CN104825392A - Processing system and method for reducing peroxide value and anisidine value of fat emulsion - Google Patents
Processing system and method for reducing peroxide value and anisidine value of fat emulsion Download PDFInfo
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- CN104825392A CN104825392A CN201510198910.XA CN201510198910A CN104825392A CN 104825392 A CN104825392 A CN 104825392A CN 201510198910 A CN201510198910 A CN 201510198910A CN 104825392 A CN104825392 A CN 104825392A
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- homogenizing
- fat milk
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- BHAAPTBBJKJZER-UHFFFAOYSA-N p-anisidine Chemical compound COC1=CC=C(N)C=C1 BHAAPTBBJKJZER-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 150000002978 peroxides Chemical class 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 20
- 238000012545 processing Methods 0.000 title claims description 10
- 239000002960 lipid emulsion Substances 0.000 title abstract 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 78
- 235000013336 milk Nutrition 0.000 claims abstract description 61
- 239000008267 milk Substances 0.000 claims abstract description 61
- 210000004080 milk Anatomy 0.000 claims abstract description 61
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 55
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 28
- 230000004087 circulation Effects 0.000 claims abstract description 4
- 210000003022 colostrum Anatomy 0.000 claims description 40
- 235000021277 colostrum Nutrition 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 18
- 239000001301 oxygen Substances 0.000 claims description 18
- 229910052760 oxygen Inorganic materials 0.000 claims description 18
- 239000008215 water for injection Substances 0.000 claims description 14
- 230000017531 blood circulation Effects 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- 238000000265 homogenisation Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- 238000006392 deoxygenation reaction Methods 0.000 claims description 8
- 230000004224 protection Effects 0.000 claims description 8
- 230000001804 emulsifying effect Effects 0.000 claims description 6
- 230000009467 reduction Effects 0.000 claims description 6
- 230000009471 action Effects 0.000 claims description 4
- 238000004891 communication Methods 0.000 claims description 3
- 238000002347 injection Methods 0.000 claims description 3
- 239000007924 injection Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 abstract description 3
- 235000011187 glycerol Nutrition 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 235000005687 corn oil Nutrition 0.000 description 11
- 238000002360 preparation method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 108010004103 Chylomicrons Proteins 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 210000001268 chyle Anatomy 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a treatment system for reducing the peroxide value and the anisidine value of fat emulsion, which comprises a deaerator (1), a homogenizer (5), a homogenizing pump (6), a configuration tank, a filling machine (8) and a nitrogen conveying pipe (9), wherein the nitrogen conveying pipe (9) is respectively communicated with the configuration tanks, the deaerator (1) is respectively communicated with a glycerin tank (2) and a primary emulsion tank (3) through pipelines, the primary emulsion tank (3), the homogenizer (5), the homogenizing pump (6) and the homogenizing tank (4) form a closed circulation automatic control system through pipelines, the homogenizing tank (4) is communicated with a filling tank (7), the filling tank (7) is communicated with a filling machine (8), a plurality of vacuumizing devices are arranged below the filling machine (8), and the treatment system also discloses a method for reducing the peroxide value and the anisidine value of the fat emulsion. The invention has the beneficial effects that: it has the advantages of improving the quality of fat milk, prolonging the storage time of the fat milk and reducing the peroxide value and the anisidine value of the fat milk.
Description
Technical field
The present invention relates to fat milk preparation field, particularly reduce fat milk peroxide value and anisidine value processing system and method thereof.
Background technology
Fat milk is a kind of not only even but also stable lipomul be made up of refined soybean oil, glycerol, lecithin etc., provides high-energy and required fatty acid under the importance that its is treated is non-bowel provisions.Proved that the fat that human body is taken in first forms Chylomicron through gastrointestinal absorption from physiology and threpsology, and the form of these product is all extremely similar to chyle with composition, directly to the venous patient infusion that can not take food, can provide lipid nutrition.
But, lipomul peroxide value aborning and anisidine value compare and are difficult to control, directly affect product quality and quality, thus jeopardize user health of human body, therefore for ensureing the quality of lipomul, ensure the health of human body of user, the lipomul that peroxide value and anisidine value are all lower must be used.
