CN104800103B - A kind of double-deck Essence with moisture-keeping efficacy and preparation method and application - Google Patents
A kind of double-deck Essence with moisture-keeping efficacy and preparation method and application Download PDFInfo
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Abstract
The invention belongs to the technical field of cosmetics, a kind of double-deck Essence with moisture-keeping efficacy and preparation method and application is disclosed.The Essence is prepared from by following raw material by mass percentage：The methyl sesquistearates of 0.1%~0.4%PEG 20,0.1%~0.8% Sucrose Polystearic Acid Esters, 2%~6% octyl group polymethyl siloxane, 3%~8% caprylic/capric triglyceride, 3%~6% jojoba oil, 5%~15% glycerine, 2% 6% plant propane diols, 0.02%~0.1%AC YEAST BETA GLUCAN, 1.0% bright peptide antimicrobial fluid, 2% 4%Aquasense CHI and excess waters.Prepared Essence is double-deck stabilising system, with strange visual effect；Formula is gentle non-stimulated, and antiseptic power is good, and moistening effect is good, applied to moisturizing field and skin care industry.
Description
Technical field
The invention belongs to the technical field of cosmetics, and in particular to a kind of double-deck Essence and its system with moisture-keeping efficacy
Preparation Method and application.
Background technology
Cosmetic industry have passed through the development of many decades, have in terms of its dosage system, efficacy effect, security and stability
Great increase and lifting.
From the point of view of formulation development, the moisturizing cream from initial soft petroleum ointment and by emulsion stabilizer of soap base is developed into
Table live body system of today mildy wash, soap base system mildy wash, amino acid system mildy wash and emulsification system mildy wash；Aqua, W/O
Type emulsion, O/W type emulsions；W/o type cream, O/W type creams；Tens of kinds of vanishing cream, BB frosts, skin lotion, elite, gel gel etc.
System.
From the point of view of efficacy effect, only there is moisture-keeping efficacy to develop into whitening and freckle-removing product of today, antiallergic from initial
Product, anti-aging remove wrinkle product, foundation cream class modified product, sunscreen product, cleaning class product, educate hair product, hair dyeing product, hair-waving
Product, depilatory, U.S. milk product, vigorous and graceful product, deodorising product etc..
In terms of security and stability, from the fine chemicals of initial extensive style production by now, from heavy metal originally
It is exceeded, abuse unauthorized substances the specifications for spreading unchecked extremely strict law ＆ policy by now, no matter in terms of regulation or from
From the point of view of the development angle of brand names itself, safety and stability all will be a main trend that can not be reversed.
Cosmetics species is various in the market, but most of elite liquid products are individual layer system, such as：Transparence, emulsion
Shape, the form of product is relatively simple.While the product quality in order to ensure shelf life, most of cosmetics are all added with
Chemical preservative, but preservative has certain excitant, generally anaphylactogen to human body.Also, in order to cover in cosmetics
The peculiar smell of raw material, product can all add certain perfume ingredient.But essence is as preservative, equally have to human body certain
Excitant.
The content of the invention
In order to overcome the shortcoming and defect of prior art, primary and foremost purpose of the invention is to provide a kind of with moisture-keeping efficacy
Double-deck Essence.
Another object of the present invention is to provide the preparation method of above-mentioned double-deck Essence.
It is still another object of the present invention to provide the application of above-mentioned double-deck Essence.
The purpose of the present invention is achieved through the following technical solutions：
A kind of double-deck Essence with moisture-keeping efficacy, is made up of following raw material by mass percentage：0.1%~
It is 0.4%PEG-20 methyls sesquistearate (SSE-20), 0.1%~0.8% Sucrose Polystearic Acid Esters, 2%~6% pungent
Base polymethyl siloxane, 3%~8% caprylic/capric triglyceride (318RC), 3%~6% jojoba oil, 5%~15% is sweet
It is oil, 2%-6% plants propane diols (ActiveDM PG-V), 0.02%~0.1%AC YEAST BETA-GLUCAN, 1.0% bright
Peptide antimicrobial fluid, 2%-4%Aquasense CHI and excess water.
