CN104800268A - Compound taraxacum mongolicum and andrographis paniculata lozenge for treating laryngopharyngitis and amygdalitis as well as preparation method thereof - Google Patents
Compound taraxacum mongolicum and andrographis paniculata lozenge for treating laryngopharyngitis and amygdalitis as well as preparation method thereof Download PDFInfo
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- CN104800268A CN104800268A CN201510194950.7A CN201510194950A CN104800268A CN 104800268 A CN104800268 A CN 104800268A CN 201510194950 A CN201510194950 A CN 201510194950A CN 104800268 A CN104800268 A CN 104800268A
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Abstract
The invention discloses a compound taraxacum mongolicum and andrographis paniculata lozenge for treating laryngopharyngitis and amygdalitis as well as a preparation method thereof. According to the lozenge, taraxacum mongolicum, andrographis paniculata, helictercs angustifolia, isatis indigotica, menthol and borneol are used as raw materials, maltodextrin, mannitol, lactose, sorbitol and sucrose powder are used diluents, aerosil is used as a lubricant, stevia sugar and sucrose powder are used as a corrigent, and an adhesive is prepared by 65-75% ethanol water. The lozenge is smooth in surface, uniform and consistent in color, cool, tasty, fine and smooth and mild after entering the mouth and good in disintegrating property and meets relevant provisions of 2010 Chinese Pharmacopoeia (part II). The lozenge is relatively simple in preparation process and suitable for industrial mass production.
Description
Technical field
The present invention relates to medical art, be specifically related to one and treat acute and chronic pharyngitis, tonsillitic compound recipe English lotus buccal tablet and preparation method thereof.
Background technology
Dandelion is feverfew Herba Taraxaci (Taraxacum mongolicum Hand.-Mazz.), alkali ground Herba Taraxaci (Taraxacum sinicum Kitag.) or belong to the dry herb of several plants together.Herba Taraxaci herb, containing taraxasterol, choline, inulin and pectin etc., is the Chinese crude drug of dietotherapeutic.Herba Taraxaci is the conventional medicament of heat-clearing and toxic substances removing, has heat-clearing and toxic substances removing, effect of dispersing swelling and dissipating binds, is used for the treatment of upper respiratory tract infection, pharyngitis, cold, fever, acute tonsillitis, acute bronchitis, lymphadenitis etc.In recent years, research proves that it has good anti-infectious function, and clinical application range is comparatively wide, and compatibility Radix Isatidis is evident in efficacy to laryngopharynx swelling and pain.
Herba Andrographis be acanthaceous plant (
andrographis paniculata (Burm. f.) Nees), have another name called Radix Gentianae, India's grass etc.Herba Andrographis bitter in the mouth, cold in nature; GUIXIN, lung, stomach, urinary bladder channel; There is heat-clearing and toxic substances removing, inducing diuresis and reducing edema effect.Containing materials such as flavone, sterol, saponin, saccharide and condensed tannins in Herba Andrographis.Research shows, Herba Andrographis have antibacterial, antipyretic, protect the liver, function of gallbladder promoting, antitumor action etc.Can be used for the treatment of upper respiratory tract infection, acute and chronic tonsillitis, acute and chronic pharyngitis, acute/chronic bronchitis, acute bacillary dysentery, acute gastroenteritis, urinary tract infection, pelvic inflammatory disease, otitis media, periodontitis clinically.
Radix Helicteris is Sterculiaceae Radix Helicteris platymiscium Radix Helicteris (Helictercs angustifolia L.), is used as medicine with root or Herb.Its root contains the compositions such as flavone, phenol, tannin, has effect of heat-clearing and toxic substances removing, cough-relieving, can be used for the treatment of cold and high fever, tonsillitis, pharyngolaryngitis, laryngopharynx swelling and pain, parotitis, measles, cough, malaria clinically.
Radix Isatidis is the dry root of cruciferae isatis (Isatis indigotica Fort.), and property is bitter, cold; GUIXIN, stomach warp.Research shows, Radix Isatidis has antibacterial, the effect such as antiviral, raising immunity of organism, antitumor.Attack in wind heat clinically, laryngopharynx swelling and pain, heat-clearing and toxic substances removing, the treatment of removing heat from blood sore-throat relieving.
