CN104873433B - A kind of wormwood face cream and preparation method thereof - Google Patents
A kind of wormwood face cream and preparation method thereof Download PDFInfo
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention disclose a kind of wormwood tea face cream and its manufacture method, the wormwood tea face cream include Aqueous extracts obtained from being extracted in the wild wormwood through ageing in 3 years after drying with the alcohol extract component that is extracted through ethanol, propane diols in Chinese medicine grass-leaved sweetflag, scutellariae,radix, kuh-seng and from the Chinese medicines such as radix glycyrrhizae, wild soybean seed, oat kernel, azadirachta leaf, althaea root, corn flower through water and and wormwood, the extract component such as probiotics fermention liquid of Chinese medicine.After the collocation balanced with 16 mixed alcohols, jojoba oil, seed of Flos Camelliae Japonicae oil, Purple Perilla Seed Oil etc. of the active ingredient of different extraction processes extraction, reasonable formula, the wormwood tea face cream product with superior protection can be made from wormwood, Chinese medicine in these.
Description
Technical field
The present invention relates to a kind of wormwood face cream and preparation method thereof, belong to cosmetics and skincare product technical field.
Background technology
The fast development of beauty industry, Gospel is brought to vast people seeking beauty.But due to southern exposure industry development early period
Lack of standard and eager for instant success and quick profits property, cause some products of inferior quality, the quick-acting product streams for even having side effect to skin enter the market
, deep or shallow injury is caused to some people seeking beauties.Furthermore the environment such as the food pollution of today's society, air pollution
Problem also affects the healthy and beautiful of the mankind in different degrees of so that no matter interior people are with diet or cosmetics for external use, all
There is the trend that " toxin " increases and accumulate.Therefore only in terms of the aspect of external application cosmetics and skincare product, further develop with toxin expelling
The pure natural skin care item of maintenance action will be current and following development trend.
Wormwood, also known as " doctor's grass ".It is the Chinese herbal medicine that people are used for " keeping away evil to get rid of evils " since ancient times.Modern science proves:
It is either interior containing multiple efficacies components such as volatile oil, flavones, eudesmane, triterpenes and Protein microassay elements in wormwood
Clothes or external application can produce human body the maintenance action of " strengthening vital QI to eliminate pathogenic factors ".But wormwood has pros and cons duality in itself, though
There are lifting resistance of human body and the positive acting of immunity, but secondary work can be also caused to human body after excessive edible or a large amount of external applications
With, or even damage.The feature of this pros and cons dual character causes this effect of wormwood " to cure grass " in the day of modern well
Often in life, it should not be grasped and used by the people of fast pace life.And apply to cosmetics and skincare product especially face cream class skin care
Patent document in product does not have also.Therefore the advantages of how making full use of wormwood, keep away its shortcoming, and balanced collocation, reasonable combination are arrived
In the common skin care item face cream product of people's energy, it will merit attention and further investigate.
The content of the invention
The present situation of blank is still occupied for application of the current wormwood in skin care face cream, the present invention provides a kind of wormwood face cream
And preparation method thereof, the bold use of the present invention " 3 years Chen Ai ", and coordinate wormwood, wild soybean seed, grass-leaved sweetflag, Neem
Leaf, scutellariae,radix, Sakura leaf, tree peony root, oat kernel, althaea root, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, cordate houttuynia, Pu
The Chinese medicines such as public English, saururus chinensis, purslane, kuh-seng, first carry out ethanol, propane diols extracts concentrate, then carries out water and extract
Aqueous extracts, then carry out probiotics fermention processing again, finally share alcohol extract, Aqueous extracts and zymotic fluid three.This new formula,
New process can be preferably using wormwood and kinds of traditional Chinese medicines in terms of toxin expelling skin care the effect of, and substantially reduces the disadvantage of wormwood in itself
End so that the wormwood face cream product of the invention can reach good skin effect and promote and apply effect.
To achieve the above object, the present invention uses following technical scheme:
A kind of wormwood face cream, is made of the component of following parts by weight:
(1) oil phase component:The oil phase component is made of following components in parts by weight:16 mixed alcohols 1~1.5
Part, 16 stearyl alcohols and 2~4 parts of 16 octadecyl glucosides, tristerin and PEG-100 stearates 2
~3 parts, 2~4 parts of jojoba oil, 2~4 parts of isomery hexadecane hydrocarbon, 1~3 part of seed of Flos Camelliae Japonicae oil, 1~2 part of Purple Perilla Seed Oil, Pork and beans
Cool 1~3 part of isopropyl propionate, 2~4 parts of dimethicone, 0.2~0.3 part of methyl hydroxybenzoate, 0.1~0.15 part of propylben,
0.03~0.05 part of di-tert-butyl p-cresol;
(2) water phase components:The water phase components are made of following components in parts by weight:5~8 parts of glycerine, modified corn sugar
Starch (commodity English name:MOISYRUP, is provided by Shanghai Shun Tuo scientific & trading Co., Ltd.s) 2~4 parts, 1~2 part of trehalose, trimethyl
2~4 parts of glycine, 40~60 parts of self-control C extracting solutions, the self-control C extracting solutions are made from the following raw materials in parts by weight:Radix glycyrrhizae 5
~10 parts, 3~5 parts of wild soybean seed, 4~5 parts of oat kernel, each 3~4 parts of tree peony root, althaea root, cordate houttuynia, Neem
Each 1~3 part of leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, purslane;
(3) extracting solution component:Make 2~4 parts of A extracting solutions, 5~10 parts of self-control D extracting solutions by oneself;
(4) assistant for emulsifying agent component:0.5~1 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5) preservative:The mixture of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.1-0.15 parts;
(6) essence:0.01-0.02 parts of floral perfume.
The preparation method of wormwood face cream, includes the following steps:
(1) preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecanes
Base glucoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple
After perilla oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol weigh in proportion
Add in the stainless steel kettle of band stirring, complete, and the perseverance at 80~85 DEG C is dissolved by heating under the stirring of 20~30 revs/min of rotating speed
Temperature disinfection 20 minutes it is stand-by;
(2) preparation of water phase components:By the glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, from
C extracting solutions processed first dissolve by heating after weighing in proportion in stainless steel kettle, are then extracted into stainless steel homogeneous kettle, 20~30
Rev/min stirring under, continue to be heated to 80~85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) oil phase is slowly pumped into water phase, and carries out scraping wall stirring, 2- is stirred in the case where scraping wall rotating speed as 40-50 revs/min
3 minutes, high speed homogenization device is started homogeneous 3-5 minutes under 3000-5000 revs/min of high speed, will be scraped wall rotating speed afterwards and be dropped to 30-
40 revs/min, and it is cooled to 45-50 DEG C under this rotating speed;
(4) and then the self-control A extracting solutions of formula ratio is added and make D extracting solutions and assistant for emulsifying agent by oneself, at 20-30 revs/min
Stirred 20-30 minutes under rotating speed, continue to cool to 40 DEG C afterwards, added the preservative and essence of formula ratio, continue same
Stirred 15-20 minutes under rotating speed, you can discharging, is made wormwood face cream.
