CN104798863A - Collagen casing and preparation method thereof - Google Patents
Collagen casing and preparation method thereof Download PDFInfo
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- CN104798863A CN104798863A CN201410758235.7A CN201410758235A CN104798863A CN 104798863 A CN104798863 A CN 104798863A CN 201410758235 A CN201410758235 A CN 201410758235A CN 104798863 A CN104798863 A CN 104798863A
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- casing
- cladding
- sausages
- collagen
- dietary fiber
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- A—HUMAN NECESSITIES
- A22—BUTCHERING; MEAT TREATMENT; PROCESSING POULTRY OR FISH
- A22C—PROCESSING MEAT, POULTRY, OR FISH
- A22C13/00—Sausage casings
- A22C13/0013—Chemical composition of synthetic sausage casings
- A22C13/0016—Chemical composition of synthetic sausage casings based on proteins, e.g. collagen
Abstract
The invention discloses a collagen casing and its preparation method. The collagen casing is composed of the following ingredients, by weight, 55-65% of collagen, 4-8% of soybean dietary fiber, 4-8% of high amylose modified starch, 0.02-0.05% of a cross-linking agent, 3-10% of a plasticizer, 0.01-0.03% of an antiseptic and 15-25% of water. The collagen casing provided by the invention has advantages of small casing thickness, smooth and crispy taste, good permeability, high tensile strength, high compression strength, high stretching rate, high temperature boiling resistance and the like. As auxiliary materials of the collagen casing are soybean dietary fiber and high amylose modified starch, the collagen casing has high safety, high nutritive value, strong film-forming property and good heat stability, is low-cost, and has a certain air permeability and moisture-penetrability. Due to the functionality, the collagen casing completely can replace other edible celluloses of synthetic chemical materials and can meet requirements of mechanical coloclysis.
Description
Technical field
The present invention relates to food processing field, particularly, relate to a kind of Collagent casing for sausages and preparation method thereof.
Background technology
Use various casing, such as hog intestine, the natural casing such as sheep casing, beef casing in a large number in sausage manufacturing industry, and the artificial casing such as nylon casing, PVDC casing, cellulose sausage casing and Collagent casing for sausages.Natural casing is mainly from animals such as pig, sheep, oxen, and its casing caliber size is not identical, and size is different in size to be caused, and quality is also different, causes being not suitable for mechanization bowel lavage, needs artificial bowel lavage, and production cost is high.Artificial casing raw material mainly comes from petrochemical industry, and oil belongs to non-renewable resources, and also very easily pollutes environment when producing artificial casing raw material, and in addition, artificial casing can not be degraded, contaminated environment.At present, Collagent casing for sausages is used widely gradually, its mainly with the collagen fabric of pig, ox-hide corium for raw material, add auxiliary material, make collagen dough through chemistry and mechanical treatment, then be made through techniques such as extruding, inflation, drying, heat-shapings.But in existing Collagent casing for sausages, auxiliary material adds assorted many, and security is lower.
Soybean dietary fiber is the fiber product adopting state-of-the-art technology to extract from the cell membrane of soybean seed leaf, there is multinomial physiological function, energy prevention of obesity and diabetes, prevent colon cancer, high fat of blood, heart disease, the necessary soybean protein of human body can also be supplemented simultaneously, by health is required, be called as " human body the 7th nutrient ".The character that soybean dietary fiber is special according to it, be widely applied in various meat products, beverage and health products, but by soybean dietary fiber and high straight chain converted starch and animal collagen by certain auxiliary agent, processing is combined with each other, make a kind of mechanical strength large, resistance to boiling, good product quality, meet the edible collagen casing of the fillings food recording various local flavor, be still in blank at present at home and abroad.
