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510291613.XA CN104909551B (en) | 2015-06-01 | 2015-06-01 | Preparation technology for the safety glass of electric four-wheel vehicle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104909551A CN104909551A (en) | 2015-09-16 |
| CN104909551B true CN104909551B (en) | 2017-11-07 |
Family
ID=54079063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510291613.XA Active CN104909551B (en) | 2015-06-01 | 2015-06-01 | Preparation technology for the safety glass of electric four-wheel vehicle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104909551B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113415983A (en) * | 2021-07-06 | 2021-09-21 | 苏州市金泰玻璃有限公司 | Toughened glass processing method |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CZ2002738A3 (en) * | 1999-09-01 | 2003-12-17 | Pilkington Plc | Thermally tempered glass part, laminated glass part, thermal tempering process and soda-lime glass |
| FR2867774B1 (en) * | 2004-03-19 | 2007-08-10 | Saint Gobain | DARK GRAY SILICO-SODO-CALCIUM GLASS COMPOSITION FOR THE MANUFACTURE OF GLAZINGS |
| CN102070297A (en) * | 2009-11-19 | 2011-05-25 | 杨德宁 | Extra-high aluminosilicate plate with high impact resistance and high bending resistance and process thereof |
| CN104211302B (en) * | 2014-09-02 | 2016-04-06 | 国家电网公司 | A kind of PV glass panel and preparation method thereof |
-
2015
- 2015-06-01 CN CN201510291613.XA patent/CN104909551B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104909551A (en) | 2015-09-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108423997B (en) | Method for preparing microcrystalline foam glass by using solid waste | |
| CN104745867A (en) | High-temperature-resistant titanium alloy plate | |
| CN101244889A (en) | Non-fluorin environment protection opacifiedglass material and method for manufacturing same | |
| CN101982444A (en) | Technology for preparing nano microcrystalline enamels | |
| CN104370464A (en) | Tempered glass | |
| CN104843997B (en) | Tempered glass for electro-tricycle | |
| CN104909551B (en) | Preparation technology for the safety glass of electric four-wheel vehicle | |
| CN106938889A (en) | A kind of preparation method of safety glass | |
| CN105693088A (en) | Explosion-proof glass material and preparation method thereof | |
| CN102603185B (en) | Glass used for absorbing optical spectrum with wavelength being 430-900nm for optical fiber panel and preparation process thereof | |
| CN103614647A (en) | Rare earth alloy steel material used for valves and preparation method of the material | |
| CN107902896A (en) | The preparation process of new tempered glass | |
| CN105669010A (en) | High-heat-exchange-rate corrosion-resistant tempered glass for air conditioners and preparation method thereof | |
| CN103498026B (en) | A kind of quenching method of 45# steel workpiece | |
| CN103484609B (en) | A kind of 45# steel quenching method | |
| CN105236737B (en) | A kind of high-performance superelevation aluminium float glass component | |
| CN107892483A (en) | A kind of insulating foam method for glass preparation | |
| CN105819686A (en) | Cold-resistant glass material and preparation method thereof | |
| CN104213042A (en) | Alloy steel material for pump shell and manufacturing method thereof | |
| CN101007704A (en) | Process for preparing coloured quartz glass tube | |
| CN105776856A (en) | Nanometer transparent scratch-resistant glass and preparation method thereof | |
| CN106086667A (en) | A kind of corrosion-resistant stamping resistance bearing and preparation method thereof | |
| CN105695807A (en) | Preparation method of corrosion-resistant and oxidation-resistant aluminium alloy material | |
| CN105481255A (en) | Method for manufacturing low-expansion glass-ceramics by high silicon-iron tailings | |
| CN104193150B (en) | A kind of preparation technology of solar battery glass |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation process of tempered glass for electric four-wheel vehicle Effective date of registration: 20211014 Granted publication date: 20171107 Pledgee: Linshang Bank Co.,Ltd. Kaiyuan sub branch Pledgor: LINYI JINLI MACHINERY Co.,Ltd. Registration number: Y2021980010714 |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220117 Address after: 276002 101, building 10, No. 0001, Gongye Third Road, industrial park, Lanshan District, Linyi City, Shandong Province Patentee after: SHANDONG JINLI CAR INDUSTRY CO.,LTD. Address before: 276015 Linyi Industrial Park, east of machanghu, Lanshan District, Linyi City, Shandong Province Patentee before: LINYI JINLI MACHINERY CO.,LTD. |