The preparation method of the self-control A extracting solutions comprises the following steps:
(1) Mao Pus, scutellariae,radix, kuh-seng coarse powder are broken into≤segment of 3cm or the small pieces of diameter≤3cm, weigh wormwood 5~
8 parts, 3~6 parts of grass-leaved sweetflag, scutellariae,radix, each 4~6 parts of kuh-seng, 10~15 parts of propane diols, volumetric concentration is 60%~80% second
600~700 parts of alcoholic solution, at 70~90 DEG C, be heated to reflux alcohol extracting 1~3 it is small when, with being respectively obtained after 600 mesh filter-cloth filterings
Filter residue 1. with alcohol extract 1.;
(2) filter residue obtained in the step (1) 1. middle addition volumetric concentration for 60%~80% ethanol solution 500~
600 parts, 5~10 parts of propane diols, at 70~90 DEG C, be heated to reflux alcohol extracting 1~3 it is small when, with being filtered after 600 mesh filter-cloth filterings
Slag 2. with alcohol extract 2.;
(3) by the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 30~50
During part, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, self-control A is named as
Extracting solution;
(4) filter residue obtained in the step (2) 2. 300~400 parts of deionized waters of middle addition, are heated to seething with excitement, and protect
Hold slight boiling condition boil 0.8~1.0 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5) obtained by the step (4) filter residue 3. in add 200~300 parts of deionized water, be heated to seething with excitement, and micro-
Boiling state boil 0.5~0.8 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6) by Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng,
Water evaporation quantity is controlled, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed.
The preparation method of the self-control C extracting solutions comprises the following steps:
(1) 5~10 parts of radix glycyrrhizae, 3~5 parts of wild soybean seed, 4~5 parts of oat kernel, tree peony root, althaea root, fish raw meat are weighed
Each 3~4 parts of grass, azadirachta leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, purslane
Each 1~3 part, by the larger coarse crushing of partial block, leaf in these Chinese medicines into after≤the segment of 3cm or the small pieces of diameter≤3cm plus
Enter into enamel Chinese medicine extracting tank;
(2) when boiling for the first time, weigh 600~700 parts of deionized water and add in enamel Chinese medicine extracting tank, soak 30 minutes
After be heated to seething with excitement, and be maintained at slight boiling condition boil 0.8~1.0 it is small when, then carry filter residue with 600 mesh filter-cloth filterings up to water
1. with Aqueous extracts 1. ';
(3) 500~600 parts of deionized water is added in 1. water made from step (2) carries filter residue, is heated to seething with excitement,
And be maintained at slight boiling condition boil 0.6~0.8 it is small when, 2. and Aqueous extracts then carry filter residue with 600 mesh filter-cloth filterings up to water
②’;
(4) by above-mentioned Aqueous extracts 1. ', Aqueous extracts are 2. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, control moisture evaporation
Amount, makes finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself.
The preparation method of the self-control D extracting solutions comprises the following steps:(1) filter residue 2. middle addition sucrose 5 is carried in the water
~8 parts, 3~5 parts of glucose, 0.3~0.5 part of dipotassium hydrogen phosphate, 0.1~0.2 part of sodium chloride, 300~400 parts of pure water, adds
For heat to seething with excitement, constant temperature disinfection 20 minutes, is then cooled to 30~35 DEG C, adds 50~100 parts of self-control C extracting solutions, (2) and then presses
2~3% inoculum concentration access for bottom material total amount of fermenting expands the Aureobasidium pullulans strain after culture, and (strain is micro- purchased from Chinese industrial
Biological inoculum collection, bacterium numbering:CICC41349), fermented and cultured is after 1~3 day, add fermentation bottom material total amount 1~
(strain is purchased from Chinese industrial Culture Collection, bacterium numbering to 2% Pichia pastoris strain:CICC33024) and send out
((strain is purchased from Chinese industrial Culture Collection to 1~3% lactobacillus plantarum strain of ferment bottom material total amount, and strain is compiled
Number:CICC6240)), continue fermented and cultured 1~3 day, system temperature is then dropped to 28~30 DEG C again, continues fermentation 1~2
Self-control B extracting solutions and filter residue are added after it 4., continues fermentation 2~3 days, take zymotic fluid to examine thalline sum, if more than
500CFU/ML then continues fermentation 1~5 day or with ozone sterilization system for handling, until viable bacteria body is depleted in system, until body
Zymotic fluid, is then crossed 600 mesh filter clothes and filtered out by thalline sum≤500CFU/ML in system, (3) and then is concentrated in vacuo below 50 DEG C
To the 1/2 of total fermentation filtrate volume, the concentrate of fermentation extracting solution is made, that is, makes D extracting solutions by oneself.
The selection and early-stage preparations of wormwood in the present invention:Contain more volatile oil and taste component in fresh wormwood, if directly
Connect extraction to be applied in skin care item, not only taste is larger, also because the pathogenic dryness in wormwood is too big skin can be caused uncomfortable.Therefore this hair
Cleaned after the bright collection by wild wormwood, first pass through solarization repeatedly and dry product is made, be then placed on shady and cool dry, draughty
Indoor lucifuge stores 3 years, makes the aging of wormwood slowly, disperses volatile oil excessive in wormwood, and mitigates its pathogenic dryness, Ran Houzai
Coarse powder is broken into≤3CM segments use.
