CN104861707A - Preparation formula and production method for ultramarine wheat straw dye - Google Patents

Preparation formula and production method for ultramarine wheat straw dye Download PDF

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Publication number
CN104861707A
CN104861707A CN201410062157.7A CN201410062157A CN104861707A CN 104861707 A CN104861707 A CN 104861707A CN 201410062157 A CN201410062157 A CN 201410062157A CN 104861707 A CN104861707 A CN 104861707A
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CN
China
Prior art keywords
wheat straw
ultramarine
raw material
parts
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410062157.7A
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Chinese (zh)
Inventor
马文侠
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Harbin Arts and Crafts Co Ltd
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Harbin Arts and Crafts Co Ltd
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Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201410062157.7A priority Critical patent/CN104861707A/en
Publication of CN104861707A publication Critical patent/CN104861707A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/007Straw
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Paper (AREA)

Abstract

A preparation formula and production method for an ultramarine wheat straw dye are provided; with isatis tinctoria, blueberry, hyacinth flower, Chinese gall, alumen, an iron ion compound solution and mineral water as main raw materials, the production method comprises the main technological processes of material selection, material cutting, drying, soaking, hot boiling, mixing, precipitating, dyeing and finished product obtaining. Provided are the preparation formula and the production method for the ultramarine wheat straw dye which is prepared from purely-natural plants, is purely natural, pollution-free, green and environmentally friendly and has no toxic or side effect to human bodies.

Description

A kind of formula and production method preparing ultramarine wheat straw dye
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing ultramarine wheat straw dye.
background technology:
in prior art, the method that the main raw material Wheat Straw making straw patchwork dyes ultramarine is had a variety of, but most dyestuff is chemical dye, the ultramarine dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed the natural plant dyestuff of ultramarine, not only color is pure for the ultramarine Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, harm that other poisonous and harmful chemical dye causes people's health in dye process processed that what degree was different solve.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing ultramarine wheat straw dye be mixed with natural plant that the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, woaded blue 25-40 part, blueberry 10-30 part, hyacinth 10-30 part, Turkey-galls 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing ultramarine wheat straw dye of the present invention is, wherein the weight proportion of various raw material is, woaded blue 25-35 part, blueberry 10-25 part, hyacinth 10-25 part, Turkey-galls 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing ultramarine wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: woaded blue 30 parts, blueberry 15 parts, hyacinth 15 parts, 8 parts, Turkey-galls, alum 8 parts, ferric ion compounds solution 7 parts, mineral water 60 parts.
above-mentioned each component is made the production method of ultramarine wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the woaded blue, blueberry, hyacinth, Turkey-galls, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure ultramarine cellulose solution; H, dyeing, the temperature of 100 liters of pure ultramarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb ultramarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to ultramarine Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing ultramarine wheat straw dye of the present invention is: woaded blue 25-40 part, blueberry 10-30 part, hyacinth 10-30 part, Turkey-galls 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing ultramarine wheat straw dye of the present invention is: woaded blue 25-35 part, blueberry 10-25 part, hyacinth 10-25 part, Turkey-galls 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing ultramarine wheat straw dye of the present invention is: woaded blue 30 parts, blueberry 15 parts, hyacinth 15 parts, 8 parts, Turkey-galls, alum 8 parts, ferric ion compounds solution 7 parts, mineral water 60 parts.
above-mentioned each component is made the production method of ultramarine wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the woaded blue, blueberry, hyacinth, Turkey-galls, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure ultramarine cellulose solution; H, dyeing, the temperature of 100 liters of pure ultramarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb ultramarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to ultramarine Wheat Straw finished product at room temperature.

Claims (4)

1. prepare the formula of ultramarine wheat straw dye for one kind, it is characterized in that: it is made up of the raw material of following weight proportioning, woaded blue 25-40 part, blueberry 10-30 part, hyacinth 10-30 part, Turkey-galls 5-15 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of ultramarine wheat straw dye for one kind, it is characterized in that: wherein the weight proportion of various raw material is, woaded blue 25-35 part, blueberry 10-25 part, hyacinth 10-25 part, Turkey-galls 5-10 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for ultramarine wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, woaded blue 30 parts, blueberry 15 parts, hyacinth 15 parts, 8 parts, Turkey-galls, alum 8 parts, ferric ion compounds solution 7 parts, mineral water 60 parts.
4. a kind of production method preparing ultramarine wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the woaded blue, blueberry, hyacinth, Turkey-galls, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, by the raw material selected except alum, ferric ion compounds solution, mineral water are cut into bulk respectively; C, oven dry, will be cut into block stock and be placed in stoving oven mummification respectively, temperature controls at 100-120 DEG C, 30 minutes time, makes evaporation raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure ultramarine cellulose solution; H, dyeing, the temperature of 100 liters of pure ultramarine cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb ultramarine cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to ultramarine Wheat Straw finished product at room temperature.
CN201410062157.7A 2014-02-22 2014-02-22 Preparation formula and production method for ultramarine wheat straw dye Pending CN104861707A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410062157.7A CN104861707A (en) 2014-02-22 2014-02-22 Preparation formula and production method for ultramarine wheat straw dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410062157.7A CN104861707A (en) 2014-02-22 2014-02-22 Preparation formula and production method for ultramarine wheat straw dye

Publications (1)

Publication Number Publication Date
CN104861707A true CN104861707A (en) 2015-08-26

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410062157.7A Pending CN104861707A (en) 2014-02-22 2014-02-22 Preparation formula and production method for ultramarine wheat straw dye

Country Status (1)

Country Link
CN (1) CN104861707A (en)

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Application publication date: 20150826