Mentholum is colourless needles or prism-shaped crystallization or white crystalline powder; Have the special aroma of Herba Menthae, taste is just scorching hot, rear refrigerant.Herba Menthae brain-capacity optionally stimulates the Cold receptor of human body skin or mucosa, produces sense of cold reflection and creeping chill, causes skin mucosa vasoconstriction; Also can cause contraction to the blood vessel of deep tissue in addition, and produce therapeutical effect.Be used as excitants clinically, make skin or mucosa produce refrigerant sense and be not suitable for alleviate, produce refrigerant itching-relieving action; Take orally and can be used as carminative, for headache and nose, pharynx, laryngitis etc.
Borneolum Syntheticum is the translucent crystalline solid like Flos Mume lobe bulk, lamellar, is that resin and the volatile oil processed goods of Spore density Borneolum Syntheticum extracts the crystallization obtained.Borneolum Syntheticum acrid in the mouth, hardship, be slightly cold; GUIXIN, liver, lung meridian; A surname is loose for delicate fragrance, has refreshment of having one's ideas straightened out, poison is fallen apart in heat clearing away, effect of improving acuity of vision and removing nebula; Gas delicate fragrance; Can be used for excess syndrome of stroke coma, conjunctival congestion and swelling pain, sore throat aphtha, skin infection swell and ache, the treatment of disease such as after bursting, not hold back.
Above-mentioned all medicine compatibility uses, evident in efficacy to treatment acute and chronic pharyngitis, tonsillitis.
Buccal tablet means to be contained in oral cavity and slowly dissolves, and is produced the tablet of local or general action, have the following advantages: act directly on pharyngeal by Sublingual and oral cavity buccal surface mucosa absorption; Due to slowly containing changing, being rested on pharyngeal the medicine energy long period, continuing to play drug effect; For instant effect such as sensation such as discomfort such as alleviation dry pharynx, pharyngalgia etc.; There is the effects such as antibacterial, sterilization, antiinflammatory, detumescence, desaturation thick secretions, convergence, stimulating mucosal secretion, be mainly used in treatment oral cavity, Throat diseases clinically.Buccal tablet is because of its excellent mouthfeel and instructions of taking and be subject to the welcome of extensive patients easily.
Summary of the invention
The object of the invention is to, a kind of compound recipe English lotus buccal tablet and preparation method thereof is provided.This Traditional Chinese medicine lozenge is through extracting obtained extractum and Mentholum, Borneolum Syntheticum for raw material with Herba Taraxaci, Herba Andrographis, Radix Helicteris, Radix Isatidis four taste Chinese crude drug, diluent is maltodextrin, mannitol, lactose, Sorbitol, cane sugar powder, lubricant is micropowder silica gel, correctives is stevioside, cane sugar powder, binding agent is that 65 ~ 75% ethanol waters are made, this buccal tablet smooth surface, uniform color is consistent, refrigerant good to eat, entrance exquisiteness is submissive, it is functional to collapse, and mass discrepancy limit etc. meets Chinese Pharmacopoeia 2010 editions two regulations.
Compound recipe English lotus buccal tablet of the present invention, this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g, diluent is maltodextrin 30 ~ 50g, mannitol 60 ~ 90g, lubricant micropowder silica gel 2 ~ 5g, correctives is the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, and binding agent is that 65 ~ 75% ethanol water 100 ~ 200mL make.
Compound recipe English lotus buccal tablet of the present invention, this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g, diluent is mannitol 50 ~ 80g, lactose 50 ~ 80g, lubricant micropowder silica gel 2 ~ 5g, correctives is the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, and binding agent is that 65 ~ 75% ethanol water 100 ~ 200mL make.
Compound recipe English lotus buccal tablet of the present invention, this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g, diluent is Sorbitol 60 ~ 100g, cane sugar powder 50 ~ 70g, lubricant micropowder silica gel 2 ~ 5g, correctives is 2 ~ 4g stevioside, and binding agent is that 65 ~ 75% ethanol water 100 ~ 200mL make.