The Collagent casing for sausages being auxiliary material with soybean dietary fiber and high straight chain converted starch has mouthfeel sliding crisp, gas permeability is strong, the advantages such as digestion resistant, simultaneously because casing thickness is little, pull-off force is large, and compressive resistance is high, and expansion and contraction is large, be more suitable for mechanization production, can farthest save production cost simultaneously.Therefore, the advantage of the Collagent casing for sausages being auxiliary material with soybean dietary fiber and high straight chain converted starch will inevitably make it replace natural casing and artificial casing, will obtain the welcome in market in the future.
Summary of the invention
The present invention mainly solves auxiliary material in existing Collagent casing for sausages and adds the technical problem many, security is low of mixing.
In order to solve the problems of the technologies described above, the embodiment of the invention discloses a kind of Collagent casing for sausages, its constituent comprise mass percent be 55% ~ 65% collagen, 4% ~ 8% soybean dietary fiber, 4% ~ 8% high straight chain converted starch, 0.02% ~ 0.05% crosslinking agent, the plasticizer of 3% ~ 10%, the anticorrisive agent of 0.01% ~ 0.03% and 15% ~ 25% water.
In a kind of preferred embodiment of the present invention, its constituent comprise mass percent be 60% collagen, 7.5% soybean dietary fiber, 7.5% high straight chain converted starch, 0.03% crosslinking agent, the plasticizer of 5%, the anticorrisive agent of 0.02% and 18% water.
In a kind of preferred embodiment of the present invention, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1.
In a kind of preferred embodiment of the present invention, described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3.
In a kind of preferred embodiment of the present invention, described anticorrisive agent comprises potassium sorbate.
Meanwhile, the present invention also provides a kind of preparation method of Collagent casing for sausages, comprises the steps:
Cladding segmentation, liming: animal dermis layer is divided into bulk, after clear water is cleaned, soak 5 ~ 20 days with saturated limewater, then cleaned up by cladding with clear water;
Acidifying Peng Run: the hydrochloric acid solution of the cladding after liming process with 0.09 ~ 0.11N is soaked 24 ~ 72 hours, and constantly stirs, then venting acid solution, with clean water cladding more than at least twice;
De-fine: the cladding after acidifying Peng Run to be carried out defiber process, and grinds to form collagen tablet;
Mix and rub filtration: dropped in vacuum kneading-and machine by described collagen tablet, Hun Rou limit, limit adds soybean dietary fiber, high straight chain converted starch and water, obtains collagenous fibres group, then filters;
Extruded: the collagenous fibres after filtering to be rolled into a ball after extruding, inflating, obtains tubulose casing;
Modification plasticising: described tubulose casing is dry under 40 ~ 50 degrees Celsius, sprays the mixed liquor of crosslinking agent, plasticizer and anticorrisive agent simultaneously, obtains Collagent casing for sausages finished product.
In a kind of preferred embodiment of the present invention, described acidifying is splashed in profit step, and control ph is between 2.5 ~ 3.5.
In a kind of preferred embodiment of the present invention, described mixing is rubbed in filtration step, and the addition of soybean dietary fiber accounts for 4% ~ 8% of cladding butt quality, and it is 3.0 ~ 4.0 that the addition of high straight chain converted starch accounts for 4% ~ 8%, pH of cladding butt quality.
In a preferred embodiment of the present invention, described mixing is rubbed in filtration step, and soybean dietary fiber is more than 140 orders, and high straight chain converted starch is more than 100 orders.
In a kind of preferred embodiment of the present invention, in described modification plasticizing step, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1; Described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3; Described anticorrisive agent comprises potassium sorbate.
Compared to prior art, the present invention with the Fibrilla collagen of animal dermis layer for major ingredient, be auxiliary material in conjunction with soybean dietary fiber and high straight chain converted starch, adopt the Collagent casing for sausages that special process processes, there is casing thickness little, mouthfeel is sliding crisp, good permeability, tensile strength is large, compressive resistance is high, the advantages such as expansion and contraction height and digestion resistant, its auxiliary material is soybean dietary fiber and high straight chain converted starch, not only security is high, and be of high nutritive value, cost is low, film forming is strong, Heat stability is good, also there is certain gas permeability and poisture-penetrability simultaneously, its functional edibility cellulose that can substitute other synthesis class industrial chemicals completely, meet the requirement of mechanization bowel lavage.