The preparation method of the double-deck Essence, comprises the following steps：
(1) by PEG-20 methyls sesquistearate, Sucrose Polystearic Acid Esters, octyl group polymethyl siloxane, octanoic acid/
Triglyceride DDD, jojoba oil are placed in container, and stirring is warming up to 75 DEG C~85 DEG C, and insulation is standby, obtains oil phase raw material；
(2) glycerine, AC YEAST BETA-GLUCAN, ActiveDM PG-V and water are placed in container, stirring heating
To 80 DEG C~90 DEG C, insulation is standby, obtains Aqueous Phase Raw Material；
(3) Aqueous Phase Raw Material is added in emulsifying homogeneous device, stirring is opened, under conditions of 80 DEG C~85 DEG C, by oil phase
Raw material is slowly sucked in emulsifier unit, obtains mixed liquor；Mixed liquor is then subjected to high speed homogenization；
(4) after the completion of homogeneous, it is constant to be kept stirring for speed, cooling；Bright peptide antimicrobial fluid, Aquasense CHI are subsequently added,
Stirring, discharging, obtains double-deck Essence.
The speed stirred described in step (1) is 800~1000r/min；The soaking time is 10~15min.
The speed stirred described in step (2) is 800~1000r/min；The soaking time is 15~20min.
Speed of agitator described in step (3) is 300r/min~900r/min；The homogeneous speed of the high speed homogenization is
1000~4000r/min；The homogenizing time is 5s~30s.
The temperature cooled down described in step (4) is 35 DEG C~40 DEG C；The mixing time is 15min~20min.
Described Essence initial appearance is white emulsion, is changed into bottom after standing for transparency liquid, and top is white breast
Liquid, after shaking up still can natural subsidence be double-deck stabilising system；PH is 6.5~7.5, and viscosity is≤200mpa.s, 45 DEG C heat-resisting 24
Hour, it is still double-deck stabilising system to recover after room temperature, is changed into stable white emulsion after jog is even, -18 DEG C are cold-resistant 24 hours,
It is still white stable homogeneous system to recover after room temperature.
Application of the described double-deck Essence in moisturizing field and skin care industry.
PEG-20 methyl sesquistearates：Purchased from Lubrizol companies of the U.S., HLB value is 15.3, saponification number
[mgKOH/g]：40.0-50.0, acid number [mgKOH/g]：≤ 1.50, hydroxyl value [mgKOH/g]：95.0-110.0, iodine number [g I2/
100g]：≤1.0；From natural products glucose, with it is gentle non-stimulated the characteristics of, its emulsifying capacity is strong in addition, obtained
Product light is fine and smooth, soft comfortable, has natural moisture preserving.
Sucrose Polystearic Acid Esters：Source is that plant, sucrose ester content are 78%-85%, and hydrocarbons content is 15-
20%, HLB value is about 8.0；Hydroxyl value [mgKOH/g]：15.0-20.0, acid number [mgKOH/g]：≤15.0；More stearic composition
Containing three esters, four esters or even higher ester, the characteristic with good profit amphiphilic.
Octyl group polymethyl siloxane：Purchased from Momentive companies of the U.S., refraction index (20 DEG C)：1.4105-1.4145,
Viscosity (25 DEG C) [cSt]：2.40-3.40；Improve the sticky sense of product, there is provided the excellent of soft silk quality for increase product spread
Skin sense.
Caprylic/capric triglyceride：Purchased from BASF Corp. of Germany, acid number [mgKOH/g]：≤ 0.2, saponification number [mgKOH/
g]：325-360, hydroxyl value [mgKOH/g]：≤ 0.1, density (20 DEG C) [g/ml]：0.930-0.960, index of refraction (20 DEG C)：
1.440-1.451。
ActiveDM PG-V (are purchased from ADM companies of the U.S.)：The propane diols of plant origin；From soybean and cocoa bean
Grease, with mellow scent.
