CN104861413A - Method for preparing decorative interior acoustic insulating material - Google Patents

Method for preparing decorative interior acoustic insulating material Download PDF

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Publication number
CN104861413A
CN104861413A CN201510310853.XA CN201510310853A CN104861413A CN 104861413 A CN104861413 A CN 104861413A CN 201510310853 A CN201510310853 A CN 201510310853A CN 104861413 A CN104861413 A CN 104861413A
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emulsion
preparation
solid content
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temperature
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CN104861413B (en
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李平兰
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Sanming City Mei Lai District Yin Yin Jue Bei Investment Management Partnership (limited Partnership)
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  • Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
  • Soundproofing, Sound Blocking, And Sound Damping (AREA)

Abstract

The invention relates to a method for preparing a decorative interior acoustic insulating material. The method comprises the following steps: (1) putting the nano-carbon black, silicon dioxide sol and an addition agent into a waterborne polyurethane emulsion, and ultrasonically processing to obtain a composite emulsion for use; (2) mixing the expanded vermiculite, magnesite and montmorillonoid with a silane coupling agent, grinding and dispersing for 2-2.5h, mixing the obtained materials with the other remaining materials, sufficiently stirring and performing melt extrusion and granulation in a twin-screw extruder at the temperature of 180-190 DEG C to obtain a modified mother granule; and (3) melting the modified mother granule in a screw extruder, ejecting the fused mass through a melt-blow die head spinneret orifice at the temperature of 230-250 DEG C, uniformly spraying the composite emulsion prepared by the step (1) to a silkscreen after the fiberyarns are collected to form a web on a receiving device, and obtaining the acoustic insulating non-woven material after the composite emulsion is fully cured and dried. By adopting the material, the specific surface area is large, the structure is more compact than that of the traditional non-woven material and the noise reduction effect is obvious.