Compared with prior art, beneficial effects of the present invention are:Both wild wormwood had been set about to shine from the pretreatment of wormwood
Carries out ageing in 3 years after dry, but carried from technique using water, alcohol refers to the new and innovative ways that probiotics fermention is combined, wormwood can be made
It is this seldom to apply to skin care production by " doctor grass " of public use is relatively mild after going pathogenic dryness, reduction and converting some anaphylactogens
In product.Both the advantages of retaining and add " the keeping away evil to get rid of evils " of wormwood in itself, lifting resistance of human body and immunity, and will can end
The gas of the too strong irritability of grass reduces, and side effect greatly reduces, meanwhile, the cooperation of the component such as wormwood and plurality of Chinese, can also play
Equilibrium collocation, the effect having complementary advantages.Therefore the present invention has not only filled up blank of the wormwood tea in skin care item application, also to be vast
People seeking beauty provides a novel skin care non-defective unit, this is in the modern society of the pollution getting worse such as air instantly, environment, nothing
It is suspected to be the big Gospel of people.
Embodiment
Embodiment 1
The preparation method for making A extracting solutions in the present embodiment by oneself comprises the following steps:
(1) Mao Pus, scutellariae,radix, kuh-seng coarse powder are broken into≤segment of 3cm or the small pieces of diameter≤3cm, weigh wormwood 8
Part, 4 parts of grass-leaved sweetflag, scutellariae,radix, each 4 parts of kuh-seng, 15 parts of propane diols, volumetric concentration is 80% 700 parts of ethanol solution, at 90 DEG C
Under, be heated to reflux alcohol extracting 3 it is small when, with respectively obtained after 600 mesh filter-cloth filterings filter residue 1. with alcohol extract 1.;
(2) 1. middle addition volumetric concentration is 600 parts of 80% ethanol solution to the filter residue obtained in the step (1), propane diols
10 parts, at 90 DEG C, be heated to reflux alcohol extracting 1~3 it is small when, with obtained after 600 mesh filter-cloth filterings filter residue 2. with alcohol extract 2.;
(3) by the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 30 parts
When, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, it is named as self-control A and carries
Take liquid;
(4) filter residue obtained in the step (2) 2. 400 parts of deionized waters of middle addition, are heated to seething with excitement, and be maintained at micro-
Boiling state boil 1.0 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5) obtained by the step (4) filter residue 3. in add 200 parts of deionized water, be heated to seething with excitement, and in slight boiling condition
Boil 0.6 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6) by Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng,
Water evaporation quantity is controlled, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed.
The preparation method for making C extracting solutions in the present embodiment by oneself comprises the following steps:
(1) 6 parts of radix glycyrrhizae, 3 parts of wild soybean seed, 5 parts of oat kernel, each 4 parts of tree peony root, althaea root, cordate houttuynia, print are weighed
Chinaberry leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, each 2 parts of purslane are spent, by these
The larger coarse crushing of partial block, leaf is into being added to enamel Chinese medicine extracting tank after the≤segment of 3cm or the small pieces of diameter≤3cm in medicine
In;
(2) when boiling for the first time, weigh 600 parts of deionized water and add in enamel Chinese medicine extracting tank, immersion adds after 30 minutes
Heat to seethe with excitement, and be maintained at slight boiling condition boil 0.8 it is small when, then carry filter residue up to water with 600 mesh filter-cloth filterings and 1. carried with water
Liquid is 1. ';
(3) 600 parts of deionized water is added in 1. water made from step (2) carries filter residue, is heated to seething with excitement, and keep
Slight boiling condition boil 0.8 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 2. with Aqueous extracts 2. ';
(4) by above-mentioned Aqueous extracts 1. ', Aqueous extracts are 2. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, control moisture evaporation
Amount, makes finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself.
The preparation method for making D extracting solutions in the present embodiment by oneself comprises the following steps:(1) filter residue 2. middle addition is proposed in the water
7 parts of sucrose, 3 parts of glucose, 0.5 part of dipotassium hydrogen phosphate, 0.2 part of sodium chloride, 400 parts of pure water, is heated to seething with excitement, constant temperature disinfection
20 minutes, 35 DEG C are then cooled to, adds 80 parts of self-control C extracting solutions, (2) and then 3% inoculum concentration by fermentation bottom material total amount
Access expands the Aureobasidium pullulans strain after culture, and (strain is purchased from Chinese industrial Culture Collection, bacterium numbering:
CICC41349), after fermentation culture for 2 days, adding 2% Pichia pastoris strain of fermentation bottom material total amount, (strain is purchased from Chinese work
Industry Culture Collection, bacterium numbering:CICC33024) and fermentation bottom material total amount 3% lactobacillus plantarum strain
((strain is purchased from Chinese industrial Culture Collection, bacterium numbering:CICC6240)), fermented and cultured is continued 3 days, then
System temperature is dropped to 30 DEG C again, self-control B extracting solutions and filter residue is added 4. after continuing fermentation 2 days, continues fermentation 3 days, take
Zymotic fluid examines thalline sum, then continues fermentation if more than 500CFU/ML 4 days or with ozone sterilization system for handling, until system
Middle viable bacteria body is depleted, until zymotic fluid, is then crossed 600 mesh filter clothes and filtered out by thalline sum≤500CFU/ML in system,
(3) and then below 50 DEG C the 1/2 of total fermentation filtrate volume is concentrated in vacuo to, the concentrate of fermentation extracting solution is made, i.e., certainly
D extracting solutions processed.
The present embodiment wormwood face cream, substitutes the pure water component in wormwood face cream, by following heavy with obtained C extracting solutions
The component of amount part is made:
(1) oil phase component:The oil phase component is made of following components in parts by weight:16 1 part of mixed alcohols, 16
3 parts of 3 parts of stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearates, jojoba oil
2 parts, 3 parts of isomery hexadecane hydrocarbon, 2 parts of seed of Flos Camelliae Japonicae oil, 1 part of Purple Perilla Seed Oil, 2 parts of isopropyl myristate, dimethicone 3
Part, 0.2 part of methyl hydroxybenzoate, 0.15 part of propylben, 0.03 part of di-tert-butyl p-cresol;
(2) water phase components:The water phase components are made of following components in parts by weight:6 parts of glycerine, modified corn syrup
(commodity English name:MOISYRUP, is provided by Shanghai Shun Tuo scientific & trading Co., Ltd.s) 4 parts, 2 parts of trehalose, trimethylglycine 4
Part, 52 parts of self-control C extracting solutions;
(3) extracting solution component:Make 3 parts of A extracting solutions, 8 parts of self-control D extracting solutions by oneself;
(4) assistant for emulsifying agent component:0.5 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5) preservative:The mixture of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.1 part;
(6) essence:0.02 part of floral perfume.