AC YEAST BETA-GLUCAN (are purchased from Active Concepes companies of the U.S.)：From Saccharomyces cerevisiae β-
Glucan；Non-derived beta glucan is originated, and molecular weight has good water-soluble between 200k dalton and 500k dalton
Property；With anti-inflammatory reparation and excellent moistening effect.
Bright peptide antimicrobial fluid：Natural pickles filter liquor, is that American ACT IVE CONCEPTS companies utilize biotechnology from South Korea
Isolated antibacterial peptide in the leukonid of pickles.
Aquasense CHI (are purchased from CHEMYUNION companies of Brazil)：Main component be water, butanediol and galactolipin I
Uncle's sugar.
The present invention be using between W/O and O/W HLB as 8.0 Sucrose Polystearic Acid Esters be main emulsified component, while with
The PEG-20 methyls sesquistearate of a small amount of high hlb (15.3) is to help emulsified component so that essence prepared by the present invention
Magnificent liquid has relatively unique double-deck system, and Sucrose Polystearic Acid Esters can make emulsified body formation stratiform liquid crystal structure, have
Long-acting moisture-retaining capacity；Again by skin-moisturizing, skin of octyl group polymethyl siloxane, caprylic/capric triglyceride and jojoba oil into
Point, the spreadabilities of three kinds of compositions reduces successively, moisten degree increases successively, and by the way that these three heterogeneities are carried out into phase lap
With soft, the unimpeded pore that can make it that the Essence of the present invention can become skin when keeping preferable spreadability, go back simultaneously
With preferable moisture-keeping efficacy；The regeneration of cell (is promoted with glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN again
And growth, the effect with cell repair), Aquasense CHI be that composition is repaired in moisturizing, wherein Aquasense CHI have
By promoting the synthesis of aquaporin, increase the quantity and glycerol content of epidermis NMF, with instant and long
The moistening effect of effect, and extracellular matrix also has preferable repairing effect, to safeguard good skin barrier function, comprehensively
Improve skin state；Finally it is aided with bright peptide antimicrobial fluid.By the way that these compositions are passed through into strict emulsifying process, so as to obtain ultralow
The double-deck system with moisture-keeping efficacy and preferable antiseptic property of viscosity is double-deck Essence.
Compared with prior art, the present invention has advantages below and beneficial effect：
1st, double-deck Essence of the invention has good, permanent moistening effect.
2nd, relatively existing system, the present invention is that (upper end is white emulsion shape to the viscous double-deck system of novel super-low, and lower floor is transparent
Phase), can be uniform under jog is several when using with strange visual effect, convenient use.
3rd, the present invention carry out formulation composition optimization, without essence, without anti-corrosion etc. potentially stimulate anaphylactogen, formula as mild as a dove
It is non-stimulated.
Embodiment
With reference to embodiment, the present invention is described in further detail, but the implementation of the present invention is not limited to this.