Description

A kind of preparation method of interior sound insulation material of decorateing
Technical field
The present invention relates to a kind of non-woven sound absorbent material, be specifically related to the preparation method of a kind of interior trim expanded vermiculite of decorateing-non-woven sound absorbent material of conjunction emulsion coating thermoplastic phenolic resin.
Background technology
Now, along with the continuous acceleration of urbanization, noise pollution also becomes more and more serious.In order to effectively cut off noise, common settling mode uses sound-proof material.Existing sound-proof material is generally cement concrete, sheet glass etc., these sound insulations etc.The soundproof effect of these sound-proof materials is not very well, and therefore common terms of settlement strengthens the thickness of sound-proof material.The problem caused like this is that sound-proof material quality is overweight, high cost, and installation process is very inconvenient.
The polypropylene-base composite nonwoven material obtained with meltblown is with its ultra-fine fibrous texture, produce simple efficient, the feature such as nontoxic becomes the sound absorbent material of class widespread use in automotive trim, the most short texture of these materials, smooth fibrous outer reduces the specific surface area of material, thus sound wave oscillatory extinction transformation time is in the material shortened, do not reach gratifying sound-absorbing effect, noise reduction is promoted often through increase material thickness when reality uses, finished product exists yielding simultaneously, anti-rebound resilience is poor, easy generation electrostatic, the shortcomings such as poor heat resistance.
Summary of the invention
The object of the invention is to, for the deficiency of current material, provide the preparation method of a kind of expanded vermiculite-non-woven sound absorbent material of urethane composite emulsion coating thermoplastic phenolic resin.This material has larger specific surface area, and in structure, comparatively traditional non-woven materials is more tight, and noise reduction is obvious.
To achieve these goals, the technical solution used in the present invention is as follows: a kind of preparation method of interior sound insulation material of decorateing, described sound-proof material is made up of the raw material of following weight part: thermoplasticity phenylphenol resin 42-56, expanded vermiculite 20-25, polystyrene foamed plastics 4-6, silane coupling agent 2-3, nano carbon black 1-1.5, polymethylmethacrylate 8-10, oxidation inhibitor 0.1-0.2, whipping agent 0.1-0.2, magnesite 0.2-0.3, solid content is the silicon dioxide gel 2-3 of 10-15%, 100-200 order polynite 20-24, solid content is the aqueous polyurethane emulsion 10-12 of 8-10%, collegen filament 10-20, waste wool felt 20-30, auxiliary agent 2-5, described expanded vermiculite doubly forms the particulate matter by inside with countless tiny thin layer hole through 1000-1200 DEG C of high-temperature roasting enlarged volume 15-25 after being pulverized by vermiculite, described collegen filament prepare through pretreated useless leather by finite concentration defibrination in paste roller mill, described auxiliary agent is made up of the raw material of following weight part: 400-500 order fine hair powder 1-2, sodium lauryl sulphate 0.5-0.6, propylene glycol 3-5, solid content are zirconia sol 4-5, nano-nickel oxide 0.6-0.8, the water 10-12 of 15-20%, preparation method is: first drop in water by propylene glycol, sodium lauryl sulphate, be stirred to after material dissolves dispersion completely, add other leftover materials again, high-speed stirring is dispersed and get final product in the solution to fine hair powder, nano-nickel oxide, the preparation method of this material is as follows:
(1) first nanometer carbon black, silicon dioxide gel, auxiliary agent are dropped into together in aqueous polyurethane emulsion, supersound process 50-60min, make material dispersed in emulsion, gained composite emulsion is for subsequent use;
(2) expanded vermiculite, magnesite and polynite and silane coupling agent mixed grinding are disperseed 2-2.5h, gained material mixes with other leftover materials, stir in rear input twin screw extruder and melt extrude granulation at 180-190 DEG C of temperature, obtain modified master batch;
(3) modified master batch of step (2) gained is dropped into melting at 180-200 DEG C in screw extrusion press, melt is the meltblown beam orifice ejection of 230-250 DEG C through temperature, and stretch under the high velocity, hot air stream effect of 250-280 DEG C laggard enter receiving trap, being gathered on the reception device after net until fiber yarn uniformly sprays in silk screen by composite emulsion prepared by step (1), and emulsion to be composite gets product after solidifying drying completely sound insulation nonwoven material.Preferably, described defibrination rotating speed is that 4000-6000 turns.Preferably, the solid content of described zirconia sol is 18%.
Usefulness of the present invention is: a kind of expanded vermiculite prepared by the present invention-urethane composite emulsion coating thermoplastic phenolic resin nonwoven acoustic insulator quality of materials is light, and thickness is little, and soundproof effect is very good, has good market outlook.The advantage of conventional polypropylene nonwoven material has been acted on through the fibre web material that obtains of composite modified master batch spray silk, and its mechanical property improves, possesses excellent weatherable, long-time use is indeformable, and the urethane composite emulsion of preparation is after the coated solidification of fiber surface, the material wherein adulterated makes fibre web intensity improve, and damping is strengthened, and effect of vibration and noise reduction is obvious; Sound-proof material light weight environmental protection prepared by the present invention, noise reduction is lasting, and not polluting environment inside car, is a kind of Soundproof material for vehicle of novel practical.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described, but the present invention's scope required for protection is not limited to the described scope of embodiment.
Embodiment:
Decorate the preparation method of interior sound insulation material, and described sound-proof material is made up of the raw material of following weight part: aqueous polyurethane emulsion 10-12, collegen filament 10-20 that silicon dioxide gel 2-3,100-200 order polynite 20-24 that thermoplasticity phenylphenol resin 42-56, expanded vermiculite 20-25, polystyrene foamed plastics 4-6, silane coupling agent 2-3, nano carbon black 1-1.5, polymethylmethacrylate 8-10, oxidation inhibitor 0.1-0.2, whipping agent 0.1-0.2, magnesite 0.2-0.3, solid content are 10-15%, solid content are 8-10%; Waste wool felt 20-30; Auxiliary agent 2-5; Described expanded vermiculite doubly forms the particulate matter by inside with countless tiny thin layer hole through 1000-1200 DEG C of high-temperature roasting enlarged volume 15-25 after being pulverized by vermiculite; Described collegen filament prepare through pretreated useless leather by finite concentration defibrination in paste roller mill; Described auxiliary agent is made up of the raw material of following weight part: 400-500 order fine hair powder 1-2, sodium lauryl sulphate 0.5-0.6, propylene glycol 3-5, solid content are zirconia sol 4-5, nano-nickel oxide 0.6-0.8, the water 10-12 of 15-20%, preparation method is: first drop in water by propylene glycol, sodium lauryl sulphate, be stirred to after material dissolves dispersion completely, add other leftover materials again, high-speed stirring is dispersed and get final product in the solution to fine hair powder, nano-nickel oxide; The preparation method of this material is as follows:
(1) first nanometer carbon black, silicon dioxide gel, auxiliary agent are dropped into together in aqueous polyurethane emulsion, supersound process 50-60min, make material dispersed in emulsion, gained composite emulsion is for subsequent use;
(2) expanded vermiculite, magnesite and polynite and silane coupling agent mixed grinding are disperseed 2-2.5h, gained material mixes with other leftover materials, stir in rear input twin screw extruder and melt extrude granulation at 180-190 DEG C of temperature, obtain modified master batch;
(3) modified master batch of step (2) gained is dropped into melting at 180-200 DEG C in screw extrusion press, melt is the meltblown beam orifice ejection of 230-250 DEG C through temperature, and stretch under the high velocity, hot air stream effect of 250-280 DEG C laggard enter receiving trap, being gathered on the reception device after net until fiber yarn uniformly sprays in silk screen by composite emulsion prepared by step (1), and emulsion to be composite gets product after solidifying drying completely sound insulation nonwoven material.
The sound-proof material obtained by the present embodiment is prepared into the thick thin layer of 8-10mm, and its area density is: 362.6-410.6g/m -2; Longitudinal tensile strength (N. (5cm) -1) be: 58.2-78.5.When frequency of sound wave is 5KHz, sound insulation coefficient ranges up to and reaches 1.64.
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.

