CN104862127A - Traditional Chinese medicine environment-friendly tableware detergent - Google Patents

Traditional Chinese medicine environment-friendly tableware detergent Download PDF

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Publication number
CN104862127A
CN104862127A CN201510279656.6A CN201510279656A CN104862127A CN 104862127 A CN104862127 A CN 104862127A CN 201510279656 A CN201510279656 A CN 201510279656A CN 104862127 A CN104862127 A CN 104862127A
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parts
extract
traditional medicine
chinese traditional
detergent
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CN201510279656.6A
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Chinese (zh)
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徐再
徐凯
赵维达
赵云龙
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Five Lakes New Material Technology Development Corp Ltd Of Zhangjagang City
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Five Lakes New Material Technology Development Corp Ltd Of Zhangjagang City
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Abstract

The invention relates to the technical field of daily chemical articles for use, particularly to a traditional Chinese medicine environment-friendly tableware detergent. The detergent comprises the following components in parts by weight: 10-30 parts of a Chinese honey locust extract, 8-15 parts of a wild argy wormwood leaf extract, 6-12 parts of a bletilla striata extract, 0.8-2.4 parts of a nanometer deoiling emulsifying agent, 1.2-3.6 parts of a fineleaf schizonepeta herb extract, 1.2-4.8 parts of a vanilla extract, 0.2-0.8 part of a biological composite enzyme and 0.2-0.6 part of a composite stabilizer. The detergent disclosed by the invention has the benefits that substances, extracted from natural plant traditional Chinese medicines, with active components are added to the total composition of the detergent, so that the growth of bacteria and molds on clothings can be inhibited, besides, the irritant of the detergent is reduced, the damage and the decomposition of cloths are not easy to cause, the condition that the skins are stimulated due to the remain of chemical preservatives on the clothings can be avoided, and the detergent is safe and reliable to use and is simple to make.