Summary of the invention
The object of the invention is to the shortcoming overcoming prior art, provide a kind of and improve product quality, the processing system that can reduce fat milk peroxide value and anisidine value and method thereof.
Object of the present invention is achieved through the following technical solutions: reduce fat milk peroxide value and anisidine value processing system, it comprises oxygen-eliminating device, glycerol tank, colostrum tank, homogenizing tank, homogenizer, Homogenizing pump, fill tank, filling machine and nitrogen carrier pipe, described nitrogen carrier pipe respectively with glycerol tank, colostrum tank, homogenizing tank, fill tank is communicated with filling machine, the bypass line that it is communicated with is provided with valve, and described oxygen-eliminating device is communicated with colostrum tank with glycerol tank respectively by pipeline, and described glycerol tank and colostrum tank pass through pipeline communication, and on its pipeline, be provided with bivalve, described colostrum tank, homogenizer, Homogenizing pump and homogenizing tank form closed circulation robot control system(RCS) by pipeline, described homogenizing tank is communicated with fill tank, and bivalve is provided with on its pipeline be communicated with, fill tank is communicated with can packing machine, and bivalve is provided with on its pipeline be communicated with, be provided with multiple vacuum extractor below described filling machine, the front end of vacuum extractor is provided with valve.
Described closed cycle system is made up of a homogenisation cycle system and second homogenate blood circulation, wherein in a homogenisation cycle system, the port of export of colostrum tank is communicated with the entrance point of Homogenizing pump, and bivalve is provided with on its pipeline be communicated with, the port of export of Homogenizing pump is communicated with homogenizer, the port of export of described homogenizer is communicated with fill tank, and the pipeline that it is communicated with is provided with bivalve; In second homogenate blood circulation, the bottom of homogenizing tank is communicated with the entrance point of Homogenizing pump, and is provided with bivalve on its pipeline be communicated with, and the port of export of Homogenizing pump is communicated with homogenizer, the port of export of described homogenizer is communicated with colostrum tank, and the pipeline that it is communicated with is provided with bivalve.
Described filling machine lower end arranges three vacuum extractors.
Described glycerol tank and the tank connected pipeline of colostrum are provided with a delivery pump and filter.
Reduce the method for fat milk peroxide value and anisidine value, it comprises following steps:
S1: source deoxygenation, water for injection is directly connected with oxygen-eliminating device by pipeline, reduces the content of injection water oxygen, obtains the water for injection that oxygen content is lower;
S2: isotonic process, is transported to water for injection in S1 in glycerol tank, makes water for injection and glycerol according to the ratio mixing of regulation, is then sent in colostrum tank by the medicinal liquid mixed, obtain fat milk;
S3; Homogenizing process, fat milk in being filled with by colostrum is through a homogenisation cycle system homogenizing, then be stored in homogenizing tank, again by the fat milk in homogenizing tank through second homogenate blood circulation homogenizing, again get back in colostrum tank, repeatedly repeat above-mentioned action, reach the object that fat milk emulsifying reduces anisidine value, then by the fat milk that homogenizing is good, be transported in fill tank by Homogenizing pump;
S4: fill process: the fat milk in fill tank, by nitrogen pressure press-in filling machine, then through multiple vacuum extractor repeatedly evacuation, repeatedly nitrogen filled protection, realizes the low oxygen and filling nitrogen fill of fat milk;
Described step S2, S3 and S4 all implement under the protection of nitrogen
The present invention has the following advantages: the present invention arranges oxygen-eliminating device in the source of preparation water, reach the object of alternate source head processed deoxygenation, and in lipomul production process, under being all in the protective effect of nitrogen, the contact of isolated lipomul and extraneous oxygen, reduces the peroxide value in lipomul; In fat milk preparation process, fat milk repeatedly enters homogenizing in homogenizer by blood circulation, reduces the anisidine value in fat milk; And in fat milk pouring process, repeatedly evacuation and fill nitrogen, further ensure that fat milk does not contact with extraneous oxygen, makes the oxygen content of fat milk on the low side, extend the storage time of fat milk, improve the quality of fat milk.