The preparation method of the present embodiment wormwood face cream, includes the following steps:
(1) preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecanes
Base glucoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple
After perilla oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol weigh in proportion
Add in the stainless steel kettle of band stirring, dissolved by heating completely under the stirring of 30 revs/min of rotating speed, and the constant temperature disinfection 20 at 85 DEG C
Minute is stand-by;
(2) preparation of water phase components:By the glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, from
C extracting solutions processed first dissolve by heating after weighing in proportion in stainless steel kettle, are then extracted into stainless steel homogeneous kettle, at 30 revs/min
Stirring under, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) oil phase is slowly pumped into water phase, and carries out scraping wall stirring, 3 points are stirred in the case where scraping wall rotating speed as 50 revs/min
Clock, starts high speed homogenization device homogeneous 5 minutes under 4000 revs/min of high speed, will scrape wall rotating speed afterwards and drop to 35 revs/min, and
50 DEG C are cooled under this rotating speed;
(4) and then the self-control A extracting solutions of formula ratio is added and make D extracting solutions and assistant for emulsifying agent by oneself, in 30 revs/min of rotating speed
Lower stirring 20 minutes, continues to cool to 40 DEG C afterwards, adds the preservative and essence of formula ratio, continue to stir under same rotating speed
Mix 18 minutes, you can discharging, is made wormwood face cream.
Embodiment 2
The preparation method for making A extracting solutions in the present embodiment by oneself comprises the following steps:
(1) Mao Pus, scutellariae,radix, kuh-seng coarse powder are broken into≤segment of 3cm or the small pieces of diameter≤3cm, weigh wormwood 7
Part, 4 parts of grass-leaved sweetflag, scutellariae,radix, each 5 parts of kuh-seng, 13 parts of propane diols, volumetric concentration is 70% 600 parts of ethanol solution, at 85 DEG C
Under, be heated to reflux alcohol extracting 2 it is small when, with respectively obtained after 600 mesh filter-cloth filterings filter residue 1. with alcohol extract 1.;
(2) 1. middle addition volumetric concentration is 550 parts of 70% ethanol solution to the filter residue obtained in the step (1), propane diols 9
Part, at 80 DEG C, be heated to reflux alcohol extracting 2 it is small when, with obtained after 600 mesh filter-cloth filterings filter residue 2. with alcohol extract 2.;
(3) by the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 45 parts
When, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, it is named as self-control A and carries
Take liquid;
(4) filter residue obtained in the step (2) 2. 350 parts of deionized waters of middle addition, are heated to seething with excitement, and be maintained at micro-
Boiling state boil 0.8 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5) obtained by the step (4) filter residue 3. in add 260 parts of deionized water, be heated to seething with excitement, and in slight boiling condition
Boil 0.7 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6) by Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng,
Water evaporation quantity is controlled, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed.
The preparation method for making C extracting solutions in the present embodiment by oneself comprises the following steps:
(1) 9 parts of radix glycyrrhizae, 5 parts of wild soybean seed, 4 parts of oat kernel, each 3 parts of tree peony root, althaea root, cordate houttuynia, print are weighed
Chinaberry leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, each 3 parts of purslane are spent, by these
The larger coarse crushing of partial block, leaf is into being added to enamel Chinese medicine extracting tank after the≤segment of 3cm or the small pieces of diameter≤3cm in medicine
In;
(2) when boiling for the first time, weigh 600 parts of deionized water and add in enamel Chinese medicine extracting tank, immersion adds after 30 minutes
Heat to seethe with excitement, and be maintained at slight boiling condition boil 1.0 it is small when, then carry filter residue up to water with 600 mesh filter-cloth filterings and 1. carried with water
Liquid is 1. ';
(3) 600 parts of deionized water is added in 1. water made from step (2) carries filter residue, is heated to seething with excitement, and keep
Slight boiling condition boil 0.7 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 2. with Aqueous extracts 2. ';
(4) by above-mentioned Aqueous extracts 1. ', Aqueous extracts are 2. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, control moisture evaporation
Amount, makes finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself.
The preparation method for making D extracting solutions in the present embodiment by oneself comprises the following steps:(1) filter residue 2. middle addition is proposed in the water
8 parts of sucrose, 5 parts of glucose, 0.5 part of dipotassium hydrogen phosphate, 0.2 part of sodium chloride, 300 parts of pure water, is heated to seething with excitement, constant temperature disinfection
20 minutes, 30 DEG C are then cooled to, adds 60 parts of self-control C extracting solutions, (2) and then 2% inoculum concentration by fermentation bottom material total amount
Access expands the Aureobasidium pullulans strain after culture, and (strain is purchased from Chinese industrial Culture Collection, bacterium numbering:
CICC41349), after fermentation culture for 3 days, adding 2% Pichia pastoris strain of fermentation bottom material total amount, (strain is purchased from Chinese work
Industry Culture Collection, bacterium numbering:CICC33024) and fermentation bottom material total amount 2% lactobacillus plantarum strain
((strain is purchased from Chinese industrial Culture Collection, bacterium numbering:CICC6240)), fermented and cultured is continued 2 days, then
System temperature is dropped to 29 DEG C again, self-control B extracting solutions and filter residue is added 4. after continuing fermentation 1 day, continues fermentation 3 days, take
Zymotic fluid examines thalline sum, then continues fermentation if more than 500CFU/ML 3 days or with ozone sterilization system for handling, until system
Middle viable bacteria body is depleted, until zymotic fluid, is then crossed 600 mesh filter clothes and filtered out by thalline sum≤500CFU/ML in system,
(3) and then below 50 DEG C the 1/2 of total fermentation filtrate volume is concentrated in vacuo to, the concentrate of fermentation extracting solution is made, i.e., certainly
D extracting solutions processed.
The present embodiment wormwood face cream, substitutes the pure water component in wormwood face cream, by following heavy with obtained C extracting solutions
The component of amount part is made:
(1) oil phase component:The oil phase component is made of following components in parts by weight:16 1.5 parts of mixed alcohols, ten
2 parts of 2 parts of six stearyl alcohols and 16 octadecyl glucosides, tristerin and PEG-100 stearates, Jojoba
4 parts of oil, 4 parts of isomery hexadecane hydrocarbon, 3 parts of seed of Flos Camelliae Japonicae oil, 2 parts of Purple Perilla Seed Oil, 3 parts of isopropyl myristate, dimethicone 4
Part, 0.3 part of methyl hydroxybenzoate, 0.15 part of propylben, 0.03 part of di-tert-butyl p-cresol;
(2) water phase components:The water phase components are made of following components in parts by weight:8 parts of glycerine, modified corn syrup
(commodity English name:MOISYRUP, is provided by Shanghai Shun Tuo scientific & trading Co., Ltd.s) 3 parts, 1 part of trehalose, trimethylglycine 3
Part, 45 parts of self-control C extracting solutions;
(3) extracting solution component:Make 4 parts of A extracting solutions, 9 parts of self-control D extracting solutions by oneself;
(4) assistant for emulsifying agent component:0.9 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5) preservative:The mixture of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.1 part;
(6) essence:0.02 part of floral perfume.