The preparation method of described compound recipe English lotus buccal tablet, carry out according to the following steps:
A. Chinese medicine producing process: Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g are pulverized, add the water boiling and extraction 3 times of 8 times amount, first time extracts 3h, and 2h is extracted in second and third time, filter, merge 3 filtrates, filtrate leaves standstill 24h, get supernatant vacuum concentration become relative density be 1.21 ~ 1.28 clear paste (60 ~ 65 DEG C), adding ethanol makes alcohol content reach 65 ~ 70%, leave standstill 48h, filter, filter vacuum is condensed into thick extractum;
B. by diluent maltodextrin, mannitol, lactose, Sorbitol, lubricant micropowder silica gel, correctives stevioside, sucrose are pulverized, and cross 80 ~ 100 mesh sieves, for subsequent use;
C. pressing every 1000 of recipe quantity is radix, get the thick extractum of extraction of step b, add diluent maltodextrin 30 ~ 50g, mannitol 60 ~ 90g or mannitol 50 ~ 80g, lactose 50 ~ 80g or Sorbitol 60 ~ 100g, cane sugar powder 50 ~ 70g, stir, put into less than 60 DEG C, drying baker and be dried to moisture less than 5%, pulverize, cross 120 mesh sieves, add the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, mix in mixer, slowly add wet adhesive 65 ~ 75% ethanol water, constantly stir simultaneously, with high-speed granulator or oscillating granulator soft material, granulate with 18 mesh sieves, soft material is made to become wet granular,
D. wet granular is placed in drying baker lower than 60 DEG C of dryings, stirs 1 time every 0.5h, to accelerate rate of drying, be dried to granule moisture level less than 5%, then with 16 mesh sieve granulate.In granulate material, evenly spray into Mentholum 0.4g, the Borneolum Syntheticum 1.3g alcoholic solution be made up of ethanol in proper amount, be mixed into micropowder silica gel 2 ~ 5g, stir, namely tabletting obtains compound recipe English lotus buccal tablet.
In compound recipe English lotus buccal tablet of the present invention containing the Herba Taraxaci of dose therapeutically effective, Herba Andrographis, Radix Helicteris, Radix Isatidis four taste Chinese crude drug through extracting obtained extractum and Mentholum, Borneolum Syntheticum and being applicable to preparing the pharmaceutical carrier of buccal tablet, described pharmaceutical carrier is selected from: diluent maltodextrin, mannitol, lactose, Sorbitol, sucrose, correctives stevioside, sucrose, binding agent is 65 ~ 75% ethanol waters.
Compound recipe English lotus buccal tablet of the present invention meets Chinese Pharmacopoeia 2010 editions relevant regulations about buccal tablet.
Further illustrate the present invention below in conjunction with example, but application claims protection domain is not limited to following embodiments.
Embodiment 1:
A. Chinese medicine producing process: get and Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g are pulverized, add the water boiling and extraction 3 times of 8 times amount, first time extracts 3h, and 2h is extracted in second and third time, filter, merge 3 filtrates, filtrate leaves standstill 24h, get supernatant vacuum concentration become relative density be 1.21 ~ 1.28 clear paste (60 ~ 65 DEG C), adding ethanol makes alcohol content reach 65 ~ 70%, leave standstill 48h, filter, filter vacuum is condensed into thick extractum;
B. by diluent mannitol, lactose, lubricant micropowder silica gel, correctives stevioside, sucrose are pulverized, and cross 80 ~ 100 mesh sieves, for subsequent use;
C. pressing every 1000 of recipe quantity is radix, get the thick extractum of extraction of step b, add diluent maltodextrin 30 ~ 50g, mannitol 60 ~ 90g, stir, put into less than 60 DEG C, drying baker and be dried to moisture less than 5%, pulverize, cross 120 mesh sieves, add the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, mix in mixer, slowly add wet adhesive 65 ~ 75% ethanol water, constantly stir simultaneously, with high-speed granulator or oscillating granulator soft material, granulate with 18 mesh sieves, make soft material become wet granular;
D. wet granular is placed in drying baker lower than 60 DEG C of dryings, stirs 1 time every 0.5h, to accelerate rate of drying, be dried to granule moisture level less than 5%, then with 16 mesh sieve granulate.In granulate material, evenly spray into Mentholum 0.4g, the Borneolum Syntheticum 1.3g alcoholic solution be made up of ethanol in proper amount, be mixed into micropowder silica gel 2 ~ 5g, stir, namely tabletting obtains compound recipe English lotus buccal tablet.