Accompanying drawing explanation
Fig. 1 is the device schematic flow sheet of the embodiment of the present invention;
In figure, 1-oxygen-eliminating device, 2-glycerol tank, 3-colostrum tank, 4-homogenizing tank, 5-homogenizer, 6-Homogenizing pump, 7-fill tank, 8-filling machine, 9-nitrogen carrier pipe.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention will be further described, and protection scope of the present invention is not limited to the following stated:
As shown in Figure 1, reduce fat milk peroxide value and anisidine value processing system, it comprises oxygen-eliminating device 1, glycerol tank 2, colostrum tank 3, homogenizing tank 4, homogenizer 5, Homogenizing pump 6, fill tank 7, filling machine 8 and nitrogen carrier pipe 9, described nitrogen carrier pipe 9 respectively with glycerol tank 2, colostrum tank 3, homogenizing tank 4, fill tank 7 is communicated with filling machine 8, the bypass line that it is communicated with is provided with valve, valve is in normally open herein, whole lipomul is all in nitrogen protection in preparation process, isolated lipomul, glycerol tank 2, colostrum tank 3, homogenizing tank 4, fill tank 7 contacts with extraneous oxygen with filling machine 8, thus the peroxide value reduced in fat milk, and make its content maintain in a less interval all the time, described oxygen-eliminating device 1 is communicated with colostrum tank 3 with glycerol tank 2 respectively by pipeline, water for injection is through oxygen-eliminating device 1 deoxygenation, thus described glycerol tank 2 passes through pipeline communication with colostrum tank 3, and bivalve is provided with on its pipeline, the water for injection that configuration emulsion products uses, all deoxygenation process has been carried out enter glycerol tank 2 and colostrum tank 3 after oxygen-eliminating device 1 deoxygenation before, reach the dissolved oxygen amount that Sources controlling prepares use water, described colostrum tank 3, homogenizer 5, Homogenizing pump 6 and homogenizing tank 4 form closed circulation robot control system(RCS) by pipeline, described homogenizing tank 4 is communicated with fill tank 7, and bivalve is provided with on its pipeline be communicated with, fill tank 7 is communicated with can packing machine 8, and bivalve is provided with on its pipeline be communicated with, lipomul in fill tank 7 is pushed down in filling machine 8 in the effect of nitrogen pressure, multiple vacuum extractor is provided with below described filling machine 8, the front end of vacuum extractor is provided with valve, in the present embodiment, described filling machine 8 lower end arranges three vacuum extractors, vacuum extractor, regulate vacuum extractor can carry out three evacuation and three nitrogen filled protections to the lipomul of fill, and can according to practical situation, at each evacuation with when filling nitrogen, can one by one to single evacuation amount and the parameter adjustment of filling nitrogen quantity, ensure the existence of medicinal liquid bottle noresidue oxygen.
In this enforcement, described closed cycle system is made up of a homogenisation cycle system and second homogenate blood circulation, wherein in a homogenisation cycle system, the port of export of colostrum tank 3 is communicated with the entrance point of Homogenizing pump 6, and bivalve is provided with on its pipeline be communicated with, the port of export of Homogenizing pump 6 is communicated with homogenizer 5, the port of export of described homogenizer 5 is communicated with fill tank 7, the pipeline that it is communicated with is provided with bivalve, fat milk in colostrum tank 3 delivers in homogenizer 5 through Homogenizing pump 6, fat milk enters in homogenizing tank 4 and stores after the anisidine value that homogenizer 5 reduces fat milk, after the fat milk in colostrum tank 3 drains, close and open corresponding valve, fat milk is made to enter in second homogenate blood circulation, in second homogenate blood circulation, the bottom of homogenizing tank 4 is communicated with the entrance point of Homogenizing pump 6, and bivalve is provided with on its pipeline be communicated with, the port of export of Homogenizing pump 6 is communicated with homogenizer 5, the port of export of described homogenizer 5 is communicated with colostrum tank 3, the pipeline that it is communicated with is provided with bivalve, fat milk in homogenizing tank 4 is transported in homogenizer through Homogenizing pump 6, fat milk enters in colostrum tank 4 and stores after the anisidine value that homogenizer 5 reduces fat milk again, after the fat milk in homogenizing tank 4 drains, close and open corresponding valve, fat milk is made to enter in a homogenisation cycle system, repeatedly repeat above-mentioned action, anisidine value in fat milk is significantly reduced.
