CN104878472A - Waterproof and breathable textile material and preparation method thereof - Google Patents
Waterproof and breathable textile material and preparation method thereof Download PDFInfo
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- CN104878472A CN104878472A CN201510313254.3A CN201510313254A CN104878472A CN 104878472 A CN104878472 A CN 104878472A CN 201510313254 A CN201510313254 A CN 201510313254A CN 104878472 A CN104878472 A CN 104878472A
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Abstract
The invention discloses a waterproof and breathable textile material and a preparation method thereof. The waterproof and breathable textile material is prepared by the following ingredients in parts by weight: 45-60 parts of polyethylene terephthalate, 20-35 parts of synthetic fabric, 20-30 parts of diglycidyl ether, 3-6 parts of condensation polymer of epoxy resin and furaldehyde cyclohexanone, 3-5 parts of glass beads, 2-5 parts of dimethylacrylicacid tri ethyleneglycol ester, 1-2 parts of metasilicic acid trimethy phosphate, 1-2 parts of barium metaborate and 0.05-1.8 parts of methyltriacetoxysilane. The invention also provides the preparation method of the waterproof and breathable textile material.
Description
Technical field
The invention belongs to textile material field, particularly a kind of waterproof, ventilative textile material and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, the requirement for weaving face fabric is also more and more higher, and various functional fabric also emerges in an endless stream thereupon.
Some outdoor clothes existing use under meeting open-air conditions because needs possess waterproof effect, and this kind of clothes not only need waterproof, more and more extra requirement is proposed to its comfortableness, existing outdoor water-proof clothes, although there is good waterproof effect, sometimes in order to reach good water proofing property, but good gas permeability can not be had, cause dress uncomfortable, and there is short problem in service life simultaneously.
Obtain one side by double-layered structure's design in China Patent Publication No. CN102031622 and refuse the hydrophilic fabric of water decontamination, one side, the solid shape oily dirt such as neck dirt, grease soils is extruded to and refuses between water and hydrophilic layer equally under external force, fluoroplast layer near dirt can hinder cleaning solution to arrive greasy dirt their location, and this type of face weave cost is also higher simultaneously.
Summary of the invention
For above-mentioned demand, invention especially provides a kind of waterproof, ventilative textile material and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
Waterproof, a ventilative textile material, be made up of the component comprising following weight portion:
Polyethylene terephthalate 45-60 part,
Blended fiber 20-35 part,
Diglycidyl ether 20-30 part,
Epoxy resin and furfural cyclohexanone condensation product 3-6 part,
Glass microballoon 3-5 part,
Dimethacrylate Triethylene Glycol 2-5 part,
Metasilicic acid trimethyl 1-2 part,
Barium metaborate 1-2 part,
Methyl triacetoxysilane 0.05-1.8 part.
Described blended fiber is the mixture of polyamide fiber and acetate fibre.
In described blended fiber, the mass ratio of polyamide fiber and acetate fibre is 2:1.
Described component also comprises pentaerythritol stearate 0-0.02 weight portion.
A preparation method for waterproof, ventilative textile material, the method comprises the following steps:
(1) take diglycidyl ether 20-30 weight portion, barium metaborate 1-2 weight portion, methyl triacetoxysilane 0.05-1.8 weight portion and pentaerythritol stearate 0-0.02 weight portion, at 85-110 DEG C, stir 5-10 minute;
(2) polyethylene terephthalate 45-60 weight portion, blended fiber 20-35 weight portion, epoxy resin and furfural cyclohexanone condensation product 3-6 weight portion, glass microballoon 3-5 weight portion, dimethacrylate Triethylene Glycol 2-5 weight portion, metasilicic acid trimethyl 1-2 weight portion is added, mixing, material after mixing is heated to 170-190 DEG C under inert atmosphere 21-25Mpa, mix, by tractive process, obtained waterproof, ventilative textile material.
Described spinning speed is 1300-1500m/min.
Compared with prior art, its beneficial effect is in the present invention:
(1) waterproof, the ventilative textile material that obtain of the present invention, using a certain proportion of polyamide fiber and acetate fibre as blended fiber, and add epoxy resin and furfural cyclohexanone condensation product, barium metaborate and methyl triacetoxysilane, make the textile material obtained have good water proofing property, and there is good gas permeability.