The preparation method of the present embodiment wormwood face cream, includes the following steps:
(1) preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecanes
Base glucoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple
After perilla oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol weigh in proportion
Add in the stainless steel kettle of band stirring, dissolved by heating completely under the stirring of 25 revs/min of rotating speed, and the constant temperature disinfection 20 at 80 DEG C
Minute is stand-by;
(2) preparation of water phase components:By the glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, from
C extracting solutions processed first dissolve by heating after weighing in proportion in stainless steel kettle, are then extracted into stainless steel homogeneous kettle, at 25 revs/min
Stirring under, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) oil phase is slowly pumped into water phase, and carries out scraping wall stirring, 3 points are stirred in the case where scraping wall rotating speed as 45 revs/min
Clock, starts high speed homogenization device homogeneous 3 minutes under 5000 revs/min of high speed, will scrape wall rotating speed afterwards and drop to 30 revs/min, and
45 DEG C are cooled under this rotating speed;
(4) and then the self-control A extracting solutions of formula ratio is added and make D extracting solutions and assistant for emulsifying agent by oneself, in 25 revs/min of rotating speed
Lower stirring 30 minutes, continues to cool to 40 DEG C afterwards, adds the preservative and essence of formula ratio, continue to stir under same rotating speed
Mix 20 minutes, you can discharging, is made wormwood face cream.
Embodiment 3
The preparation method for making A extracting solutions in the present embodiment by oneself comprises the following steps:
(1) Mao Pus, scutellariae,radix, kuh-seng coarse powder are broken into≤segment of 3cm or the small pieces of diameter≤3cm, weigh wormwood 6
Part, 5 parts of grass-leaved sweetflag, scutellariae,radix, each 5 parts of kuh-seng, 14 parts of propane diols, volumetric concentration is 75% 650 parts of ethanol solution, at 75 DEG C
Under, be heated to reflux alcohol extracting 1.5 it is small when, with respectively obtained after 600 mesh filter-cloth filterings filter residue 1. with alcohol extract 1.;
(2) 1. middle addition volumetric concentration is 550 parts of 75% ethanol solution to the filter residue obtained in the step (1), propane diols 8
Part, at 75 DEG C, be heated to reflux alcohol extracting 2 it is small when, with obtained after 600 mesh filter-cloth filterings filter residue 2. with alcohol extract 2.;
(3) by the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 35 parts
When, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, it is named as self-control A and carries
Take liquid;
(4) filter residue obtained in the step (2) 2. 350 parts of deionized waters of middle addition, are heated to seething with excitement, and be maintained at micro-
Boiling state boil 0.8 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5) obtained by the step (4) filter residue 3. in add 280 parts of deionized water, be heated to seething with excitement, and in slight boiling condition
Boil 0.5 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6) by Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng,
Water evaporation quantity is controlled, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed.
The preparation method for making C extracting solutions in the present embodiment by oneself comprises the following steps:
(1) 8 parts of radix glycyrrhizae, 4 parts of wild soybean seed, 5 parts of oat kernel, each 4 parts of tree peony root, althaea root, cordate houttuynia, print are weighed
Chinaberry leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, each 1 part of purslane are spent, by these
The larger coarse crushing of partial block, leaf is into being added to enamel Chinese medicine extracting tank after the≤segment of 3cm or the small pieces of diameter≤3cm in medicine
In;
(2) when boiling for the first time, weigh 680 parts of deionized water and add in enamel Chinese medicine extracting tank, immersion adds after 30 minutes
Heat to seethe with excitement, and be maintained at slight boiling condition boil 1.0 it is small when, then carry filter residue up to water with 600 mesh filter-cloth filterings and 1. carried with water
Liquid is 1. ';
(3) 580 parts of deionized water is added in 1. water made from step (2) carries filter residue, is heated to seething with excitement, and keep
Slight boiling condition boil 0.6 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 2. with Aqueous extracts 2. ';
(4) by above-mentioned Aqueous extracts 1. ', Aqueous extracts are 2. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, control moisture evaporation
Amount, makes finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself.
The preparation method for making D extracting solutions in the present embodiment by oneself comprises the following steps:(1) filter residue 2. middle addition is proposed in the water
6 parts of sucrose, 3 parts of glucose, 0.3 part of dipotassium hydrogen phosphate, 0.2 part of sodium chloride, 350 parts of pure water, is heated to seething with excitement, constant temperature disinfection
20 minutes, 33 DEG C are then cooled to, adds 90 parts of self-control C extracting solutions, (2) and then 3% inoculum concentration by fermentation bottom material total amount
Access expands the Aureobasidium pullulans strain after culture, and (strain is purchased from Chinese industrial Culture Collection, bacterium numbering:
CICC41349), after fermentation culture for 2 days, adding 1% Pichia pastoris strain of fermentation bottom material total amount, (strain is purchased from Chinese work
Industry Culture Collection, bacterium numbering:CICC33024) and fermentation bottom material total amount 3% lactobacillus plantarum strain
((strain is purchased from Chinese industrial Culture Collection, bacterium numbering:CICC6240)), fermented and cultured is continued 3 days, then
System temperature is dropped to 29 DEG C again, self-control B extracting solutions and filter residue is added 4. after continuing fermentation 2 days, continues fermentation 3 days, take
Zymotic fluid examines thalline sum, then continues fermentation if more than 500CFU/ML 5 days or with ozone sterilization system for handling, until system
Middle viable bacteria body is depleted, until zymotic fluid, is then crossed 600 mesh filter clothes and filtered out by thalline sum≤500CFU/ML in system,
(3) and then below 50 DEG C the 1/2 of total fermentation filtrate volume is concentrated in vacuo to, the concentrate of fermentation extracting solution is made, i.e., certainly
D extracting solutions processed.