Detailed description of the invention
Be clearly and completely described the technical scheme in the embodiment of the present invention below, obviously, described embodiment is only a part of embodiment of the present invention, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making other embodiments all obtained under creative work prerequisite, belong to the scope of protection of the invention.
The invention provides a kind of Collagent casing for sausages, its constituent comprise mass percent be 55% ~ 65% collagen, 4% ~ 8% soybean dietary fiber, 4% ~ 8% high straight chain converted starch, 0.02% ~ 0.05% crosslinking agent, the plasticizer of 3% ~ 10%, the anticorrisive agent of 0.01% ~ 0.03% and 15% ~ 25% water.
Preferably, its constituent comprise mass percent be 60% collagen, 7.5% soybean dietary fiber, 7.5% high straight chain converted starch, 0.03% crosslinking agent, the plasticizer of 5%, the anticorrisive agent of 0.02% and 18% water.
Further, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1.
Described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3.
Described anticorrisive agent comprises potassium sorbate.
Correspondingly, the present invention also provides a kind of preparation method of Collagent casing for sausages, specifically implements according to following steps:
Step S1, cladding segmentation, liming: sorted by cladding size, thin and thick by animal dermis layer, be divided into the homogeneous bulky of size 5cm × 10cm, after clear water is cleaned, soak 5 ~ 20 days with saturated limewater, then cleaned up by cladding with clear water;
Step S2, acidifying Peng Run: the hydrochloric acid solution of the cladding after liming process with 0.09 ~ 0.11N is soaked 24 ~ 72 hours, and constantly stirs, control ph is between 2.5 ~ 3.5, cladding is made to become soft, translucent expansion shape, then venting acid solution, with clean water cladding more than at least twice;
Step S3, de-fine: the cladding after acidifying Peng Run to be carried out defiber process, and grinds to form collagen tablet;
Step S4, mix and rub filtration: described collagen tablet is dropped in vacuum kneading-and machine, Hun Rou limit, limit adds soybean dietary fiber, high straight chain converted starch and water, mix and rub 2 ~ 5 hours time, obtain collagenous fibres group, collagenous fibres group can mix further through homogenizer, and pH value is 3.0 ~ 4.0, then filters through high-pressure filteration machine;
Wherein soybean dietary fiber is more than 140 orders, and its addition accounts for 4% ~ 8% of cladding butt quality, and high straight chain converted starch is more than 100 orders, and its addition accounts for 4% ~ 8% of cladding butt quality.
Step S5, extruded: proceed in extruder by the collagenous fibres group after filtering, pressure is 15 ~ 30MPa, after extruding, inflating, obtains tubulose casing;
Step S6, modification plasticising: described tubulose casing is sent into drying line, dry under 40 ~ 50 degrees Celsius, spray the mixed liquor of crosslinking agent, plasticizer and anticorrisive agent simultaneously, drying line is gone out after abundant drying, flatten through machinery, refolding winding or the rear packaging of cover contracting, can obtain Collagent casing for sausages finished product.
Wherein, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1; Described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3; Described anticorrisive agent comprises potassium sorbate.Preferably, described crosslinking agent accounts for 0.1% ~ 0.3% of cladding butt quality, and described plasticizer accounts for 8% ~ 12% of cladding butt quality, and described anticorrisive agent accounts for 0.05% ~ 0.15% of cladding butt quality.