Embodiment 2:
A. Chinese medicine producing process: get and Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g are pulverized, add the water boiling and extraction 3 times of 8 times amount, first time extracts 3h, and 2h is extracted in second and third time, filter, merge 3 filtrates, filtrate leaves standstill 24h, get supernatant vacuum concentration become relative density be 1.21 ~ 1.28 clear paste (60 ~ 65 DEG C), adding ethanol makes alcohol content reach 65 ~ 70%, leave standstill 48h, filter, filter vacuum is condensed into thick extractum;
B. by diluent maltodextrin, mannitol, lubricant micropowder silica gel, correctives stevioside, sucrose are pulverized, and cross 80 ~ 100 mesh sieves, for subsequent use;
C. pressing every 1000 of recipe quantity is radix, get the thick extractum of extraction of step b, add diluent mannitol 50 ~ 80g, lactose 50 ~ 80g, stir, put into less than 60 DEG C, drying baker and be dried to moisture less than 5%, pulverize, cross 120 mesh sieves, add the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, mix in mixer, slowly add wet adhesive 65 ~ 75% ethanol water, constantly stir simultaneously, with high-speed granulator or oscillating granulator soft material, granulate with 18 mesh sieves, make soft material become wet granular;
D. wet granular is placed in drying baker lower than 60 DEG C of dryings, stirs 1 time every 0.5h, to accelerate rate of drying, be dried to granule moisture level less than 5%, then with 16 mesh sieve granulate.In granulate material, evenly spray into Mentholum 0.4g, the Borneolum Syntheticum 1.3g alcoholic solution be made up of ethanol in proper amount, be mixed into micropowder silica gel 2 ~ 5g, stir, namely tabletting obtains compound recipe English lotus buccal tablet.
Embodiment 3:
A. Chinese medicine producing process: get and Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g are pulverized, add the water boiling and extraction 3 times of 8 times amount, first time extracts 3h, and 2h is extracted in second and third time, filter, merge 3 filtrates, filtrate leaves standstill 24h, get supernatant vacuum concentration become relative density be 1.21 ~ 1.28 clear paste (60 ~ 65 DEG C), adding ethanol makes alcohol content reach 65 ~ 70%, leave standstill 48h, filter, filter vacuum is condensed into thick extractum;
B. by diluent Sorbitol, sucrose, lubricant micropowder silica gel, correctives stevioside is pulverized, and crosses 80 ~ 100 mesh sieves, for subsequent use;
C. pressing every 1000 of recipe quantity is radix, gets the thick extractum of extraction of step b, adds diluent Sorbitol 60 ~ 100g, cane sugar powder 50 ~ 70g, stir, put into less than 60 DEG C, drying baker and be dried to moisture less than 5%, pulverize, cross 120 mesh sieves, add 2 ~ 4g stevioside, mix in mixer, slowly add wet adhesive 65 ~ 75% ethanol water, constantly stir simultaneously, with high-speed granulator or oscillating granulator soft material, granulate with 18 mesh sieves, make soft material become wet granular;
D. wet granular is placed in drying baker lower than 60 DEG C of dryings, stirs 1 time every 0.5h, to accelerate rate of drying, be dried to granule moisture level less than 5%, then with 16 mesh sieve granulate.In granulate material, evenly spray into Mentholum 0.4g, the Borneolum Syntheticum 1.3g alcoholic solution be made up of ethanol in proper amount, be mixed into micropowder silica gel 2 ~ 5g, stir, namely tabletting obtains compound recipe English lotus buccal tablet.
Claims (4)
1. treat acute and chronic pharyngitis, a tonsillitic compound recipe English lotus buccal tablet, it is characterized in that this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g; Diluent is maltodextrin 30 ~ 50g, mannitol 60 ~ 90g; Lubricant micropowder silica gel 2 ~ 5g; Binding agent is 65 ~ 75% ethanol waters; Correctives is that the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form is made.
2. compound recipe English lotus buccal tablet as claimed in claim 1, it is characterized in that this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g; Diluent is mannitol 50 ~ 80g, lactose 50 ~ 80g; Lubricant micropowder silica gel 2 ~ 5g; Binding agent is 65 ~ 75% ethanol waters; Correctives is that the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form is made.
3. compound recipe English lotus buccal tablet as claimed in claim 1, it is characterized in that this buccal tablet with 1000 for radix, raw material is Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g, Mentholum 0.4g, Borneolum Syntheticum 1.3g; Diluent is Sorbitol 60 ~ 100g, cane sugar powder 50 ~ 70g; Lubricant micropowder silica gel 2 ~ 5g; Binding agent is 65 ~ 75% ethanol waters; Correctives is that 2 ~ 4g stevioside is made.
