CN104846671A - Composition for leveling agent and leveling agent as well as preparation method thereof - Google Patents
Composition for leveling agent and leveling agent as well as preparation method thereof Download PDFInfo
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- CN104846671A CN104846671A CN201510233165.8A CN201510233165A CN104846671A CN 104846671 A CN104846671 A CN 104846671A CN 201510233165 A CN201510233165 A CN 201510233165A CN 104846671 A CN104846671 A CN 104846671A
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- leveling agent
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Abstract
The invention discloses a composition for a leveling agent, the leveling agent and a preparation method thereof. The composition for the leveling agent comprises the following raw materials in parts by weight: 15 to 20 parts of polyethylene glycol stearate, 3 to 6 parts of fatty amine polyoxyethylene ether, 6 to 8 parts of polysorbate, 2 to 4 parts of sodium dodecyl benzene sulfonate, and 35 to 40 parts of deionized water. The invention also provides a method for preparing the leveling agent by using the composition. The method for preparing the leveling agent by using the composition comprises the following steps of adding the polyethylene glycol stearate, the fatty amine polyoxyethylene ether, the polysorbate and the dodecyl benzene sulfonate into a reaction kettle with an agitator in sequence, mixing and agitating an obtained mixture, and adding the deionized water into the obtained mixture while agitating the obtained mixture. The invention also provides the leveling agent, which is prepared according to the method. Matching raw materials of the composition for the leveling agent are a few, and are simple and easy to obtain; the preparation cost is low; the prepared leveling agent is good in retarding, migration and dispersion effects; further, the reparation method is simple.
Description
Technical field
The present invention relates to dye field, be specifically related to a kind of composition for levelling agent, levelling agent and preparation method thereof.
Background technology
Silvalin, line or fabric, in dyeing course, for impelling even dyeing, do not produce the fault such as vitta, color spot and a kind of material added is levelling agent.Levelling agent great majority are water miscible surfactants, according to the impact of levelling agent on dye diffusion and concentration class, are mainly divided into two types: close fibroid levelling agent and the dye levelling agent of parent.For the levelling agent used in polyester fibre at high temp and pressure dyeing, ubiquity formula is comparatively complicated, the shortcoming that cost of manufacture is higher.
Summary of the invention
Provide hereinafter about brief overview of the present invention, to provide about the basic comprehension in some of the present invention.Should be appreciated that this general introduction is not summarize about exhaustive of the present invention.It is not that intention determines key of the present invention or pith, and nor is it intended to limit the scope of the present invention.Its object is only provide some concept in simplified form, in this, as the preorder in greater detail discussed after a while.
The object of the embodiment of the present invention is the defect for above-mentioned prior art, a kind of slow dye is provided, move dye and dispersion effect good, and proportioning is simple, the levelling agent that preparation cost is low.
To achieve these goals, the technical scheme that the present invention takes is:
For a composition for levelling agent, comprise the raw material of following weight portion:
Solutol HS15-20 parts; Aliphatic amine polyoxyethylene ether 3-6 part; Polysorbate 6-8 part; Neopelex 2-4 part; Deionized water 35-40 part.
The preferred technical scheme that the embodiment of the present invention provides: a kind of composition for levelling agent, comprises the raw material of following weight portion:
Polyethylene glycol stearate 17 parts; Aliphatic amine polyoxyethylene ether 5 parts; Polysorbate 7 parts; Neopelex 3 parts; Deionized water 38 parts.
The present invention also provides a kind of method using above-mentioned composition to prepare levelling agent, comprises the following steps:
Polyethylene glycol stearate, aliphatic amine polyoxyethylene ether, polysorbate, neopelex are added successively in the reactor with agitator, mix and blend, adds deionized water while stirring.
Temperature in described reactor is 80-90 DEG C.
The rotating speed of described stirring is 400-500 rev/min, and the time of stirring is 30-50 minute.
Invention further provides a kind of levelling agent, prepare according to above-mentioned method.
Compared with prior art, the invention has the beneficial effects as follows:
Proportioning raw material of the present invention is few, simple and easy to get, and preparation cost is low, the slow dye of the levelling agent of preparation, move dye and dispersion effect good, and preparation method is simple.