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
Step S1, cladding segmentation, liming: by ox-hide skin corium by size, thin and thick sorts, cut into the homogeneous bulky of size 5cm × 10cm, get cladding 1000kg, after clear water is cleaned, be placed in saturated limewater to soak 15 days, stirred 10 minutes every 30 minutes in immersion process, then with clear water, cladding is cleaned up;
Step S2, acidifying Peng Run: the hydrochloric acid solution of the cladding 0.10N after liming process is soaked 30 hours, and constantly stir, control ph is between 2.5 ~ 3.0, cladding is made to become soft, translucent expansion shape, and extruding cladding makes fiber definition visible, then venting acid solution, with clean water cladding more than at least twice;
Step S3, de-fine: the cladding after acidifying Peng Run to be dropped into fiber peeling-off machine and carries out defiber process, and grind to form collagen tablet;
Step S4, mix and rub filtration: described collagen tablet is dropped in vacuum kneading-and machine, Hun Rou limit, limit adds 37.5kg soybean dietary fiber, 37.5kg height straight chain converted starch and appropriate water, mix and rub 2 ~ 5 hours time, obtain collagenous fibres group, collagenous fibres group can mix further through homogenizer, and pH value is 3.0 ~ 4.0, then filters through high-pressure filteration machine;
Step S5, extruded: proceed in extruder by the collagenous fibres group after filtering, pressure is 20MPa, after extruding, inflating, obtains the tubulose casing that bore is 21mm;
Step S6, modification plasticising: described tubulose casing is sent into drying line, dry under 40 degrees Celsius, spray the mixed liquor be made up of 1kg crosslinking agent, 50kg plasticizer and 0.5kg anticorrisive agent simultaneously, drying line is gone out after abundant drying, flatten through machinery, refolding winding or the rear packaging of cover contracting, can obtain Collagent casing for sausages finished product.
The Collagent casing for sausages that the present embodiment is obtained, detects through sampling: casing thickness is 0.025mm, and longitudinal pull-off force is 21N, and compressive resistance is 0.03MPa, and boiling dilatability is that 18%, 80 DEG C of boilings, 30 minutes nothings are melted, broken.
Embodiment 2
Step S1, cladding segmentation, liming: by ox-hide skin corium by size, thin and thick sorts, cut into the homogeneous bulky of size 5cm × 10cm, get cladding 2000kg, after clear water is cleaned, be placed in saturated limewater to soak 16 days, stirred 10 minutes every 30 minutes in immersion process, then with clear water, cladding is cleaned up;
Step S2, acidifying Peng Run: the hydrochloric acid solution of the cladding 0.10N after liming process is soaked 36 hours, and constantly stir, control ph is between 2.5 ~ 3.0, cladding is made to become soft, translucent expansion shape, and extruding cladding makes fiber definition visible, then venting acid solution, with clean water cladding more than at least twice;
Step S3, de-fine: the cladding after acidifying Peng Run to be dropped into fiber peeling-off machine and carries out defiber process, and grind to form collagen tablet;
Step S4, mix and rub filtration: described collagen tablet is dropped in vacuum kneading-and machine, Hun Rou limit, limit adds 75kg soybean dietary fiber, 75kg height straight chain converted starch and appropriate water, mix and rub 2 ~ 5 hours time, obtain collagenous fibres group, collagenous fibres group can mix further through homogenizer, and pH value is 3.0 ~ 4.0, then filters through high-pressure filteration machine;
Step S5, extruded: proceed in extruder by the collagenous fibres group after filtering, pressure is 25MPa, after extruding, inflating, obtains the tubulose casing that bore is 23mm;
Step S6, modification plasticising: described tubulose casing is sent into drying line, dry under 45 degrees Celsius, spray the mixed liquor be made up of 2kg crosslinking agent, 100kg plasticizer and 1kg anticorrisive agent simultaneously, drying line is gone out after abundant drying, flatten through machinery, refolding winding or the rear packaging of cover contracting, can obtain Collagent casing for sausages finished product.
The Collagent casing for sausages that the present embodiment is obtained, detects through sampling: casing thickness is 0.024mm, and longitudinal pulling force is 24N, and compressive resistance is 0.04MPa, and boiling dilatability is that 20%, 80 DEG C of boilings, 30 minutes nothings are melted, broken.
