CN104875518A - Coating material, thermal transfer printing paper, and thermal transfer printing paper preparation method - Google Patents
Coating material, thermal transfer printing paper, and thermal transfer printing paper preparation method Download PDFInfo
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- CN104875518A CN104875518A CN201410070616.6A CN201410070616A CN104875518A CN 104875518 A CN104875518 A CN 104875518A CN 201410070616 A CN201410070616 A CN 201410070616A CN 104875518 A CN104875518 A CN 104875518A
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Abstract
The present invention discloses a coating material, thermal transfer printing paper, and a thermal transfer printing paper preparation method, wherein per 100 parts by mass of the coating material comprises 40-60 parts by mass of light calcium carbonate, 20-40 parts by mass of heavy calcium carbonate, 10-30 parts by mass of porcelain clay, and 2-10 parts by mass of an Octadecanamide and ethylene-vinyl acetate copolymer mixing emulsion. According to the present invention, the coating material has characteristics of good ink absorption and good toner adhesion rate, and the thermal transfer printing paper using the coating material can overcome the limitation of requirement of special production equipment of the thermal transfer printing paper using the conventional silica formula.
Description
Technical field
The present invention relates to a kind of coating, hot transfer printing paper using and preparation method thereof.
Background technology
China adhesive label market still presents the good continuity impetus at high speed development, but the hot transfer printing paper using of high-quality adhesive sticker is all based on import, the subject matter of domestic paper is that the adaptability performance of the different print speed of different type of machines of hot transfer printing is different, and main cause is that high-quality hot transfer printing art paper coating is mainly main with silicon dioxide body.
And internal copper millboard manufacturer is because the hot transfer printing art paper that the limitation of the factors such as technology, equipment and cost fails to realize having silica system paint formulation is produced.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of coating, hot transfer printing paper using and preparation method thereof, coating of the present invention has good absorbency and carbon dust adhesive rate, the limitation making the hot transfer printing paper using utilizing this coating can overcome the hot transfer printing paper using of Normal silica formula system to need special producing equipment.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is: provide a kind of coating, wherein, the described coating of 100 mass parts comprises following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates; 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion.
Wherein, described precipitated calcium carbonate to be average grain diameter the be needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron; Described powdered whiting is the powdered whiting of average grain diameter 0.4 ~ 0.8 micron; Described china clay is the china clay of average grain diameter 0.2 ~ 0.6 micron.
Wherein, in described stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, the mass ratio of stearic amide and ethylene-vinyl acetate copolymer is 30 ~ 45:70 ~ 55.
Wherein, 5 ~ 12 mass parts styrene-butadiene latexes are also comprised in the described coating of 100 mass parts.
Wherein, described coating also comprises at least one among resistance to hydrated agent, dispersant, defoamer.
Wherein, described coating is not containing silica.
For solving the problems of the technologies described above, another technical solution used in the present invention is: provide a kind of hot transfer printing paper using, and described hot transfer printing paper using comprises sized paper and coats the coating on described sized paper surface, and wherein, described coating is above-mentioned coating.
Wherein, the surface roughness that described sized paper is is less than 5.0 microns.
Wherein, the surface roughness that described sized paper is is less than 4.0 microns.
For solving the problems of the technologies described above, another technical scheme provided by the invention is: the preparation method providing a kind of hot transfer printing paper using, described preparation method comprises: preparation coating, and wherein, coating described in 100 mass parts comprises following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates; 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion; Prepare sized paper; At described sized paper surface coating composition.
Wherein, the amount of described sized paper surface coating composition is 10-20g/m
2.
Wherein, described method also comprises: the sized paper being coated with described coating is carried out press polish process at the nip of more than 120KN/m pressure.
Wherein, described precipitated calcium carbonate to be average grain diameter the be needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron; Described powdered whiting is the powdered whiting of average grain diameter 0.4 ~ 0.8 micron; Described china clay is the china clay of average grain diameter 0.2 ~ 0.6 micron.