(2) waterproof, the ventilative textile material that obtain of the present invention, overcomes the performance of the surface not scratch resistance of existing waterproof woven material, makes material while having good mechanical strength, have good surface property.
(3) waterproof of the present invention, ventilative textile material, its preparation method is simple, is easy to suitability for industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) take diglycidyl ether 20kg, barium metaborate 1kg, methyl triacetoxysilane 0.05kg, stir 5 minutes at 85 DEG C;
(2) polyethylene terephthalate 45kg, polyamide fiber 14kg, acetate fibre 7kg, epoxy resin and furfural cyclohexanone condensation product 3kg, glass microballoon 3kg, dimethacrylate Triethylene Glycol 2kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 170 DEG C under inert atmosphere 21Mpa, mix, with 1300m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Embodiment 2
(1) take diglycidyl ether 20kg, barium metaborate 2kg, methyl triacetoxysilane 0.05kg, stir 5 minutes at 85 DEG C;
(2) polyethylene terephthalate 45kg, polyamide fiber 14kg, acetate fibre 7kg, epoxy resin and furfural cyclohexanone condensation product 3kg, glass microballoon 3kg, dimethacrylate Triethylene Glycol 2kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 170 DEG C under inert atmosphere 21Mpa, mix, with 1300m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Embodiment 3
(1) take diglycidyl ether 30kg, barium metaborate 2kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 22kg, acetate fibre 11kg, epoxy resin and furfural cyclohexanone condensation product 3kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 2kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Embodiment 4
(1) take diglycidyl ether 30kg, barium metaborate 2kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 22kg, acetate fibre 11kg, epoxy resin and furfural cyclohexanone condensation product 6kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 2kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Embodiment 5
(1) take diglycidyl ether 30kg, barium metaborate 2kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 22kg, acetate fibre 11kg, epoxy resin and furfural cyclohexanone condensation product 6kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Comparative example 1
(1) take diglycidyl ether 30kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 22kg, acetate fibre 11kg, epoxy resin and furfural cyclohexanone condensation product 6kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Comparative example 2
(1) take diglycidyl ether 30kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 22kg, acetate fibre 11kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
Comparative example 3
(1) take diglycidyl ether 30kg, barium metaborate 2kg, methyl triacetoxysilane 1.8kg and pentaerythritol stearate 0.02kg, stir 10 minutes at 110 DEG C;
(2) polyethylene terephthalate 60kg, polyamide fiber 33kg, epoxy resin and furfural cyclohexanone condensation product 6kg, glass microballoon 5kg, dimethacrylate Triethylene Glycol 5kg, metasilicic acid trimethyl 1kg is added, mixing, material after mixing is heated to 190 DEG C under inert atmosphere 25Mpa, mix, with 1500m/min by tractive process, obtained waterproof, ventilative textile material.
The performance test results of obtained waterproof, ventilative textile material is as shown in table 1.
After the textile material of embodiment 1-5 and comparative example 1-3 is made cloth, carry out 1000 friction on the surface of cloth to draw round mode with sand paper, the breakage rate of its cloth is specifically shown in Table 1.
By the material of embodiment 1-5, its good air permeability.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (6)
1. waterproof, a ventilative textile material, is characterized in that, is made up of the component comprising following weight portion:
Polyethylene terephthalate 45-60 part,
Blended fiber 20-35 part,
Diglycidyl ether 20-30 part,
Epoxy resin and furfural cyclohexanone condensation product 3-6 part,
Glass microballoon 3-5 part,
Dimethacrylate Triethylene Glycol 2-5 part,
Metasilicic acid trimethyl 1-2 part,
Barium metaborate 1-2 part,
Methyl triacetoxysilane 0.05-1.8 part.
2. waterproof, ventilative textile material according to claim 1, it is characterized in that, described blended fiber is the mixture of polyamide fiber and acetate fibre.
3. waterproof, ventilative textile material according to claim 2, it is characterized in that, in described blended fiber, the mass ratio of polyamide fiber and acetate fibre is 2:1.
4. waterproof, ventilative textile material according to claim 1, it is characterized in that, described component also comprises pentaerythritol stearate 0-0.02 weight portion.