4. the preparation method of the compound recipe English lotus buccal tablet according to claim 1,2,3, is characterized in that carrying out according to the following steps:
A. Chinese medicine producing process: Herba Taraxaci 120g, Herba Andrographis 100g, Radix Helicteris 100g, Radix Isatidis 120g are pulverized, add the water boiling and extraction 3 times of 8 times amount, first time extracts 3h, and 2h is extracted in second and third time, filter, merge 3 filtrates, filtrate leaves standstill 24h, get supernatant vacuum concentration become relative density be 1.21 ~ 1.28 clear paste (60 ~ 65 DEG C), adding ethanol makes alcohol content reach 65 ~ 70%, leave standstill 48h, filter, filter vacuum is condensed into thick extractum;
B. by diluent maltodextrin, mannitol, lactose, Sorbitol, lubricant micropowder silica gel, correctives stevioside, sucrose are pulverized, and cross 80 ~ 100 mesh sieves, for subsequent use;
C. pressing every 1000 of recipe quantity is radix, get the thick extractum of extraction of step b, add diluent maltodextrin 30 ~ 50g, mannitol 60 ~ 90g or mannitol 50 ~ 80g, lactose 50 ~ 80g or Sorbitol 60 ~ 100g, cane sugar powder 50 ~ 70g, stir, put into less than 60 DEG C, drying baker and be dried to moisture less than 5%, pulverize, cross 120 mesh sieves, add the premix material that 2 ~ 4g stevioside and 10 ~ 20g cane sugar powder form, mix in mixer, slowly add wet adhesive 65 ~ 75% ethanol water, constantly stir simultaneously, with high-speed granulator or oscillating granulator soft material, granulate with 18 mesh sieves, soft material is made to become wet granular,
D. wet granular is placed in drying baker lower than 60 DEG C of dryings, stirs 1 time every 0.5h, to accelerate rate of drying, be dried to granule moisture level less than 5%, then with 16 mesh sieve granulate; In granulate material, evenly spray into Mentholum 0.4g, the Borneolum Syntheticum 1.3g alcoholic solution be made up of ethanol in proper amount, be mixed into micropowder silica gel 2 ~ 5g, stir, namely tabletting obtains compound recipe English lotus buccal tablet.
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| CN201510194950.7A CN104800268A (en) | 2015-04-23 | 2015-04-23 | Compound taraxacum mongolicum and andrographis paniculata lozenge for treating laryngopharyngitis and amygdalitis as well as preparation method thereof |
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| CN201510194950.7A CN104800268A (en) | 2015-04-23 | 2015-04-23 | Compound taraxacum mongolicum and andrographis paniculata lozenge for treating laryngopharyngitis and amygdalitis as well as preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106138161A (en) * | 2016-07-15 | 2016-11-23 | 佛山市朗达信息科技有限公司 | One breeding larynx protects throat-fitting buccal tablet and preparation method thereof |
| CN106581206A (en) * | 2016-11-28 | 2017-04-26 | 安徽国顺中药发展有限公司 | Scented tea capable of clearing throat and preparation method of scented tea |
| CN107536890A (en) * | 2017-10-12 | 2018-01-05 | 吉林化工学院 | A kind of double green grass lozenges and preparation method thereof |
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| CN103550274A (en) * | 2013-10-30 | 2014-02-05 | 昆明理工大学 | Oral medicinal preparation |
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| CN103550274A (en) * | 2013-10-30 | 2014-02-05 | 昆明理工大学 | Oral medicinal preparation |
Non-Patent Citations (1)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106138161A (en) * | 2016-07-15 | 2016-11-23 | 佛山市朗达信息科技有限公司 | One breeding larynx protects throat-fitting buccal tablet and preparation method thereof |
| CN106581206A (en) * | 2016-11-28 | 2017-04-26 | 安徽国顺中药发展有限公司 | Scented tea capable of clearing throat and preparation method of scented tea |
| CN107536890A (en) * | 2017-10-12 | 2018-01-05 | 吉林化工学院 | A kind of double green grass lozenges and preparation method thereof |
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Application publication date: 20150729 |