The present embodiment wormwood face cream, substitutes the pure water component in wormwood face cream, by following heavy with obtained C extracting solutions
The component of amount part is made:
(1) oil phase component:The oil phase component is made of following components in parts by weight:16 1 part of mixed alcohols, 16
3 parts of 4 parts of stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearates, jojoba oil
3 parts, 2 parts of isomery hexadecane hydrocarbon, 2 parts of seed of Flos Camelliae Japonicae oil, 1 part of Purple Perilla Seed Oil, 1 part of isopropyl myristate, dimethicone 2
Part, 0.2 part of methyl hydroxybenzoate, 0.15 part of propylben, 0.03 part of di-tert-butyl p-cresol;
(2) water phase components:The water phase components are made of following components in parts by weight:7 parts of glycerine, modified corn syrup
(commodity English name:MOISYRUP, is provided by Shanghai Shun Tuo scientific & trading Co., Ltd.s) 2 parts, 2 parts of trehalose, trimethylglycine 2
Part, 55 parts of self-control C extracting solutions;
(3) extracting solution component:Make 2 parts of A extracting solutions, 10 parts of self-control D extracting solutions by oneself;
(4) assistant for emulsifying agent component:0.5 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5) preservative:The mixture of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.1 part;
(6) essence:0.02 part of floral perfume.
The preparation method of the present embodiment wormwood face cream, includes the following steps:
(1) preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecanes
Base glucoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple
After perilla oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol weigh in proportion
Add in the stainless steel kettle of band stirring, dissolved by heating completely under the stirring of 25 revs/min of rotating speed, and the constant temperature disinfection 20 at 85 DEG C
Minute is stand-by;
(2) preparation of water phase components:By the glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, from
C extracting solutions processed first dissolve by heating after weighing in proportion in stainless steel kettle, are then extracted into stainless steel homogeneous kettle, at 30 revs/min
Stirring under, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) oil phase is slowly pumped into water phase, and carries out scraping wall stirring, 3 points are stirred in the case where scraping wall rotating speed as 45 revs/min
Clock, starts high speed homogenization device homogeneous 5 minutes under 3000 revs/min of high speed, will scrape wall rotating speed afterwards and drop to 40 revs/min, and
50 DEG C are cooled under this rotating speed;
(4) and then the self-control A extracting solutions of formula ratio is added and make D extracting solutions and assistant for emulsifying agent by oneself, in 30 revs/min of rotating speed
Lower stirring 20 minutes, continues to cool to 40 DEG C afterwards, adds the preservative and essence of formula ratio, continue to stir under same rotating speed
Mix 20 minutes, you can discharging, is made wormwood face cream.
Embodiment 4
The preparation method for making A extracting solutions in the present embodiment by oneself comprises the following steps:
(1) Mao Pus, scutellariae,radix, kuh-seng coarse powder are broken into≤segment of 3cm or the small pieces of diameter≤3cm, weigh wormwood 5
Part, 3 parts of grass-leaved sweetflag, scutellariae,radix, each 6 parts of kuh-seng, 10 parts of propane diols, volumetric concentration is 60% 600 parts of ethanol solution, at 70 DEG C
Under, be heated to reflux alcohol extracting 1 it is small when, with respectively obtained after 600 mesh filter-cloth filterings filter residue 1. with alcohol extract 1.;
(2) 1. middle addition volumetric concentration is 500 parts of 60% ethanol solution to the filter residue obtained in the step (1), propane diols 5
Part, at 70 DEG C, be heated to reflux alcohol extracting 3 it is small when, with obtained after 600 mesh filter-cloth filterings filter residue 2. with alcohol extract 2.;
(3) by the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 50 parts
When, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, it is named as self-control A and carries
Take liquid;
(4) filter residue obtained in the step (2) 2. 300 parts of deionized waters of middle addition, are heated to seething with excitement, and be maintained at micro-
Boiling state boil 0.9 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5) obtained by the step (4) filter residue 3. in add 300 parts of deionized water, be heated to seething with excitement, and in slight boiling condition
Boil 0.8 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6) by Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng,
Water evaporation quantity is controlled, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed.
The preparation method for making C extracting solutions in the present embodiment by oneself comprises the following steps:
(1) 10 parts of radix glycyrrhizae is weighed, 5 parts of wild soybean seed, 4 parts of oat kernel, each 4 parts of tree peony root, althaea root, cordate houttuynia,
Each 2 parts of azadirachta leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, purslane, by these
The larger coarse crushing of partial block, leaf is into being added to enamel traditional Chinese medicine extraction after the≤segment of 3cm or the small pieces of diameter≤3cm in Chinese medicine
In tank;
(2) when boiling for the first time, weigh 700 parts of deionized water and add in enamel Chinese medicine extracting tank, immersion adds after 30 minutes
Heat to seethe with excitement, and be maintained at slight boiling condition boil 0.8 it is small when, then carry filter residue up to water with 600 mesh filter-cloth filterings and 1. carried with water
Liquid is 1. ';
(3) 500 parts of deionized water is added in 1. water made from step (2) carries filter residue, is heated to seething with excitement, and keep
Slight boiling condition boil 0.8 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 2. with Aqueous extracts 2. ';
(4) by above-mentioned Aqueous extracts 1. ', Aqueous extracts are 2. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, control moisture evaporation
Amount, makes finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself.
The preparation method for making D extracting solutions in the present embodiment by oneself comprises the following steps:(1) filter residue 2. middle addition is proposed in the water
5 parts of sucrose, 4 parts of glucose, 0.4 part of dipotassium hydrogen phosphate, 0.1 part of sodium chloride, 300 parts of pure water, is heated to seething with excitement, constant temperature disinfection
20 minutes, 30 DEG C are then cooled to, adds 50 parts of self-control C extracting solutions, (2) and then 2% inoculum concentration by fermentation bottom material total amount
Access expands the Aureobasidium pullulans strain after culture, and (strain is purchased from Chinese industrial Culture Collection, bacterium numbering:
CICC41349), after fermentation culture for 1 days, adding 2% Pichia pastoris strain of fermentation bottom material total amount, (strain is purchased from Chinese work
Industry Culture Collection, bacterium numbering:CICC33024) and fermentation bottom material total amount 1% lactobacillus plantarum strain
((strain is purchased from Chinese industrial Culture Collection, bacterium numbering:CICC6240)), fermented and cultured is continued 1 day, then
System temperature is dropped to 28 DEG C again, self-control B extracting solutions and filter residue is added 4. after continuing fermentation 1 day, continues fermentation 2 days, take
Zymotic fluid examines thalline sum, then continues fermentation if more than 500CFU/ML 3 days or with ozone sterilization system for handling, until system
Middle viable bacteria body is depleted, until zymotic fluid, is then crossed 600 mesh filter clothes and filtered out by thalline sum≤500CFU/ML in system,
(3) and then below 50 DEG C the 1/2 of total fermentation filtrate volume is concentrated in vacuo to, the concentrate of fermentation extracting solution is made, i.e., certainly
D extracting solutions processed.