Wherein, when preparing described coating, be that 30 ~ 45:70 ~ 55 first mix in mass ratio by described stearic amide and ethylene-vinyl acetate copolymer, and then put in described coating.
Wherein, 5 ~ 12 mass parts styrene-butadiene latexes are also comprised in the described coating of 100 mass parts.
Wherein, when configuring described coating, at least one of also adding in described coating among resistance to hydrated agent, dispersant, defoamer.
The invention has the beneficial effects as follows: the situation being different from prior art, coating of the present invention is using the precipitated calcium carbonate of certain mass part, powdered whiting, china clay and stearic amide and ethylene-vinyl acetate copolymer mixed emulsion as main formula, by such formula, the compatibility of coating surface to carbon belt printing ink can not only be promoted, promote coating to carbon belt printing ink absorption property simultaneously, and the limitation that existing silica system paint formulation needs special producing equipment can be overcome.
Accompanying drawing explanation
Fig. 1 is the structural representation of the hot transfer printing paper using of the present invention;
Fig. 2 is the flow chart of preparation method's embodiment of the hot transfer printing paper using of the present invention.
Detailed description of the invention
Core concept of the present invention is for internal copper millboard manufacturer because the hot transfer printing art paper that the limitation of the factors such as technology, equipment and cost fails to realize the having silica system formula coating technical problem of producing, a kind of coating is provided, and the hot transfer printing paper using using this coating and preparation method thereof, this coating has good absorbency and carbon dust inhales adhesive rate, thus make the hot transfer printing paper using hot transfer printing bar code utilizing this coating clear, be applicable to high speed print speed region.
Below in conjunction with detailed description of the invention, technical scheme of the present invention is described in detail, but these are the specific embodiment of the present invention, not in order to limit protection scope of the present invention.
In the embodiment of a kind of coating provided by the invention, the coating of 100 mass parts comprises following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates, 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay can also be comprised in the coating of 00 mass parts; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion.
Wherein, sprawl preferably to guarantee to realize the paper surface that ink is scribbling coating and be adsorbed on coating surface preferably, in embodiment of the present invention, the preferred average grain diameter of precipitated calcium carbonate is the needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron, and such as particle diameter is any one precipitated calcium carbonate of 0.4,0.5,0.6,0.7,0.8,0.9 micron.The preferred average grain diameter of weight calcium carbonate is the powdered whiting of 0.4 ~ 0.8 micron.Such as particle diameter is any one powdered whiting of 0.4,0.5,0.6,0.7,0.8 micron.The preferred average grain diameter of china clay is the china clay of 0.2 ~ 0.6 micron, and such as particle diameter is any one china clay of 0.2,0.3,0.4,0.5,0.6 micron.
Be that 0.4 ~ 1.0 micron of needle-like precipitated calcium carbonate is for paint structure framework with particle diameter, the powdered whiting of 0.4 ~ 0.8 micron and the narrower china clay of 0.2 ~ 0.6 micron of domain size distribution can under lower calendering pressure condition echelon superposition formed macroscopical smoothness better but the larger unique coating surface structure of local roughness, macroscopic view smoothness better can make a certain amount of carbon belt printing ink transfer amount situation can paper surface sprawl more even, the feature that local roughness is larger can promote transfer after ink can better be attached to coating surface.
In order to stable firmly paint structure, in a preferred embodiment, in the above-mentioned coating of 100 mass parts, can further include 5 ~ 12 mass parts styrene-butadiene latexes.Stable paint structure is carried out by styrene-butadiene latex.
Wherein, in embodiment of the present invention, in stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, the mass ratio of stearic amide and ethylene-vinyl acetate copolymer is 30 ~ 45:70 ~ 55.Such as 30:70,35:65,40:60,45:55 etc.
Certainly, in the coating of embodiment of the present invention, by adding styrene-butadiene latex, stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, stablize at styrene-butadiene latex on the basis of the structure of coating, the function being embedded in stearic amide in paint structure and ethylene-vinyl acetate copolymer mixed emulsion is that point-like increases coating to the compatibility of carbon belt printing ink and adhesive force.And stearic amide and ethylene-vinyl acetate copolymer two kinds of emulsions are first mixed, then add in coating with the form of mixed emulsion, after contributing to the fine dispersion of mixed emulsion in coating and drying, point-like increases the uniformity coefficient of compatibility and adhesive force.