Embodiment 1
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate, Sucrose Polystearic Acid Esters, octyl group polymethyl siloxane,
Caprylic/capric triglyceride, jojoba oil are placed in A beakers, and stirring is warming up to 75 DEG C (mixing speed is 800r/min), are incubated
5min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN and water are placed in B beakers, are stirred
Mix and be warming up to 80 DEG C (mixing speed is 800r/min), be incubated 5min；
3rd, stirring (speed of agitator is 300r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 10s is finished down), opened
Open homogenizer and carry out homogeneous, speed 1800r/min, homogenizing time is 15s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 35 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 15min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.4, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 2.0:8.0, hyaline layer has
It is a little muddy.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and lower transparent
Liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 2
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate, Sucrose Polystearic Acid Esters, octyl group polymethyl siloxane,
Caprylic/capric triglyceride, jojoba oil are placed in A beakers, and stirring is warming up to 80 DEG C (mixing speed is 900r/min), are incubated
7min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are placed in B beakers, stirring
It is warming up to 82 DEG C (mixing speed is 900r/min), is incubated 7min；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 10s is finished down), opened
Open homogenizer and carry out homogeneous, speed 1800r/min, 15s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 17min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.3, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 4.5:5.5, hyaline layer
Transparency is preferable.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and bottom
Transparency liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 3
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate, Sucrose Polystearic Acid Esters, octyl group polymethyl siloxane
(silsoft034), caprylic/capric triglyceride, jojoba oil be in A beakers, and stirring is warming up to 85 DEG C, and (mixing speed is
1000r/min), it is incubated 10min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 10min to 85 DEG C (mixing speed is 1000r/min)；
3rd, stirring (speed of agitator is 900r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 15s is finished down), opened
Open homogenizer and carry out homogeneous, speed 1800r/min, 15s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 40 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 20min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.1, and viscosity is 100mpa.s；It is quiet by 24h under normal temperature
Put, Essence is divided into top white emulsion and lower transparent liquid, the height ratio of white layer and hyaline layer is 7.0:3.0, it is transparent
The transparency of layer is preferable.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, be divided into top white emulsion and
Lower transparent liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 4
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane (silsoft034), caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C of (stirrings
Speed is 900r/min), it is incubated 8min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 8min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 20s is finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 1000r/min, 15s
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 17min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 1.8:8.2, hyaline layer has
It is a little muddy.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and lower transparent
Liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 5
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane (silsoft034), caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C of (stirrings
Speed is 900r/min), it is incubated 12min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 17min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 20s is finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 2000r/min, 15s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 17min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 4.0:6.0, hyaline layer has
It is a little muddy.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and bottom is saturating
Prescribed liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 6
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane (silsoft034), caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C of (stirrings
Speed is 900r/min), it is incubated 12min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 17min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 20s is finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 4000r/min, and homogenizing time is 15s
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 17min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 7.5:2.5, hyaline layer has
It is a little muddy.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and bottom is saturating
Prescribed liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 7
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane (silsoft034), caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C of (stirrings
Speed is 900r/min), it is incubated 12min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 17min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (moon, 20s was finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 2000r/min, and homogenizing time is 5s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid (AMS
Leucidal Liquid), Aquasense CHI, stir 17min, discharge it is filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 1.5:8.5, hyaline layer has
It is a little muddy.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and bottom is saturating
Prescribed liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 8
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane (silsoft034), caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C of (stirrings
Speed is 900r/min), it is incubated 12min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 17min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 20s is finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 2000r/min, and homogenizing time is 10s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid, Aquasense
CHI, stirs 17min, discharges filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 4.7:5.3, hyaline layer
Transparency is preferable.Centrifugation test (3000r/min, 30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and bottom
Transparency liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
Embodiment 9
A kind of double-deck Essence without anti-corrosion without essence with moisture-keeping efficacy：
The preparation method of the Essence：
1st, accurate weighing PEG-20 methyls sesquistearate (SSE-20), Sucrose Polystearic Acid Esters, the poly- first of octyl group
Radical siloxane, caprylic/capric triglyceride, jojoba oil are in A beakers, and stirring is warming up to 80 DEG C, and (mixing speed is 900r/
Min), it is incubated 12min；
2nd, accurate weighing glycerine, ActiveDM PG-V, AC YEAST BETA-GLUCAN, water are in B beakers, and stirring rises
Temperature is incubated 17min to 82 DEG C (mixing speed is 900r/min)；
3rd, stirring (speed of agitator is 600r/min) is opened, A beaker raw materials are slowly poured into B beakers (about 20s is finished down), opened
Open high-shear homogenizer and carry out homogeneous, homogeneous speed is 2000r/min, and homogenizing time is 30s；
4th, after the completion of homogeneous, it is constant to be kept stirring for speed, is naturally cooling to 37 DEG C, adds bright peptide antimicrobial fluid, Aquasense
CHI, stirs 17min, discharges filling.
The Essence outward appearance just prepared is white emulsion, and PH is 7.2, and viscosity is 60mpa.s；Stood under normal temperature by 24h,
Essence is divided into top white emulsion and lower transparent liquid, and the height ratio of white layer and hyaline layer is 9.0:1.0.Centrifugation test
(3000r/min,30min)：Without water-oil separating without precipitation, it is divided into top white emulsion and lower transparent liquid.