Description

A kind of Chinese traditional medicine environment-friendlytableware tableware detergent
Technical field
The present invention relates to cosmetics of everyday use technical field, especially a kind of Chinese traditional medicine environment-friendlytableware tableware detergent.
Background technology
Conventional cutlery washing composition is synthetic detergent, mainly adopts sodium lauryl sulphate, Sodium dodecylbenzene sulfonate etc. as tensio-active agent, other thickening materials, silver-colored optical brightener, emulsifying agent and pore forming material.
Tensio-active agent in dish washing detergent can infiltrate human body, and the washing composition nearly 0.5% sticked on skin infiltrates blood, if skin has wound, seepage force improves more than 10 times.The soapless soap entered in human body can make calcium ion concn in blood decline, and acidification of blood, people is easily tired.These toxin also make the functions of expelling toxin of liver reduce.Originally this toxin alluvial excreted is taken care of the pence in vivo, and make people's immunity degradation, liver cell lesion aggravates, and easily brings out cancer.
After dish washing detergent cleaning, on the bowls and chopsticks tableware do not used for a long time, accumulating the material of one deck yellow, is exactly the residue of washing composition.They can be dissolved among we of edible food more than 30 DEG C every day.It is reported have people to buy 9 kinds of dish washing detergents in the market and do experiment, after tableware detergent washing utensil, then rush 12 times tap water, on average still have the residual substance of 0.03% to leave over.Life-time service, the objectionable impurities of dish washing detergent will take care of the pence, and causes serious threat to health.
Summary of the invention
The object of the invention is: overcome deficiency of the prior art, a kind of environmental protection is provided, to human body and environmentally friendly, and also washes clean, not easily residual Chinese traditional medicine environment-friendlytableware tableware detergent.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is as follows:
A kind of Chinese traditional medicine environment-friendlytableware tableware detergent, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 10-30 part, wild Folium Artemisiae Argyi extract 8-15 part, bletilla striata extract 6-12 part, nanometer are except emulsifier 0.8-2.4 part, Herba Schizonepetae extract 1.2-3.6 part, vanilla extract 1.2-4.8 part, compound bio-enzyme 0.2-0.8 part, one package stabilizer 0.2-0.6 part.
Further, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 3-4 time, ethanol consumption is 8-12ml/g raw material, extraction time is 1-3h, filters, and merges alcohol extract, being evaporated to relative density is 1.25-1.32, then go up adsorption resin column, use 20% successively, 40%, 60%DE ethanol elution, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.
Further, have diatomite layer above described adsorption resin column, the thickness of described diatomite layer is 4-8cm.
Further, described ethanol consumption is 10ml/g raw material, and extraction time is 2h.
Further, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverizes tarragon and crosses 100 mesh sieves, soak by 2.5-4.5L ethyl acetate, 30-40min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
Further, described compound bio-enzyme selects one or more in alkaline pectase, amylase and proteolytic enzyme.
Further, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 1-5 part, calcium chloride 0.8-3.6 part, nonionogenic tenside 5-15 part, propylene glycol 1-10 part.
Further, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 3 parts, 2.4 parts, calcium chloride, nonionogenic tenside 10 parts, propylene glycol 6 parts.
Further, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 20 parts, wild Folium Artemisiae Argyi extract 12 parts, bletilla striata extract 9 parts, nanometer are except emulsifier 1.6 parts, Herba Schizonepetae extract 2.4 parts, vanilla extract 3 parts, compound bio-enzyme 0.5 part, one package stabilizer 0.4 part.
Further, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 18 parts, wild Folium Artemisiae Argyi extract 10 parts, bletilla striata extract 8 parts, nanometer are except emulsifier 1.8 parts, Herba Schizonepetae extract 2.5 parts, vanilla extract 3.6 parts, compound bio-enzyme 0.6 part, one package stabilizer 0.5 part.
The Advantageous Effects of technical scheme of the present invention is adopted to be: what add in washing composition total composition is the material with activeconstituents proposed from the Chinese medicine of natural phant, not only enough suppress clothing growth bacterium and mould, reduce the pungency of washing composition simultaneously, not easily cause the breakage of clothing, rot and chemical residue sanitas and skin irritation; Safe and reliable, simple for production.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described.
Embodiment 1
A kind of Chinese traditional medicine environment-friendlytableware tableware detergent, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 10 parts, wild Folium Artemisiae Argyi extract 8 parts, bletilla striata extract 6 parts, nanometer are except emulsifier 0.8 part, Herba Schizonepetae extract 1.2 parts, vanilla extract 1.2 parts, compound bio-enzyme 0.2 part, one package stabilizer 0.2 part.
Preferably, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 3 times, ethanol consumption is 12ml/g raw material, extraction time is 1h, filters, and merges alcohol extract, being evaporated to relative density is 1.25, then go up adsorption resin column, use the ethanol elution of 20%, 40%, 60% successively, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.Have diatomite layer above adsorption resin column, the thickness of described diatomite layer is 4cm.
Preferably, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverizes tarragon and crosses 100 mesh sieves, soak by 2.5L ethyl acetate, 40min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
Preferably, described compound bio-enzyme selects alkaline pectase.
Preferably, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 1 part, 0.8 part, calcium chloride, nonionogenic tenside 5 parts, propylene glycol 1 part.
Embodiment 2
A kind of Chinese traditional medicine environment-friendlytableware tableware detergent, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 20 parts, wild Folium Artemisiae Argyi extract 12 parts, bletilla striata extract 9 parts, nanometer are except emulsifier 1.6 parts, Herba Schizonepetae extract 2.4 parts, vanilla extract 3 parts, compound bio-enzyme 0.5 part, one package stabilizer 0.4 part.
Preferably, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 4 times, ethanol consumption is 10ml/g raw material, extraction time is 2h, filters, and merges alcohol extract, being evaporated to relative density is 1.28, then go up adsorption resin column, use the ethanol elution of 20%, 40%, 60% successively, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.Have diatomite layer above adsorption resin column, the thickness of described diatomite layer is 6cm.
Preferably, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverizes tarragon and crosses 100 mesh sieves, soak by 3.5L ethyl acetate, 35min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
Preferably, described compound bio-enzyme selects alkaline pectase and amylase.
Preferably, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 3 parts, 2.4 parts, calcium chloride, nonionogenic tenside 10 parts, propylene glycol 6 parts.
Embodiment 3