As the preferred embodiment of one, on the basis of the coating of above arbitrary embodiment, described coating can further include at least one among resistance to hydrated agent, dispersant, defoamer.
It should be noted that, the coating in the arbitrary embodiment of the present invention, not containing silica composition.
In order to further describe the component proportion of coating of the present invention, as a kind of concrete example, below provide the embodiment of the coating of multiple different component, the component of the coating of several different embodiment refers to following table 1:
Table 1: the component formula of several different embodiment coating
On the basis of each embodiment of the coating provided above, the present invention further provides a kind of hot transfer printing paper using, refer to Fig. 1, hot transfer printing paper using of the present invention comprises sized paper 01 and coats the coating 02 on sized paper 01 surface, wherein, coating 02 is the coating that above-mentioned arbitrary embodiment provides.
In present embodiment, the proportion relation of the composition of the coating of hot transfer printing paper using surface coating and each composition see above detailed description of giving coating embodiment, can not repeat them here.The coated weight of coating on sized paper surface can be 10-20g/m
2, more preferably coated weight is 12-18g/m
2, preferred coated weight is 15g/m
2.
The sized paper surface roughness of the hot transfer printing paper using of present embodiment is preferably less than 5.0 microns, is more preferably and is less than 4.0 microns.
After the surperficial coating composition 02 of sized paper 01, the hot transfer printing paper using that can be used for adhesive sticker printing with good planarization and uniform pore structure can be obtained after more than 120KN/m pressure nip supercalendering.
In actual application, can as required at two surfaces all coating compositions 02 that sized paper 01 is relative.
The present invention also provides a kind of preparation method of hot transfer printing paper using, refers to Fig. 2, and Fig. 2 is the flow chart of preparation method's embodiment of the hot transfer printing paper using of the present invention, and the preparation method of the hot transfer printing paper using of the present invention comprises:
S101: preparation coating, wherein, 100 mass parts coating comprise following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates, 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion;
First preparation is used for the coating of hot transfer printing paper using, and wherein, this coating of 100 mass parts comprises following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates, 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion.
Wherein, sprawl preferably to guarantee to realize the paper surface that ink is scribbling coating and be adsorbed on coating surface preferably, in embodiment of the present invention, the preferred average grain diameter of precipitated calcium carbonate is the needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron, and such as particle diameter is any one precipitated calcium carbonate of 0.4,0.5,0.6,0.7,0.8,0.9 micron.The preferred average grain diameter of weight calcium carbonate is the powdered whiting of 0.4 ~ 0.8 micron.Such as particle diameter is any one powdered whiting of 0.4,0.5,0.6,0.7,0.8 micron.The preferred average grain diameter of china clay is the china clay of 0.2 ~ 0.6 micron, and such as particle diameter is any one china clay of 0.2,0.3,0.4,0.5,0.6 micron.
Be that 0.4 ~ 1.0 micron of needle-like precipitated calcium carbonate is for paint structure framework with particle diameter, the powdered whiting of 0.4 ~ 0.8 micron and the narrower china clay of 0.2 ~ 0.6 micron of domain size distribution can under lower calendering pressure condition echelon superposition formed macroscopical smoothness better but the larger unique coating surface structure of local roughness, macroscopic view smoothness better can make a certain amount of carbon belt printing ink transfer amount situation can paper surface sprawl more even, the feature that local roughness is larger can promote transfer after ink can better be attached to coating surface.
In order to stable firmly paint structure, in a preferred embodiment, in the above-mentioned coating of 100 mass parts, can further include 5 ~ 12 mass parts styrene-butadiene latexes.Stable paint structure is carried out by styrene-butadiene latex.
Wherein, in embodiment of the present invention, in stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, the mass ratio of stearic amide and ethylene-vinyl acetate copolymer is 30 ~ 45:70 ~ 55.Such as 30:70,35:65,40:60,45:55 etc.