The present embodiment wormwood face cream, is made of the component of following parts by weight:
(1) oil phase component:The oil phase component is made of following components in parts by weight:16 1.2 parts of mixed alcohols, ten
2 parts of 2 parts of six stearyl alcohols and 16 octadecyl glucosides, tristerin and PEG-100 stearates, Jojoba
2 parts of oil, 2 parts of isomery hexadecane hydrocarbon, 1 part of seed of Flos Camelliae Japonicae oil, 1 part of Purple Perilla Seed Oil, 1 part of isopropyl myristate, dimethicone 2
Part, 0.2 part of methyl hydroxybenzoate, 0.1 part of propylben, 0.05 part of di-tert-butyl p-cresol;
(2) water phase components:The water phase components are made of following components in parts by weight:5 parts of glycerine, modified corn syrup
(commodity English name:MOISYRUP, is provided by Shanghai Shun Tuo scientific & trading Co., Ltd.s) 2 parts, 1 part of trehalose, trimethylglycine 2
Part, 40 parts of self-control C extracting solutions;
(3) extracting solution component:Make 2 parts of A extracting solutions, 5 parts of self-control D extracting solutions by oneself;
(4) assistant for emulsifying agent component:1 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5) preservative:The mixture of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.15 part;
(6) essence:0.01 part of floral perfume.
The preparation method of the present embodiment wormwood face cream, includes the following steps:
(1) preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecanes
Base glucoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple
After perilla oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol weigh in proportion
Add in the stainless steel kettle of band stirring, dissolved by heating completely under the stirring of 20 revs/min of rotating speed, and the constant temperature disinfection 20 at 80 DEG C
Minute is stand-by;
(2) preparation of water phase components:By the glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, from
C extracting solutions processed first dissolve by heating after weighing in proportion in stainless steel kettle, are then extracted into stainless steel homogeneous kettle, at 20 revs/min
Stirring under, continue to be heated to 80 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) oil phase is slowly pumped into water phase, and carries out scraping wall stirring, 2 points are stirred in the case where scraping wall rotating speed as 40 revs/min
Clock, starts high speed homogenization device homogeneous 4 minutes under 3500 revs/min of high speed, will scrape wall rotating speed afterwards and drop to 30 revs/min, and
47 DEG C are cooled under this rotating speed;
(4) and then the self-control A extracting solutions of formula ratio is added and make D extracting solutions and assistant for emulsifying agent by oneself, in 20 revs/min of rotating speed
Lower stirring 25 minutes, continues to cool to 40 DEG C afterwards, adds the preservative and essence of formula ratio, continue to stir under same rotating speed
Mix 15 minutes, you can discharging, is made wormwood face cream.
Claims (2)
1. a kind of wormwood face cream, it is characterised in that be made of the component of following parts by weight:
(1)Oil phase component:The oil phase component is made of following components in parts by weight:16 1~1.5 part of mixed alcohols, ten
Six stearyl alcohols and 2~4 parts of 16 octadecyl glucosides, tristerin and PEG-100 stearates 2~3
Part, 2~4 parts of jojoba oil, 2~4 parts of isomery hexadecane hydrocarbon, 1~3 part of seed of Flos Camelliae Japonicae oil, 1~2 part of Purple Perilla Seed Oil, myristic acid
1~3 part of isopropyl ester, 2~4 parts of dimethicone, 0.2~0.3 part of methyl hydroxybenzoate, 0.1~0.15 part of propylben, two uncles
0.03~0.05 part of butyl paracresol;
(2)Water phase components:The water phase components are made of following components in parts by weight:5~8 parts of glycerine, modified corn syrup 2
~4 parts, 1~2 part of trehalose, 2~4 parts of trimethylglycine, 40~60 parts of self-control C extracting solutions, the self-control C extracting solutions are under
The raw material of row parts by weight is made:5~10 parts of radix glycyrrhizae, 3~5 parts of wild soybean seed, 4~5 parts of oat kernel, tree peony root, althaea root,
Each 3~4 parts of cordate houttuynia, azadirachta leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, horse
Each 1~3 part of bitterroot;
(3)Extracting solution component:Make 2~4 parts of A extracting solutions, 5~10 parts of self-control D extracting solutions by oneself;
(4)Assistant for emulsifying agent component:0.5~1 part of hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers;
(5)Preservative:The mixture 0.1- of 2-methyl-4-isothiazolin-3-one and the iodo- 2-propynyl butyl carbamates of 3-
0.15 part;
(6)Essence:0.01-0.02 parts of floral perfume;
The preparation method of the self-control A extracting solutions comprises the following steps:
(1)5~8 parts of wormwood is weighed, 3~6 parts of grass-leaved sweetflag, scutellariae,radix, each 4~6 parts of kuh-seng, 10~15 parts of propane diols, volume is dense
Spend 600~700 parts of the ethanol solution for 60%~80%, at 70~90 DEG C, be heated to reflux alcohol extracting 1~3 it is small when, with 600 mesh
Respectively obtained after filter-cloth filtering filter residue 1. with alcohol extract 1.;
(2)In the step(1)1. middle addition volumetric concentration is 500~600 parts of 60%~80% ethanol solution to obtained filter residue,
5~10 parts of propane diols, at 70~90 DEG C, be heated to reflux alcohol extracting 1~3 it is small when, with obtained after 600 mesh filter-cloth filterings filter residue 2. and
Alcohol extract is 2.;
(3)By the alcohol extract 1., alcohol extract heat concentration and recovery ethanol after 2. merging, liquid to be mixed is concentrated to 30~50 parts
When, up to the concentrate of wormwood, grass-leaved sweetflag, scutellariae,radix, the ethanol of kuh-seng and propane diols extracting solution is made by oneself, it is named as self-control A and carries
Take liquid;
(4)In the step(2)Obtained filter residue is 2. middle to add 300~400 parts of deionized waters, is heated to seething with excitement, and be maintained at
Slight boiling condition boil 0.8~1.0 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 3. with Aqueous extracts 1.;
(5)In step(4)Gained filter residue 3. in add 200~300 parts of deionized water, be heated to seething with excitement, and in slightly boiling shape