Heat resistance is tested：The Essence just prepared is positioned in 45 DEG C of environment heat-resisting 24 hours, no water-oil separating without
Precipitation, is divided into top white emulsion and lower transparent liquid.
Cold tolerance is tested：The Essence just prepared is positioned in -18 DEG C of environment and resisted cold 24 hours, recovers essence after room temperature
Magnificent liquid is still white emulsion.
From the embodiment 1~9 given, optimal white layer and transparent layer height ratio are close to 1:1 is the most suitable, and just
For transparency, embodiment 8 is better than embodiment 5.
Comparative example
Comparative example a：SSE-20 is lacked, other compositions, consumption and production technology are same as Example 8, as a result show
Show that the transparent oil reservoir in upper strata (water-oil separating) occurs in heat-resisting test, do not reach double-deck stabilising system；
Comparative example b：Aquasense CHI are lacked, other compositions, consumption and production technology are same as Example 8,
As a result show that pH, normal temperature stand every physical and chemical indexs such as 24h, heat-resisting cold-resistant test roughly the same with embodiment 8；
Comparative example c：Only Aquasense CHI and water, wherein Aquasense CHI：9g, water：291g, production
Technique is same as Example 8, and it is clear homogeneous liquid as a result to show the mixture；
Comparative example d：Water：300g.
Performance of keeping humidity test, test knot are carried out to embodiment 8, comparative example b, comparative example c, comparative example d
Fruit is as shown in table 1：
Table 1：Performance of keeping humidity is tested
Subject number of cases n=96, the time on probation is 4 weeks, and upper table data are on probation preceding and corresponding index after tested 4 weeks flat
Average；
Moisture value reflects keratoderma water content, and keratoderma moisture is more sufficient, is worth bigger；
Percutaneous water loss value reflection speed of the deep skin moisture through skin losses, keratoderma barrier function is got over
It is good, it is worth smaller；P value≤0.05, it is believed that there were significant differences before on probation and after trying out.
Preservative challenge testing is carried out to embodiment 8, test result is as shown in table 2：
Table 2：Antiseptic property is tested：
Detection method：American Pharmacopeia USP32 (51) antimicrobial preservation efficacy test
Bacterium：Pseudomonas aeruginosa (Pseudomonas aeruginosa) ATCC 9027
ETEC (Escherichia coli) ATCC 8739
Staphylococcus aureus (Staphylococcus aureus) ATCC 6538
Mould and saccharomycete：Candida albicans (Candida albicans) ATCC 10231
Aspergillus niger (Aspergillus niger) ATCC 16404
As a result show, the control ability of the microorganism of the product is good.
Above-described embodiment is preferably embodiment, but embodiments of the present invention are not by above-described embodiment of the invention
Limitation, other any Spirit Essences without departing from the present invention and the change made under principle, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (6)
1. a kind of double-deck Essence with moisture-keeping efficacy, it is characterised in that：Prepared by following raw material by mass percentage
Form：0.1%~0.4% PEG-20 methyls sesquistearate, 0.1%~0.8% Sucrose Polystearic Acid Esters,
2%~6% octyl group polymethyl siloxane, 3%~8% caprylic/capric triglyceride, 3%~6% jojoba oil, 5%
~15% glycerine, 2%-6% ActiveDM PG-V, 0.02%~0.1% AC YEAST BETA-GLUCAN, 1.0%
Bright peptide antimicrobial fluid, 2%-4% Aquasense CHI and excess water；
The ActiveDM PG-V are the propane diols of plant origin；The AC YEAST BETA-GLUCAN are Saccharomyces cerevisiae
The beta glucan in source；The Aquasense CHI, its main component is water, butanediol and galactolipin arabinose.