Certainly, in the coating of embodiment of the present invention, styrene-butadiene latex, stearic amide and ethylene-vinyl acetate copolymer mixed emulsion is added in coating, stablize at styrene-butadiene latex on the basis of the structure of coating, the function being embedded in stearic amide in paint structure and ethylene-vinyl acetate copolymer mixed emulsion is that point-like increases coating to the compatibility of carbon belt printing ink and adhesive force.And stearic amide and ethylene-vinyl acetate copolymer two kinds of emulsions are first mixed, then add in coating with the form of mixed emulsion, after contributing to the fine dispersion of mixed emulsion in coating and drying, point-like increases the uniformity coefficient of compatibility and adhesive force.
As the preferred embodiment of one, on the basis of the coating of above arbitrary embodiment, described coating can further include at least one among resistance to hydrated agent, dispersant, defoamer.Wherein, the deal that resistance to hydrated agent, dispersant, defoamer add can select suitable deal according to actual needs.
It should be noted that, the coating in the arbitrary embodiment of the present invention, not containing silica composition.
S102: prepare sized paper;
Sized paper surface roughness for hot transfer printing paper using is preferably less than 5.0 microns, and more preferably surface roughness is less than 4.0 microns.
Certainly, in actual application, step S101 and S102 does not strictly distinguish sequencing, even likely synchronously carries out.
S103: at sized paper surface coating composition;
At the coating of the above-mentioned arbitrary embodiment configuration of sized paper surface coating.Wherein, the coated weight of coating on sized paper surface can be 10-20g/m
2, more preferably coated weight is 12-18g/m
2, preferred coated weight is 15g/m
2.
After the coating composition of sized paper surface, the hot transfer printing paper using that can be used for adhesive sticker printing with good planarization and uniform pore structure can be obtained after more than 120KN/m pressure nip supercalendering.
Wherein, in actual application, all can be coated with above-mentioned coating on two surfaces that sized paper is relative as required.
In order to the effect of definitely hot transfer printing paper using of the present invention, the bar code printing test result of the hot transfer printing paper using that the coating below providing several specific embodiment different ratio component obtains, refers to following table 2:
Table 2: different hot transfer printing paper using bar code printing test result
The detailed description of the embodiment of the coating provided by the invention described above, hot transfer printing paper using and preparation method thereof, be appreciated that, coating of the present invention is using the precipitated calcium carbonate of certain mass part, powdered whiting, china clay, stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, as main formula, by such formula, the compatibility of coating surface to carbon belt printing ink can not only be promoted, promote coating to carbon belt printing ink absorption property simultaneously, and existing silica can be overcome embody paint formulation and need the limitation of special producing equipment.
In addition, form on the basis of the basic structure of coating at precipitated calcium carbonate, powdered whiting, styrene-butadiene latex and other additional functionality material can also be added as resistance to hydrated agent, dispersant, defoamer etc.
And additionally provide precipitated calcium carbonate in embodiment of the present invention, powdered whiting, the average particle size range of china clay, be that 0.4 ~ 1.0 micron of needle-like precipitated calcium carbonate is for paint structure framework with particle diameter, the powdered whiting of 0.4 ~ 0.8 micron and the narrower china clay of 0.2 ~ 0.6 micron of domain size distribution can under lower calendering pressure condition echelon superposition formed macroscopical smoothness better but the larger unique coating surface structure of local roughness, macroscopic view smoothness better can make can sprawl more even at paper surface in the situation of a certain amount of carbon belt printing ink transfer amount, the feature that local roughness is larger can promote that the ink after shifting can better be attached to coating surface.
And styrene-butadiene latex add the structure can stablizing coating, stablize at styrene-butadiene latex on the basis of the structure of coating, be embedded in stearic amide in paint structure and ethylene-vinyl acetate copolymer mixed emulsion better can increase coating to the affinity of carbon belt printing ink and adhesive force.
The foregoing is only embodiments of the present invention; not thereby the scope of the claims of the present invention is limited; every utilize description of the present invention and accompanying drawing content to do equivalent structure or equivalent flow process conversion; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.