Embodiment 3
Step S1, cladding segmentation, liming: by ox-hide skin corium by size, thin and thick sorts, cut into the homogeneous bulky of size 5cm × 10cm, get cladding 2500kg, after clear water is cleaned, be placed in saturated limewater to soak 16 days, stirred 10 minutes every 30 minutes in immersion process, then with clear water, cladding is cleaned up;
Step S2, acidifying Peng Run: the hydrochloric acid solution of the cladding 0.10N after liming process is soaked 38 hours, and constantly stir, control ph is between 2.5 ~ 3.0, cladding is made to become soft, translucent expansion shape, and extruding cladding makes fiber definition visible, then venting acid solution, with clean water cladding more than at least twice;
Step S3, de-fine: the cladding after acidifying Peng Run to be dropped into fiber peeling-off machine and carries out defiber process, and grind to form collagen tablet;
Step S4, mix and rub filtration: described collagen tablet is dropped in vacuum kneading-and machine, Hun Rou limit, limit adds 93.75kg soybean dietary fiber, 93.75kg height straight chain converted starch and appropriate water, mix and rub 2 ~ 5 hours time, obtain collagenous fibres group, collagenous fibres group can mix further through homogenizer, and pH value is 3.0 ~ 4.0, then filters through high-pressure filteration machine;
Step S5, extruded: proceed in extruder by the collagenous fibres group after filtering, pressure is 25MPa, after extruding, inflating, obtains the tubulose casing that bore is 26mm;
Step S6, modification plasticising: described tubulose casing is sent into drying line, dry under 45 degrees Celsius, spray the mixed liquor be made up of 2.5kg crosslinking agent, 125kg plasticizer and 1.25kg anticorrisive agent simultaneously, drying line is gone out after abundant drying, flatten through machinery, refolding winding or the rear packaging of cover contracting, can obtain Collagent casing for sausages finished product.
The Collagent casing for sausages that the present embodiment is obtained, detects through sampling: casing thickness is 0.025mm, and longitudinal pulling force is 23N, and compressive resistance is 0.05MPa, and boiling dilatability is that 21%, 80 DEG C of boilings, 30 minutes nothings are melted, broken.
The soybean dietary fiber adopted in embodiment 1 ~ 3 and high straight chain converted starch are commercially available, wherein soybean dietary fiber is more than 140 orders, high straight chain converted starch is more than 100 orders, described crosslinking agent is glutaraldehyde and calcium chloride, the mass ratio of glutaraldehyde and calcium chloride is 4:1, described plasticizer is oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3, and described anticorrisive agent is potassium sorbate.
Compared to prior art, the present invention with the Fibrilla collagen of animal dermis layer for major ingredient, be auxiliary material in conjunction with soybean dietary fiber and high straight chain converted starch, adopt the Collagent casing for sausages that special process processes, there is casing thickness little, mouthfeel is sliding crisp, good permeability, tensile strength is large, compressive resistance is high, the advantages such as expansion and contraction height and digestion resistant, its auxiliary material is soybean dietary fiber and high straight chain converted starch, not only security is high, and be of high nutritive value, cost is low, film forming is strong, Heat stability is good, also there is certain gas permeability and poisture-penetrability simultaneously, its functional edibility cellulose that can substitute other synthesis class industrial chemicals completely, meet the requirement of mechanization bowel lavage.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every utilize description of the present invention to do equivalent structure or equivalent flow process conversion; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.
Claims (10)
1. a Collagent casing for sausages, it is characterized in that, its constituent comprise mass percent be 55% ~ 65% collagen, 4% ~ 8% soybean dietary fiber, 4% ~ 8% high straight chain converted starch, 0.02% ~ 0.05% crosslinking agent, the plasticizer of 3% ~ 10%, the anticorrisive agent of 0.01% ~ 0.03% and 15% ~ 25% water.
