Summary of the invention
For above-mentioned demand, invention especially provides a kind of anti-stain textile material and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of anti-stain textile material, be made up of the component comprising following weight portion:
Described fiber is selected from one or more in cotton fiber, flax fibre, wool fibre and silk fiber.
Described fiber is through methyl triacetoxysilane process.
Described component also comprises polyacrylonitrile fibre 10-15 weight portion.
A preparation method for anti-stain textile material, the method comprises the following steps:
(1) take fiber 68-81 weight portion, epoxy propane butyl ether 15-20 weight portion, ethyl cellulose 4-7 weight portion, brown coal cerinic acid second diester 1-3 weight portion, silk-fibroin 1.5-2 weight portion, Dawsonite Kompensan 0.2-0.8 weight portion and polyacrylonitrile fibre 10-15 weight portion, add in cutter and mix;
(2) add polyethylene glycol 8-10 weight portion, laruyl alcohol 3-5 weight portion, at 80-100 DEG C, stir 20-40 minute, add tung oil acid anhydride 0.2-1.8 weight portion, mix, melting at airtight condition, 205-215 DEG C, spinning, by tractive process, obtained anti-stain textile material.
Described spinning speed is 1600-1800m/min.
Compared with prior art, its beneficial effect is in the present invention:
(1) the anti-stain textile material that obtains of the present invention is by adding brown coal cerinic acid second diester, silk-fibroin, tung oil acid anhydride and Dawsonite Kompensan, the textile material obtained is made to have good mechanical strength and pliability, textile material of the present invention has good antifouling effect simultaneously, can effectively prevent spot from adhering to.
(2) the anti-stain textile material long service life that obtains of the present invention, has good gas permeability.
(3) anti-stain textile material of the present invention, its preparation method is simple, and raw material environmental protection in process of production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) take cotton fiber 68kg, epoxy propane butyl ether 15kg, ethyl cellulose 4kg, brown coal cerinic acid second diester 1kg, silk-fibroin 1.5kg, Dawsonite Kompensan 0.2kg and polyacrylonitrile fibre 30kg, add in cutter and mix;
(2) add polyethylene glycol 8kg, laruyl alcohol 3kg, stir 20 minutes at 80 DEG C, add tung oil acid anhydride 0.2kg, mix, in airtight condition, melting at 205 DEG C, with the speed spinning of 1600m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Embodiment 2
(1) take the cotton fiber 68kg of methyl triacetoxysilane process, epoxy propane butyl ether 15kg, ethyl cellulose 4kg, brown coal cerinic acid second diester 1kg, silk-fibroin 1.5kg, Dawsonite Kompensan 0.2kg and polyacrylonitrile fibre 10kg, add in cutter and mix;
(2) add polyethylene glycol 8kg, laruyl alcohol 3kg, stir 20 minutes at 80 DEG C, add tung oil acid anhydride 0.2kg, mix, in airtight condition, melting at 205 DEG C, with the speed spinning of 1600m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Embodiment 3
(1) take the cotton fiber 81kg of methyl triacetoxysilane process, epoxy propane butyl ether 20kg, ethyl cellulose 7kg, brown coal cerinic acid second diester 1kg, silk-fibroin 2kg, Dawsonite Kompensan 0.8kg, add in cutter and mix;
(2) add polyethylene glycol 10kg, laruyl alcohol 5kg, stir 40 minutes at 100 DEG C, add tung oil acid anhydride 1.8kg, mix, in airtight condition, melting at 215 DEG C, with the speed spinning of 1800m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Embodiment 4
(1) take the cotton fiber 81kg of methyl triacetoxysilane process, epoxy propane butyl ether 20kg, ethyl cellulose 7kg, brown coal cerinic acid second diester 3kg, silk-fibroin 2kg, Dawsonite Kompensan 0.8kg, add in cutter and mix;
(2) add polyethylene glycol 10kg, laruyl alcohol 5kg, stir 40 minutes at 100 DEG C, add tung oil acid anhydride 1.8kg, mix, in airtight condition, melting at 215 DEG C, with the speed spinning of 1800m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Embodiment 5
(1) take the cotton fiber 81kg of methyl triacetoxysilane process, epoxy propane butyl ether 20kg, ethyl cellulose 7kg, brown coal cerinic acid second diester 3kg, silk-fibroin 2kg, Dawsonite Kompensan 0.2kg, add in cutter and mix;
(2) add polyethylene glycol 10kg, laruyl alcohol 5kg, stir 40 minutes at 100 DEG C, add tung oil acid anhydride 1.8kg, mix, in airtight condition, melting at 215 DEG C, with the speed spinning of 1800m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Comparative example 1
(1) take the cotton fiber 81kg of methyl triacetoxysilane process, epoxy propane butyl ether 20kg, ethyl cellulose 7kg, silk-fibroin 2kg, Dawsonite Kompensan 0.2kg, add in cutter and mix;
(2) add polyethylene glycol 10kg, laruyl alcohol 5kg, stir 40 minutes at 100 DEG C, add tung oil acid anhydride 1.8kg, mix, in airtight condition, melting at 215 DEG C, with the speed spinning of 1800m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Comparative example 2
(1) take the cotton fiber 81kg of methyl triacetoxysilane process, epoxy propane butyl ether 20kg, ethyl cellulose 7kg, brown coal cerinic acid second diester 3kg, silk-fibroin 2kg, add in cutter and mix;
(2) add polyethylene glycol 10kg, laruyl alcohol 5kg, stir 40 minutes at 100 DEG C, add tung oil acid anhydride 1.8kg, mix, in airtight condition, melting at 215 DEG C, with the speed spinning of 1800m/min, by tractive process, obtained anti-stain textile material.
The performance test results of obtained anti-stain textile material is as shown in table 1.
Scribbling lipstick by the textile material of embodiment 1-5 and comparative example 1-2, add in the aqueous solution of soap class washing agent, surveying its greasiness removal time by stirring.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.