In the present embodiment, the pipeline that described glycerol tank 2 is connected with colostrum tank 3 is provided with a delivery pump and filter, and do not indicate in the drawings, medicinal liquid enters into colostrum tank 3 by delivery pump and metre filter.
In the present embodiment, the pipeline be communicated with arranges bivalve, can valves leakage be prevented, improve safety coefficient, be also provided with blow-off pipe in the bottom of glycerol tank 2, colostrum tank 3, homogenizing tank 4, fill tank 7, blow-off pipe be provided with valve, do not indicate in figure.
Described reduction fat milk peroxide value and the method for anisidine value, it comprises following steps:
S1: source deoxygenation, water for injection is directly connected with oxygen-eliminating device 1 by pipeline, reaches the dissolved oxygen amount that Sources controlling prepares use water, reduces the content of injection water oxygen, obtains the water for injection that oxygen content is lower;
S2: isotonic process, is transported to water for injection in S1 in glycerol tank 2, makes water for injection and glycerol according to the ratio mixing of regulation, is then sent in colostrum tank 3 by the medicinal liquid mixed, obtain fat milk;
S3; Emulsifying, by the fat milk in colostrum filling 3 through a homogenisation cycle system homogenizing, then be stored in homogenizing tank 4, again by the fat milk in homogenizing tank 4 through second homogenate blood circulation homogenizing, again get back in colostrum tank 3, repeatedly repeat above-mentioned action, reach the object that fat milk emulsifying reduces anisidine value, then by the fat milk that homogenizing is good, be transported in fill tank 7 by Homogenizing pump 6;
S4: fill process: the fat milk in fill tank 7 is by nitrogen pressure press-in filling machine 8, completely cut off the contact with extraneous oxygen, and then through filling machine 8 fill in medicinal liquid bottle, filling machine possesses carrying out evacuation to product splendid attire medicinal liquid bottle and filling nitrogen of three discontinuity, the parameter adjustment of single splendid attire medicinal liquid bottle vacuum and nitrogen amount size can be implemented, to ensure the existence of medicinal liquid bottle noresidue oxygen.
Implement under protection all at nitrogen of described step S2, S3 and S4; thus reach source deoxygenation; in emulsifying and pouring process; completely cut off the contact with extraneous oxygen; play the object reducing fat milk peroxide value; and fat milk is through repeatedly emulsifying, make the anisidine value content in fat milk less, serve the effect reducing anisidine value.
Claims (5)
1. reduce fat milk peroxide value and anisidine value processing system, it is characterized in that: it comprises oxygen-eliminating device (1), glycerol tank (2), colostrum tank (3), homogenizing tank (4), homogenizer (5), Homogenizing pump (6), fill tank (7), filling machine (8) and nitrogen carrier pipe (9), described nitrogen carrier pipe (9) respectively with glycerol tank (2), colostrum tank (3), homogenizing tank (4), fill tank (7) is communicated with filling machine (8), the bypass line that it is communicated with is provided with valve, described oxygen-eliminating device (1) is communicated with colostrum tank (3) with glycerol tank (2) respectively by pipeline, described glycerol tank (2) and colostrum tank (3) pass through pipeline communication, and on its pipeline, be provided with bivalve, described colostrum tank (3), homogenizer (5), Homogenizing pump (6) and homogenizing tank (4) form closed circulation robot control system(RCS) by pipeline, described homogenizing tank (4) is communicated with fill tank (7), and bivalve is provided with on its pipeline be communicated with, fill tank (7) is communicated with can packing machine (8), and bivalve is provided with on its pipeline be communicated with, described filling machine (8) below is provided with multiple vacuum extractor, and the front end of vacuum extractor is provided with valve.