Claims (3)

1. the preparation method of interior sound insulation material that decoratees, it is characterized in that: described sound-proof material is made up of the raw material of following weight part: thermoplasticity phenylphenol resin 42-56 part, expanded vermiculite 20-25 part, polystyrene foamed plastics 4-6 part, silane coupling agent 2-3 part, nano carbon black 1-1.5 part, polymethylmethacrylate 8-10 part, oxidation inhibitor 0.1-0.2 part, whipping agent 0.1-0.2 part, magnesite 0.2-0.3 part, solid content is silicon dioxide gel 2-3 part of 10-15%, 100-200 order polynite 20-24 part, solid content is aqueous polyurethane emulsion 10-12 part of 8-10%, collegen filament 10-20 part, waste wool felt 20-30 part, auxiliary agent 2-5 part etc.,
Described expanded vermiculite doubly forms the particulate matter by inside with countless tiny thin layer hole through 1000-1200 DEG C of high-temperature roasting enlarged volume 15-25 after being pulverized by vermiculite;
Described collegen filament prepare through pretreated useless leather by finite concentration defibrination in paste roller mill;
Described auxiliary agent is made up of the raw material of following weight part: 400-500 order fine hair powder 1-2, sodium lauryl sulphate 0.5-0.6, propylene glycol 3-5, solid content are zirconia sol 4-5, nano-nickel oxide 0.6-0.8, the water 10-12 of 15-20%, preparation method is: first drop in water by propylene glycol, sodium lauryl sulphate, be stirred to after material dissolves dispersion completely, add other leftover materials again, high-speed stirring is dispersed and get final product in the solution to fine hair powder, nano-nickel oxide;
The preparation method of this sound-proof material is as follows:
(1) first nanometer carbon black, silicon dioxide gel, auxiliary agent are dropped into together in aqueous polyurethane emulsion, supersound process 50-60min, make material dispersed in emulsion, gained composite emulsion is for subsequent use;
(2) expanded vermiculite, magnesite and polynite and silane coupling agent mixed grinding are disperseed 2-2.5h, gained material mixes with other leftover materials, stir in rear input twin screw extruder and melt extrude granulation at 180-190 DEG C of temperature, obtain modified master batch;
(3) modified master batch of step (2) gained is dropped into melting at 180-200 DEG C in screw extrusion press, melt is the meltblown beam orifice ejection of 230-250 DEG C through temperature, and stretch under the high velocity, hot air stream effect of 250-280 DEG C laggard enter receiving trap, being gathered on the reception device after net until fiber yarn uniformly sprays in silk screen by composite emulsion prepared by step (1), and emulsion to be composite gets product after solidifying drying completely sound insulation nonwoven material.
2. the preparation method of decoration interior sound insulation material as claimed in claim 1, is characterized in that: described defibrination rotating speed is that 4000-6000 turns.
3. the preparation method of the decoration interior sound insulation material as described in claim 1 and 2, is characterized in that: the solid content of described zirconia sol is 18%.
CN201510310853.XA 2015-06-09 2015-06-09 A kind of preparation method of interior sound insulation material of decorateing Active CN104861413B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105271943A (en) * 2015-10-12 2016-01-27 苏州法斯特信息科技有限公司 Sound insulation and adsorption material for indoor decoration and preparation method thereof
CN106009494A (en) * 2016-06-23 2016-10-12 温州德业化工有限公司 Sound-insulation material and preparation method thereof
CN106084630A (en) * 2016-06-08 2016-11-09 刘高志 A kind of decoration sound insulation environment-friendly materials and preparation method thereof
CN107118511A (en) * 2017-06-22 2017-09-01 合肥易美特建材有限公司 A kind of building decoration environmentally friendly acoustic material and preparation method thereof
CN107266120A (en) * 2017-07-05 2017-10-20 合肥市片叶装饰工程有限公司 Sound-insulation and heat-preservation building material and preparation method thereof
CN107325527A (en) * 2017-07-18 2017-11-07 合肥峰腾节能科技有限公司 Environmentally friendly acoustic material of a kind of building interior trim and preparation method thereof
CN107815063A (en) * 2017-09-28 2018-03-20 王占舟 A kind of domestic type noise reduction coil winder
CN114130120A (en) * 2021-10-19 2022-03-04 安徽元琛环保科技股份有限公司 Waterproof high-wear-resistance PTFE filter material and preparation method thereof