Detailed description of the invention
For making the object of the embodiment of the present invention, technical scheme and advantage clearly, be clearly and completely described below to the technical scheme in the embodiment of the present invention, obviously, described embodiment is the present invention's part embodiment, instead of whole embodiments.The element described in one embodiment of the invention and feature can combine with the element shown in one or more embodiment and feature.It should be noted that for purposes of clarity, in explanation, eliminate expression and the description of unrelated to the invention, parts known to persons of ordinary skill in the art and process.Based on the embodiment in the present invention, those of ordinary skill in the art, not paying the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
Raw material (kilogram) is taken according to following proportioning:
Polyethylene glycol stearate 17 kilograms; Aliphatic amine polyoxyethylene ether 5 kilograms; Polysorbate 7 kilograms; Neopelex 3 kilograms; Deionized water 38 kilograms.
The preparation method of levelling agent: 17 kilograms of polyethylene glycol stearates, 5 kilograms of aliphatic amine polyoxyethylene ethers, 7 kilograms of polysorbates, 3 kilograms of neopelexes are added in the reactor with agitator successively, control the temperature 85 DEG C of reactor, with the speed mix and blend of 400-500 rev/min, add 38 kilograms of deionized waters while stirring, until deionized water adds, the time of stirring is 40 minutes.
Embodiment 2
Raw material (kilogram) is taken according to following proportioning:
Solutol HS15 kilogram; Aliphatic amine polyoxyethylene ether 6 kilograms; Polysorbate 6 kilograms; Neopelex 4 kilograms; Deionized water 35 kilograms.
The preparation method of levelling agent: 15 kilograms of polyethylene glycol stearates, 6 kilograms of aliphatic amine polyoxyethylene ethers, 6 kilograms of polysorbates, 4 kilograms of neopelexes are added in the reactor with agitator successively, control the temperature 90 DEG C of reactor, with the speed mix and blend of 500 revs/min, add 35 kilograms of deionized waters while stirring, until deionized water adds, the time of stirring is 30 minutes.
Solutol HS15-20 parts; Aliphatic amine polyoxyethylene ether 3-6 part; Polysorbate 6-8 part; Neopelex 2-4 part; Deionized water 35-40 part.
Embodiment 3
Raw material (kilogram) is taken according to following proportioning:
Polyethylene glycol stearate 20 kilograms; Aliphatic amine polyoxyethylene ether 3 kilograms; Polysorbate 8 kilograms; Neopelex 2 kilograms; Deionized water 40 kilograms.
The preparation method of levelling agent: 20 kilograms of polyethylene glycol stearates, 3 kilograms of aliphatic amine polyoxyethylene ethers, 8 kilograms of polysorbates, 2 kilograms of neopelexes are added in the reactor with agitator successively, control the temperature 80 DEG C of reactor, with the speed mix and blend of 400 revs/min, add 40 kilograms of deionized waters while stirring, until deionized water adds, the time of stirring is 50 minutes.
Through inspection, use levelling agent of the present invention, the fabric color after dyeing is more even, bright-coloured, does not occur the product with the fault such as vitta, color spot.
Last it is noted that above embodiment is only in order to illustrate technical scheme of the present invention, be not intended to limit; Although with reference to previous embodiment to invention has been detailed description, those of ordinary skill in the art is to be understood that: it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature; And these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (6)
1. for a composition for levelling agent, it is characterized in that, comprise the raw material of following weight portion:
Solutol HS15-20 parts; Aliphatic amine polyoxyethylene ether 3-6 part; Polysorbate 6-8 part; Neopelex 2-4 part; Deionized water 35-40 part.
2. the composition for levelling agent according to claim 1, is characterized in that, comprises the raw material of following weight portion:
Polyethylene glycol stearate 17 parts; Aliphatic amine polyoxyethylene ether 5 parts; Polysorbate 7 parts; Neopelex 3 parts; Deionized water 38 parts.
3. use the composition described in claim 1 or 2 to prepare a method for levelling agent, it is characterized in that, comprise the following steps:
Polyethylene glycol stearate, aliphatic amine polyoxyethylene ether, polysorbate, neopelex are added successively in the reactor with agitator, mix and blend, adds deionized water while stirring.
4. method according to claim 1, is characterized in that, the temperature in described reactor is 80-90 DEG C.
5. method according to claim 1, is characterized in that, the rotating speed of described stirring is 400-500 rev/min, and the time of stirring is 30-50 minute.