5. a preparation method for waterproof, ventilative textile material, it is characterized in that, the method comprises the following steps:
(1) take diglycidyl ether 20-30 weight portion, barium metaborate 1-2 weight portion, methyl triacetoxysilane 0.05-1.8 weight portion and pentaerythritol stearate 0-0.02 weight portion, at 85-110 DEG C, stir 5-10 minute;
(2) polyethylene terephthalate 45-60 weight portion, blended fiber 20-35 weight portion, epoxy resin and furfural cyclohexanone condensation product 3-6 weight portion, glass microballoon 3-5 weight portion, dimethacrylate Triethylene Glycol 2-5 weight portion, metasilicic acid trimethyl 1-2 weight portion is added, mixing, material after mixing is heated to 170-190 DEG C under inert atmosphere 21-25Mpa, mix, by tractive process, obtained waterproof, ventilative textile material.
6. the preparation method of waterproof according to claim 5, ventilative textile material, is characterized in that, described spinning speed is 1300-1500m/min.
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| CN201510313254.3A CN104878472A (en) | 2015-06-09 | 2015-06-09 | Waterproof and breathable textile material and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105220467A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of novel textile material waterproofing agent and preparation method thereof |
| CN105220265A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of new type natural fiber textile material and preparation method thereof |
| CN105220497A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of new type natural fiber softener and preparation method thereof |
| CN106883459A (en) * | 2017-04-19 | 2017-06-23 | 马志明 | A kind of textile material of ventilation wear-resistance and preparation method thereof |
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| CN1699684A (en) * | 2004-02-26 | 2005-11-23 | 日本戈尔-得克斯股份有限公司 | Waterproof and breathable composite film, and waterproof and breathable composite fabric |
| US20060019563A1 (en) * | 2004-07-23 | 2006-01-26 | Larry Rising | "Barrier" substrate |
| CN101041277A (en) * | 2006-07-27 | 2007-09-26 | 宁波山泉建材有限公司 | Three layered composite film for purifying and preventing the air and the preparing method and the application |
| CN101534666A (en) * | 2006-11-03 | 2009-09-16 | 纳幕尔杜邦公司 | Breathable waterproof fabrics with a dyed and welded microporous layer |
| CN101534667A (en) * | 2006-11-03 | 2009-09-16 | 纳幕尔杜邦公司 | Liquid water resistant and water vapor permeable garments |
| CN102031622A (en) * | 2011-01-25 | 2011-04-27 | 安徽好波国际内衣有限公司 | Water-repellent anti-contamination hygroscopic perspiratory composite tissue knitted fabric and production method thereof |
| CN104674379A (en) * | 2015-03-06 | 2015-06-03 | 苏州爱立方服饰有限公司 | Waterproof fabric material and preparation method thereof |
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Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1699684A (en) * | 2004-02-26 | 2005-11-23 | 日本戈尔-得克斯股份有限公司 | Waterproof and breathable composite film, and waterproof and breathable composite fabric |
| US20060019563A1 (en) * | 2004-07-23 | 2006-01-26 | Larry Rising | "Barrier" substrate |
| CN101041277A (en) * | 2006-07-27 | 2007-09-26 | 宁波山泉建材有限公司 | Three layered composite film for purifying and preventing the air and the preparing method and the application |
| CN101534666A (en) * | 2006-11-03 | 2009-09-16 | 纳幕尔杜邦公司 | Breathable waterproof fabrics with a dyed and welded microporous layer |
| CN101534667A (en) * | 2006-11-03 | 2009-09-16 | 纳幕尔杜邦公司 | Liquid water resistant and water vapor permeable garments |
| CN102031622A (en) * | 2011-01-25 | 2011-04-27 | 安徽好波国际内衣有限公司 | Water-repellent anti-contamination hygroscopic perspiratory composite tissue knitted fabric and production method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105220467A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of novel textile material waterproofing agent and preparation method thereof |
| CN105220265A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of new type natural fiber textile material and preparation method thereof |
| CN105220497A (en) * | 2015-10-20 | 2016-01-06 | 湖州博润实业有限公司 | A kind of new type natural fiber softener and preparation method thereof |
| CN106883459A (en) * | 2017-04-19 | 2017-06-23 | 马志明 | A kind of textile material of ventilation wear-resistance and preparation method thereof |
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Application publication date: 20150902 |