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106633819A (en) * 2016-11-29 2017-05-10 天长市良文运动器材有限公司 Low-temperature-resistant and crack-resistant synthetic leather applied to baseballs

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101285285A (en) * 2008-04-08 2008-10-15 陕西科技大学 Preparing process of composite sound absorbing paper
CN102977529A (en) * 2012-11-22 2013-03-20 芜湖跃飞新型吸音材料股份有限公司 Nano vermiculite modified composite sound absorbing material and preparation method thereof
CN102977530A (en) * 2012-11-22 2013-03-20 芜湖跃飞新型吸音材料股份有限公司 Gypsum whisker modified composite sound absorbing material and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101285285A (en) * 2008-04-08 2008-10-15 陕西科技大学 Preparing process of composite sound absorbing paper
CN102977529A (en) * 2012-11-22 2013-03-20 芜湖跃飞新型吸音材料股份有限公司 Nano vermiculite modified composite sound absorbing material and preparation method thereof
CN102977530A (en) * 2012-11-22 2013-03-20 芜湖跃飞新型吸音材料股份有限公司 Gypsum whisker modified composite sound absorbing material and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
罗英,张美云,刘正伟: "蛭石粉和胶原纤维配抄吸音纸的探讨", 《纸和造纸》 *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105271943A (en) * 2015-10-12 2016-01-27 苏州法斯特信息科技有限公司 Sound insulation and adsorption material for indoor decoration and preparation method thereof
CN106084630A (en) * 2016-06-08 2016-11-09 刘高志 A kind of decoration sound insulation environment-friendly materials and preparation method thereof
CN106084630B (en) * 2016-06-08 2018-09-28 台州创兴环保科技有限公司 A kind of decoration sound insulation environment-friendly materials and preparation method thereof
CN106009494A (en) * 2016-06-23 2016-10-12 温州德业化工有限公司 Sound-insulation material and preparation method thereof
CN106009494B (en) * 2016-06-23 2017-10-17 温州德业化工有限公司 A kind of acoustic material and preparation method thereof
CN107118511A (en) * 2017-06-22 2017-09-01 合肥易美特建材有限公司 A kind of building decoration environmentally friendly acoustic material and preparation method thereof
CN107266120A (en) * 2017-07-05 2017-10-20 合肥市片叶装饰工程有限公司 Sound-insulation and heat-preservation building material and preparation method thereof
CN107325527A (en) * 2017-07-18 2017-11-07 合肥峰腾节能科技有限公司 Environmentally friendly acoustic material of a kind of building interior trim and preparation method thereof
CN107815063A (en) * 2017-09-28 2018-03-20 王占舟 A kind of domestic type noise reduction coil winder
CN114130120A (en) * 2021-10-19 2022-03-04 安徽元琛环保科技股份有限公司 Waterproof high-wear-resistance PTFE filter material and preparation method thereof

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