6. a levelling agent, is characterized in that, prepares according to the method described in any one of claim 3-5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510233165.8A CN104846671A (en) | 2015-05-08 | 2015-05-08 | Composition for leveling agent and leveling agent as well as preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510233165.8A CN104846671A (en) | 2015-05-08 | 2015-05-08 | Composition for leveling agent and leveling agent as well as preparation method thereof |
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| CN104846671A true CN104846671A (en) | 2015-08-19 |
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| CN201510233165.8A Pending CN104846671A (en) | 2015-05-08 | 2015-05-08 | Composition for leveling agent and leveling agent as well as preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105239425A (en) * | 2015-10-20 | 2016-01-13 | 湖州博仁纺织品有限公司 | Acid dye leveling agent integrating uniform dyeing, color increasing and color fixing and preparation method thereof |
| CN105544248A (en) * | 2016-01-25 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Efficient leveling agent and preparation method thereof |
| CN105648797A (en) * | 2016-04-12 | 2016-06-08 | 湖州吉昌丝绸有限公司 | Environment-friendly and efficient biparental levelling agent |
| CN107217510A (en) * | 2017-06-23 | 2017-09-29 | 太仓大唐化纤厂 | A kind of chemical ＆ blended fabric environment-friendly high-efficiency levelling agent |
| CN109235083A (en) * | 2018-07-11 | 2019-01-18 | 黄勇 | A kind of textile levelling agent |
| CN110699987A (en) * | 2019-10-24 | 2020-01-17 | 艾绳瑞 | Leveling agent and application thereof in polyester dyeing |
| CN115787324A (en) * | 2022-11-04 | 2023-03-14 | 绍兴丰禾科技有限公司 | Acidic leveling agent and preparation method thereof |
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| CN102839549A (en) * | 2012-09-19 | 2012-12-26 | 吴江市意胜纺织有限公司 | Novel leveling and dispersing agent |
| CN103243582A (en) * | 2013-04-16 | 2013-08-14 | 杜芳莉 | Acidic levelling agent and preparation method thereof |
| CN104389203A (en) * | 2014-12-17 | 2015-03-04 | 无锡瑞贝纺织品实业有限公司 | Wool levelling agent and preparation method thereof |
| CN104532617A (en) * | 2014-12-24 | 2015-04-22 | 常熟市淼泉盛达助剂厂 | Leveling agent for fabrics |
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| CN102839549A (en) * | 2012-09-19 | 2012-12-26 | 吴江市意胜纺织有限公司 | Novel leveling and dispersing agent |
| CN103243582A (en) * | 2013-04-16 | 2013-08-14 | 杜芳莉 | Acidic levelling agent and preparation method thereof |
| CN104389203A (en) * | 2014-12-17 | 2015-03-04 | 无锡瑞贝纺织品实业有限公司 | Wool levelling agent and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105239425A (en) * | 2015-10-20 | 2016-01-13 | 湖州博仁纺织品有限公司 | Acid dye leveling agent integrating uniform dyeing, color increasing and color fixing and preparation method thereof |
| CN105239425B (en) * | 2015-10-20 | 2017-10-17 | 湖州优创科技有限公司 | A kind of acid dyes levelling agent for collecting the hyperchromic fixation one of level dyeing and preparation method thereof |
| CN105544248A (en) * | 2016-01-25 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Efficient leveling agent and preparation method thereof |
| CN105648797A (en) * | 2016-04-12 | 2016-06-08 | 湖州吉昌丝绸有限公司 | Environment-friendly and efficient biparental levelling agent |
| CN107217510A (en) * | 2017-06-23 | 2017-09-29 | 太仓大唐化纤厂 | A kind of chemical ＆ blended fabric environment-friendly high-efficiency levelling agent |
| CN109235083A (en) * | 2018-07-11 | 2019-01-18 | 黄勇 | A kind of textile levelling agent |
| CN110699987A (en) * | 2019-10-24 | 2020-01-17 | 艾绳瑞 | Leveling agent and application thereof in polyester dyeing |
| CN115787324A (en) * | 2022-11-04 | 2023-03-14 | 绍兴丰禾科技有限公司 | Acidic leveling agent and preparation method thereof |
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Application publication date: 20150819 |