A kind of Chinese traditional medicine environment-friendlytableware tableware detergent, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 18 parts, wild Folium Artemisiae Argyi extract 10 parts, bletilla striata extract 8 parts, nanometer are except emulsifier 1.8 parts, Herba Schizonepetae extract 2.5 parts, vanilla extract 3.6 parts, compound bio-enzyme 0.6 part, one package stabilizer 0.5 part.
Preferably, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 4 times, ethanol consumption is 8ml/g raw material, extraction time is 3h, filters, and merges alcohol extract, being evaporated to relative density is 1.32, then go up adsorption resin column, use the ethanol elution of 20%, 40%, 60% successively, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.Have diatomite layer above adsorption resin column, the thickness of described diatomite layer is 8cm.
Preferably, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverizes tarragon and crosses 100 mesh sieves, soak by 4.5L ethyl acetate, 30min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
Preferably, described compound bio-enzyme selects alkaline pectase, amylase and proteolytic enzyme.
Preferably, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 3 parts, 2.4 parts, calcium chloride, nonionogenic tenside 10 parts, propylene glycol 6 parts.
Embodiment 4
A kind of Chinese traditional medicine environment-friendlytableware tableware detergent, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 30 parts, wild Folium Artemisiae Argyi extract 15 parts, bletilla striata extract 12 parts, nanometer are except emulsifier 2.4 parts, Herba Schizonepetae extract 3.6 parts, vanilla extract 4.8 parts, compound bio-enzyme 0.8 part, one package stabilizer 0.6 part.
Preferably, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 4 times, ethanol consumption is 12ml/g raw material, extraction time is 2h, filters, and merges alcohol extract, being evaporated to relative density is 1.32, then go up adsorption resin column, use the ethanol elution of 20%, 40%, 60% successively, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.Have diatomite layer above adsorption resin column, the thickness of described diatomite layer is 4cm.
Preferably, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverizes tarragon and crosses 100 mesh sieves, soak by 2.5L ethyl acetate, 40min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
Preferably, described compound bio-enzyme selects alkaline pectase, amylase and proteolytic enzyme.
Preferably, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 5 parts, 3.6 parts, calcium chloride, nonionogenic tenside 15 parts, propylene glycol 10 parts.
Embodiment 3 is preferred embodiment.
Experiment:
Surface tension is tested:
Capillary rise method is adopted to measure the surface tension of solution.A clean kapillary is vertically inserted in the testing liquid surface that can be soaked, liquid will rise in kapillary, until intraluminal fluid face is higher than the outer liquid level of pipe and liquid level is spill.The height that liquid level rises is directly proportional in the surface tension of liquid.Measure foam height by Ross-Miles method and surely steep the time.
Table 1 is Fructus Gleditsia extract, nanometer removes emulsifier, wild Folium Artemisiae Argyi extract and other chemical active agent Performance comparision, and strength of solution is 0.5%, experiment condition: 20 DEG C, 1atm
Promoting agent title Interfacial tension (mN/m) Foam height (ml/50ml) Steady bubble time (s)
Distilled water 73.25 0 0
Sodium laurylsulfonate 35.14 172 365
Sodium dodecylbenzene sulfonate 38.12 182 375
Fructus Gleditsia extract 44.25 126 468
Nanometer is except emulsifier 44.18 123 464
Wild Folium Artemisiae Argyi extract 43.98 124 465
As shown in Table 1, Fructus Gleditsia extract, nanometer except emulsifier, wild Folium Artemisiae Argyi extract solution surface tension be starkly lower than distilled water.Under equal conditions, Fructus Gleditsia extract, nanometer remove emulsifier, wild Folium Artemisiae Argyi extract solution reduces capillary close with the ability of sodium laurylsulfonate, Sodium dodecylbenzene sulfonate, but activity is more weak, but be added with compound bio-enzyme and one package stabilizer in formula of the present invention, make the stability of washing composition of the present invention, surely steep time lengthening, so Fructus Gleditsia extract, nanometer remove emulsifier and wild Folium Artemisiae Argyi extract can use as the decontamination composition of dish washing detergent.
Bactericidal property is tested:
In daily life, streptococcus aureus, intestinal bacteria, dysentery bacterium are modal pathogenic bacterium.Adopt By Dilution bletilla striata extract and Herba Schizonepetae extract to the minimum inhibitory concentration (MIC) of these three kinds of bacteriums and minimum bactericidal concentration (MBC), thus confirm the bactericidal property of bletilla striata extract and Herba Schizonepetae extract.
First coat General nutrition agar plate, at 37 DEG C of constant temperature culture 24h by each for examination bacterial classification.Get a platinum ear lawn to be inoculated in the phenol red meat soup culture tube of glucose, at 37 DEG C of constant temperature culture 12h, determine bacterium amount by turbidimetry, then use broth dilution, make its bacteria containing amount be about 10-3CFU/ml, as supplying examination bacterium suspension.Chlorogenic acid powder is dissolved in distilled water, makes chlorogenic acid extracting solution.Adopt two-fold dilution's method to be diluted to various concentration, every concentration makees 2 parallel pipes, and each pipe adds respectively for examination bacteria suspension 0.1ml, and mixing, puts into incubator, 37 DEG C of constant temperature culture 24h, observes cultivation results.The nutrient solution transferred species of getting in the MIC negative tube of above-mentioned observation is coated on ordinary nutrient agar plate plate, 37 DEG C of constant temperature culture 18 ~ 24h, observed and recorded colony number.Colony number be less than 3 or the minimum concentration of asepsis growth be the minimum bactericidal concentration (MBC) of Japanese Honeysuckle.
The minimum inhibitory concentration (MIC) of table 2 bletilla striata extract and Herba Schizonepetae extract and minimum bactericidal concentration (MBC) (mg/ml)
Bacterial strain MIC MBC
Streptococcus aureus 22 46
Intestinal bacteria - -
Dysentery bacterium 45 95
Detersive power measures:
The detersive power of embodiment 1-4 is respectively: 78.8%, 83.8%, 82.8%, 81.5%.
By national standard preparation standard dish washing detergent, and do detersive power mensuration, deoil rate is 58.6%.Specify in national standard, if the deoil rate of tested dish washing detergent is not less than the deoil rate of standard wash agent, then the detersive power of this dish washing detergent is judged to qualified, otherwise is defective.It is qualified that formula in 4 embodiments in the present invention is.
According to technical requirements in GB9985-2000 annex, carry out performance evaluation to adopting the obtained finished product of optimum formula.
The performance test results of table 3 tableware detergent of the present invention.
The above is only the preferred embodiment of the present invention; be not limited to the present invention; should be understood that; for those skilled in the art; under the prerequisite not departing from the technology of the present invention principle; can also make some improvement and modification, these improve and modification also should be considered as protection scope of the present invention.