2. reduction fat milk peroxide value according to claim 1 and anisidine value processing system, it is characterized in that: described closed cycle system is made up of a homogenisation cycle system and second homogenate blood circulation, wherein in a homogenisation cycle system, the port of export of colostrum tank (3) is communicated with the entrance point of Homogenizing pump () 6, and bivalve is provided with on its pipeline be communicated with, the port of export of Homogenizing pump (6) is communicated with homogenizer (5), the port of export of described homogenizer (5) is communicated with fill tank (7), and the pipeline that it is communicated with is provided with bivalve; In second homogenate blood circulation, the bottom of homogenizing tank (4) is communicated with the entrance point of Homogenizing pump (6), and bivalve is provided with on its pipeline be communicated with, the port of export of Homogenizing pump (6) is communicated with homogenizer (5), the port of export of described homogenizer (5) is communicated with colostrum tank (3), and the pipeline that it is communicated with is provided with bivalve.
3. reduction fat milk peroxide value according to claim 1 and anisidine value processing system, is characterized in that: described filling machine (8) lower end arranges three vacuum extractors.
4. reduction fat milk peroxide value according to claim 1 and anisidine value processing system, is characterized in that: the pipeline that described glycerol tank (2) is connected with colostrum tank (3) is provided with a delivery pump and filter.
5., based on the method for the reduction fat milk peroxide value described in any one of claim 1 ~ 4 and anisidine value, it is characterized in that: it comprises following steps:
S1: source deoxygenation, water for injection is directly connected with oxygen-eliminating device (1) by pipeline, reduces the content of injection water oxygen, obtains the water for injection that oxygen content is lower;
S2: isotonic process, is transported to water for injection in S1 in glycerol tank (2), makes water for injection and glycerol according to the ratio mixing of regulation, is then sent in colostrum tank (3) by the medicinal liquid mixed, obtain fat milk;
S3; Homogenizing process, by the fat milk in colostrum filling (3) through a homogenisation cycle system homogenizing, then be stored in homogenizing tank (4), again by the fat milk in homogenizing tank (4) through second homogenate blood circulation homogenizing, again get back in colostrum tank (3), repeatedly repeat above-mentioned action, reach the object that fat milk emulsifying reduces anisidine value, then by the fat milk that homogenizing is good, be transported in fill tank by Homogenizing pump (6);
S4: fill process: the fat milk in fill tank (7) is pressed in filling machine (8) by nitrogen pressure, then through multiple vacuum extractor repeatedly evacuation, repeatedly nitrogen filled protection, realizes the low oxygen and filling nitrogen fill of fat milk;
The method of reduction fat milk peroxide value according to claim 5 and anisidine value, is characterized in that: described step S2, S3 and S4 all implement under the protection of nitrogen.
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Cited By (5)
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CN105950285A (en) * | 2016-04-21 | 2016-09-21 | 内蒙古蒙牛乳业(集团)股份有限公司 | Extraction method for fat in dairy product and determination method for peroxide value of fat |
CN106074672A (en) * | 2016-07-18 | 2016-11-09 | 四川科伦药业股份有限公司 | Constant temperature system for improving quality of fat milk product |
CN106490656A (en) * | 2016-12-13 | 2017-03-15 | 厦门惠盈动物科技有限公司 | A kind of emulsification liquid additive premix production system and production technology |
CN106881049A (en) * | 2015-12-15 | 2017-06-23 | 上海奥星制药技术装备有限公司 | Homogeneous control system and its control method |
CN114948871A (en) * | 2022-06-14 | 2022-08-30 | 四川科伦药业股份有限公司 | Fat emulsion injection and preparation method and device thereof |
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CN114948871B (en) * | 2022-06-14 | 2023-11-17 | 四川科伦药业股份有限公司 | Fat emulsion injection and preparation method and device thereof |
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