State boil 0.5~0.8 it is small when, then with 600 mesh filter-cloth filterings up to filter residue 4. and Aqueous extracts 2.;
(6)By Aqueous extracts 1., Aqueous extracts 2. merge after up to self-control wormwood, grass-leaved sweetflag, scutellariae,radix, the Aqueous extracts of kuh-seng, control
Water evaporation quantity, it is add total Water 1/3 to make finally to concentrate molding Aqueous extracts total amount, derived from B extracting solutions processed;
The preparation method of the self-control C extracting solutions comprises the following steps:
(1)5~10 parts of radix glycyrrhizae is weighed, 3~5 parts of wild soybean seed, 4~5 parts of oat kernel, tree peony root, althaea root, cordate houttuynia are each
3~4 parts, azadirachta leaf, Sakura leaf, gynostemma pentaphyllum leaf, very thin geranium wilfordii, corn flower, dandelion, saururus chinensis, purslane each 1~
3 parts, it is added in enamel Chinese medicine extracting tank;
(2)When boiling for the first time, weigh 600~700 parts of deionized water and add in enamel Chinese medicine extracting tank, immersion adds after 30 minutes
Heat to seethe with excitement, and be maintained at slight boiling condition boil 0.8~1.0 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 1. and
Aqueous extracts are 1. ';
(3)In step(2)Obtained water adds 500~600 parts of deionized water in carrying filter residue 1., be heated to seething with excitement, and protect
Hold slight boiling condition boil 0.6~0.8 it is small when, then with 600 mesh filter-cloth filterings up to water carry filter residue 2. with Aqueous extracts 2. ';
(4)', Aqueous extracts are 2. by above-mentioned Aqueous extracts 1. ' after mixing up to homemade traditional Chinese drug Aqueous extracts, moisture evaporation amount is controlled,
Make finally to concentrate molding Aqueous extracts total amount to add the half of water, up to C extracting solutions are made by oneself;
The preparation method of the self-control D extracting solutions comprises the following steps:(1)Filter residue 2. middle 5~8 parts of sucrose of addition, Portugal are carried in water
3~5 parts of grape sugar, 0.3~0.5 part of dipotassium hydrogen phosphate, 0.1~0.2 part of sodium chloride, 300~400 parts of pure water, is heated to seething with excitement,
Constant temperature disinfection 20 minutes, is then cooled to 30~35 DEG C, adds 50~100 parts of self-control C extracting solutions,(2)Then by fermentation bottom material
2~3% inoculum concentration access of total amount expands the Aureobasidium pullulans strain after culture, and fermented and cultured adds hair after 1~3 day
1~2% Pichia pastoris strain of ferment bottom material total amount and 1~3% lactobacillus plantarum strain of fermentation bottom material total amount, after supervention
System temperature, is then dropped to 28~30 DEG C by ferment culture 1~3 day again, and self-control B extracting solutions are added after continuing fermentation 1~2 day
And filter residue is 4., continue fermentation 2~3 days, until zymotic fluid, is then crossed 600 mesh filter clothes by thalline sum≤500CFU/ML in system
Filter out,(3)Then the 1/2 of total fermentation filtrate volume is concentrated in vacuo to below 50 DEG C, the concentrate of fermentation extracting solution is made,
Make D extracting solutions by oneself.
2. the preparation method of the wormwood face cream described in claim 1, it is characterised in that include the following steps:
(1)The preparation of oil phase component:By 16 mixed alcohols of formula ratio, 16 stearyl alcohols and 16 octadecyl Portugals
Polyglycoside, tristerin and PEG-100 stearates, jojoba oil, isomery hexadecane hydrocarbon, seed of Flos Camelliae Japonicae oil, purple perilla seed
Oil, nutmeg propyl ester, dimethicone, methyl hydroxybenzoate, propylben, di-tert-butyl p-cresol add after weighing in proportion
In stainless steel kettle with stirring, dissolved by heating under the stirring of 20~30 revs/min of rotating speed complete, and constant temperature disappears at 80~85 DEG C
Malicious 20 minutes stand-by;
(2)The preparation of water phase components:The glycerine of formula ratio, modified corn syrup, trehalose, trimethylglycine, self-control C are carried
Take liquid first to be dissolved by heating after weighing in proportion in stainless steel kettle, be then extracted into stainless steel homogeneous kettle, at 20~30 revs/min
Under stirring, continue to be heated to 80~85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3)Oil phase is pumped into water phase, and carries out scraping wall stirring, stirs 2-3 minutes, opens in the case where scraping wall rotating speed as 40-50 revs/min
Dynamic high speed homogenization device will scrape wall rotating speed and drop to 30-40 revs/min afterwards homogeneous 3-5 minutes under 3000-5000 revs/min of high speed,
And it is cooled to 45-50 DEG C under this rotating speed;
(4)Then the self-control A extracting solutions and self-control D extracting solutions and assistant for emulsifying agent of formula ratio are added, in 20-30 revs/min of rotating speed
Lower stirring 20-30 minutes, continues to cool to 40 DEG C afterwards, adds the preservative and essence of formula ratio, continues in same rotating speed
Lower stirring 15-20 minutes, you can discharging, is made wormwood face cream.
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CN104083317A (en) * | 2014-06-27 | 2014-10-08 | 郑州市嘉蓓丽生物科技有限公司 | White bud tea eye care cream and preparation method thereof |
CN104306319A (en) * | 2014-10-30 | 2015-01-28 | 郑州市嘉蓓丽生物科技有限公司 | Ghee whitening skin cream and preparation method thereof |
CN104622783A (en) * | 2015-02-10 | 2015-05-20 | 济南康众医药科技开发有限公司 | Traditional Chinese medicine bioproduct for treating pimples |
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CN101565694A (en) * | 2008-04-25 | 2009-10-28 | 天津天士力制药股份有限公司 | Salvianolic acid enzyme and mixed enzyme of same and ginsenoside and method for converting same into medicinal materials |
CN104083317A (en) * | 2014-06-27 | 2014-10-08 | 郑州市嘉蓓丽生物科技有限公司 | White bud tea eye care cream and preparation method thereof |
CN104306319A (en) * | 2014-10-30 | 2015-01-28 | 郑州市嘉蓓丽生物科技有限公司 | Ghee whitening skin cream and preparation method thereof |
CN104622783A (en) * | 2015-02-10 | 2015-05-20 | 济南康众医药科技开发有限公司 | Traditional Chinese medicine bioproduct for treating pimples |
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