Claims (16)
1. a coating, is characterized in that, coating described in 100 mass parts comprises following mass component than material:
40 ~ 60 mass parts precipitated calcium carbonates;
20 ~ 40 mass parts powdered whitings;
10 ~ 30 mass parts china clay;
The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion.
2. coating according to claim 1, is characterized in that, described precipitated calcium carbonate to be average grain diameter the be needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron; Described powdered whiting is the powdered whiting of average grain diameter 0.4 ~ 0.8 micron; Described china clay is the china clay of average grain diameter 0.2 ~ 0.6 micron.
3. coating according to claim 1, is characterized in that, in described stearic amide and ethylene-vinyl acetate copolymer mixed emulsion, the mass ratio of stearic amide and ethylene-vinyl acetate copolymer is 30 ~ 45:70 ~ 55.
4. coating according to claim 1, is characterized in that, also comprises 5 ~ 12 mass parts styrene-butadiene latexes in the described coating of 100 mass parts.
5. the coating according to any one of claim 1-4, is characterized in that, described coating also comprises at least one among resistance to hydrated agent, dispersant, defoamer.
6. the coating according to any one of claim 1-4, is characterized in that, described coating is not containing silica.
7. a hot transfer printing paper using, is characterized in that, described hot transfer printing paper using comprises sized paper and coats the coating on described sized paper surface, and wherein, described coating is the coating described in any one of claim 1-6.
8. hot transfer printing paper using according to claim 7, it is characterized in that, the surface roughness that described sized paper is is less than 5.0 microns.
9. hot transfer printing paper using according to claim 8, it is characterized in that, the surface roughness that described sized paper is is less than 4.0 microns.
10. a preparation method for hot transfer printing paper using, is characterized in that, described preparation method comprises:
Preparation coating, wherein, coating described in 100 mass parts comprises following mass component than material: 40 ~ 60 mass parts precipitated calcium carbonates; 20 ~ 40 mass parts powdered whitings; 10 ~ 30 mass parts china clay; The stearic amide of 2 ~ 10 mass parts and ethylene-vinyl acetate copolymer mixed emulsion;
Prepare sized paper;
At described sized paper surface coating composition.
11. preparation methods according to claim 10, is characterized in that, the amount of described sized paper surface coating composition is 10-20g/m
2.
12. preparation methods according to claim 10 or 11, it is characterized in that, described method also comprises: the sized paper being coated with described coating is carried out press polish process at the nip of more than 120KN/m pressure.
13. preparation methods according to claim 10, is characterized in that, described precipitated calcium carbonate to be average grain diameter the be needle-like precipitated calcium carbonate of 0.4 ~ 1.0 micron; Described powdered whiting is the powdered whiting of average grain diameter 0.4 ~ 0.8 micron; Described china clay is the china clay of average grain diameter 0.2 ~ 0.6 micron.
14. preparation methods according to claim 10, is characterized in that, when preparing described coating, be that 30 ~ 45:70 ~ 55 first mix in mass ratio, and then put into described stearic amide and ethylene-vinyl acetate copolymer in described coating.
15. preparation methods according to claim 10, is characterized in that, also comprise 5 ~ 12 mass parts styrene-butadiene latexes in the described coating of 100 mass parts.
16. preparation methods according to claim 10, is characterized in that, when configuring described coating, and at least one of also adding in described coating among resistance to hydrated agent, dispersant, defoamer.
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| CN107287982A (en) * | 2017-06-30 | 2017-10-24 | 常州豫春化工有限公司 | A kind of preparation method of thermal transfer paint for papers |
| CN110168162A (en) * | 2017-01-25 | 2019-08-23 | 三菱制纸株式会社 | Paper is used in printing and dyeing used in the paper method of printing and dyeing |
| CN110656540A (en) * | 2019-09-27 | 2020-01-07 | 宜兴市佳普林新材料有限公司 | Coating on low-gram-number thermal sublimation transfer paper |
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| CN104875518B (en) | 2017-12-19 |
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