Claims (10)

1. a Chinese traditional medicine environment-friendlytableware tableware detergent, it is characterized in that, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 10-30 part, wild Folium Artemisiae Argyi extract 8-15 part, bletilla striata extract 6-12 part, nanometer are except emulsifier 0.8-2.4 part, Herba Schizonepetae extract 1.2-3.6 part, vanilla extract 1.2-4.8 part, compound bio-enzyme 0.2-0.8 part, one package stabilizer 0.2-0.6 part.
2. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, it is characterized in that, described Fructus Gleditsia extract adopts following methods to obtain: Chinese honey locust drying and crushing crosses 100 mesh sieves, the extraction using alcohol of employing 95% 3-4 time, ethanol consumption is 8-12ml/g raw material, extraction time is 1-3h, filter, merge alcohol extract, being evaporated to relative density is 1.25-1.32, then goes up adsorption resin column, use 20% successively, 40%, 60%DE ethanol elution, reclaim ethanol eluate concentrating under reduced pressure, vacuum-drying, obtains required Fructus Gleditsia extract.
3. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 2, is characterized in that, has diatomite layer above described adsorption resin column, and the thickness of described diatomite layer is 4-8cm.
4. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 2, is characterized in that, described ethanol consumption is 10ml/g raw material, and extraction time is 2h.
5. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, it is characterized in that, described wild Folium Artemisiae Argyi extract adopts following methods to obtain: get wild dry moxa leaf 0.5kg, pulverize tarragon and cross 100 mesh sieves, soak by 2.5-4.5L ethyl acetate, 30-40min is collected in backflow, leaves standstill to be cooled to room temperature and to filter, through vacuum-drying and get final product after gained liquid concentration.
6. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, is characterized in that, described compound bio-enzyme selects one or more in alkaline pectase, amylase and proteolytic enzyme.
7. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, is characterized in that, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 1-5 part, calcium chloride 0.8-3.6 part, nonionogenic tenside 5-15 part, propylene glycol 1-10 part.
8. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 7, is characterized in that, the mass parts of described one package stabilizer is composed as follows: cyclodextrin 3 parts, 2.4 parts, calcium chloride, nonionogenic tenside 10 parts, propylene glycol 6 parts.
9. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, it is characterized in that, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 20 parts, wild Folium Artemisiae Argyi extract 12 parts, bletilla striata extract 9 parts, nanometer are except emulsifier 1.6 parts, Herba Schizonepetae extract 2.4 parts, vanilla extract 3 parts, compound bio-enzyme 0.5 part, one package stabilizer 0.4 part.
10. a kind of Chinese traditional medicine environment-friendlytableware tableware detergent according to claim 1, it is characterized in that, the mass parts of described washing composition is composed as follows: Fructus Gleditsia extract 18 parts, wild Folium Artemisiae Argyi extract 10 parts, bletilla striata extract 8 parts, nanometer are except emulsifier 1.8 parts, Herba Schizonepetae extract 2.5 parts, vanilla extract 3.6 parts, compound bio-enzyme 0.6 part, one package stabilizer 0.5 part.
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Application publication date: 20150826