2. there is the preparation method of the double-deck Essence of moisture-keeping efficacy according to claim 1, it is characterised in that：Including following
Step：
(1) by PEG-20 methyls sesquistearate, Sucrose Polystearic Acid Esters, octyl group polymethyl siloxane, caprylic/capric
Triglycerides, jojoba oil are placed in container, and stirring is warming up to 75 DEG C~85 DEG C, and insulation is standby, obtains oil phase raw material；
(2) glycerine, AC YEAST BETA-GLUCAN, ActiveDM PG-V and water are placed in container, stirring is warming up to 80
DEG C~90 DEG C, insulation is standby, obtains Aqueous Phase Raw Material；
(3) Aqueous Phase Raw Material is added in emulsifying homogeneous device, stirring is opened, under conditions of 80 DEG C~85 DEG C, by oil phase raw material
In slow suction emulsifier unit, mixed liquor is obtained；Mixed liquor is then subjected to high speed homogenization；
(4) after the completion of homogeneous, it is constant to be kept stirring for speed, cooling；Bright peptide antimicrobial fluid, Aquasense CHI are subsequently added, is stirred
Mix, discharge, obtain double-deck Essence.
3. there is the preparation method of the double-deck Essence of moisture-keeping efficacy according to claim 2, it is characterised in that：Step (1)
Described in the speed that stirs be 800~1000r/min；The soaking time is 10~15min.
4. there is the preparation method of the double-deck Essence of moisture-keeping efficacy according to claim 2, it is characterised in that：Step (2)
Described in the speed that stirs be 800~1000r/min；The soaking time is 15~20min.
5. there is the preparation method of the double-deck Essence of moisture-keeping efficacy according to claim 2, it is characterised in that：Step (3)
Described in high speed homogenization homogeneous speed be 1000~4000r/min；The homogenizing time is 5s~30s；Described in step (3)
Speed of agitator is 300~900r/min.
6. there is the preparation method of the double-deck Essence of moisture-keeping efficacy according to claim 2, it is characterised in that：Step (4)
Described in the temperature that cools down be 35 DEG C~40 DEG C；The mixing time is 15min~20min.
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| CN106389194B (en) * | 2016-09-05 | 2019-03-22 | 上海萧雅生物科技股份有限公司 | Bilayer with the light line effect of moisturizing skin lightening is sprayed essence and preparation method thereof |
| CN106361634A (en) * | 2016-09-14 | 2017-02-01 | 广东丸美生物技术股份有限公司 | Multiple essence with effects of moisturizing, whitening and anti-aging, and preparation method and application thereof |
| CN107198675B (en) * | 2017-04-20 | 2020-02-14 | 广东丸美生物技术股份有限公司 | Double-layer essence with repairing and anti-aging effects and preparation method thereof |
| CN109528557B (en) * | 2018-12-28 | 2022-01-28 | 澳宝化妆品（惠州）有限公司 | A dual-layer skin care spray composition with low swelling to plastic container |
| CN111568778B (en) * | 2020-06-19 | 2023-02-03 | 上海新高姿化妆品有限公司 | Three-layer essence with skin modification and nourishing effects, and preparation method and application thereof |
| CN111743789B (en) * | 2020-07-22 | 2023-05-05 | 广州玥颜化妆品有限公司 | Double-layer moisturizing essence and preparation method thereof |
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| CN1420760A (en) * | 1999-11-08 | 2003-05-28 | 宝洁公司 | Cosmetic compositions |
| CN103494714A (en) * | 2013-10-16 | 2014-01-08 | 广东轻工职业技术学院 | Emulsifier composition capable of forming liquid crystal structure and application of emulsifier composition |
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| KR101803902B1 (en) * | 2011-09-16 | 2017-12-04 | (주)아모레퍼시픽 | Composition for skin external application containing ceramide |
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| CN1420760A (en) * | 1999-11-08 | 2003-05-28 | 宝洁公司 | Cosmetic compositions |
| CN103494714A (en) * | 2013-10-16 | 2014-01-08 | 广东轻工职业技术学院 | Emulsifier composition capable of forming liquid crystal structure and application of emulsifier composition |
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