2. Collagent casing for sausages according to claim 1, it is characterized in that, its constituent comprise mass percent be 60% collagen, 7.5% soybean dietary fiber, 7.5% high straight chain converted starch, 0.03% crosslinking agent, the plasticizer of 5%, the anticorrisive agent of 0.02% and 18% water.
3. Collagent casing for sausages according to claim 1, is characterized in that, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1.
4. Collagent casing for sausages according to claim 1, is characterized in that, described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3.
5. Collagent casing for sausages according to claim 1, is characterized in that, described anticorrisive agent comprises potassium sorbate.
6. a preparation method for Collagent casing for sausages, for the preparation of Collagent casing for sausages as claimed in claim 1, is characterized in that, described preparation method comprises the steps:
Cladding segmentation, liming: animal dermis layer is divided into bulk, after clear water is cleaned, soak 5 ~ 20 days with saturated limewater, then cleaned up by cladding with clear water;
Acidifying Peng Run: the hydrochloric acid solution of the cladding after liming process with 0.09 ~ 0.11N is soaked 24 ~ 72 hours, and constantly stirs, then venting acid solution, with clean water cladding more than at least twice;
De-fine: the cladding after acidifying Peng Run to be carried out defiber process, and grinds to form collagen tablet;
Mix and rub filtration: dropped in vacuum kneading-and machine by described collagen tablet, Hun Rou limit, limit adds soybean dietary fiber, high straight chain converted starch and water, obtains collagenous fibres group, then filters;
Extruded: the collagenous fibres after filtering to be rolled into a ball after extruding, inflating, obtains tubulose casing;
Modification plasticising: described tubulose casing is dry under 40 ~ 50 degrees Celsius, sprays the mixed liquor of crosslinking agent, plasticizer and anticorrisive agent simultaneously, obtains Collagent casing for sausages finished product.
7. the preparation method of Collagent casing for sausages according to claim 6, is characterized in that, described acidifying is splashed in profit step, and control ph is between 2.5 ~ 3.5.
8. the preparation method of Collagent casing for sausages according to claim 6, it is characterized in that, described mixing is rubbed in filtration step, the addition of soybean dietary fiber accounts for 4% ~ 8% of cladding butt quality, it is 3.0 ~ 4.0 that the addition of high straight chain converted starch accounts for 4% ~ 8%, pH of cladding butt quality.
9. the preparation method of Collagent casing for sausages according to claim 8, is characterized in that, described mixing is rubbed in filtration step, and soybean dietary fiber is more than 140 orders, and high straight chain converted starch is more than 100 orders.
10. the preparation method of Collagent casing for sausages according to claim 6, is characterized in that, in described modification plasticizing step, described crosslinking agent comprises glutaraldehyde and calcium chloride, and the mass ratio of glutaraldehyde and calcium chloride is 4:1; Described plasticizer comprises oleic acid and glycerine, and the mass ratio of oleic acid and glycerine is 1:3; Described anticorrisive agent comprises potassium sorbate.
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| CN105104493A (en) * | 2015-08-06 | 2015-12-02 | 梧州神冠蛋白肠衣有限公司 | Preparation method of collagen casings |
| CN106035598A (en) * | 2016-07-01 | 2016-10-26 | 陈永红 | Edible casings prepared from collagen and other edible proteins |
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| CN109996444A (en) * | 2016-10-21 | 2019-07-09 | 阿特兰提斯－帕克生产商业有限公司 | Gauffer carries the moisture-proof casing and its manufacturing method of bar form at rigidity certainly |
| CN112471217A (en) * | 2020-11-25 | 2021-03-12 | 山东海奥斯生物科技有限公司 | Preparation method of fresh collagen casing |
| CN112931578A (en) * | 2021-02-05 | 2021-06-11 | 天津科技大学 | Preparation method of nanocellulose reinforced collagen casing |
| CN113475557A (en) * | 2021-07-14 | 2021-10-08 | 江南大学 | Preparation method of fried type collagen casing |
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| CN112471217A (en) * | 2020-11-25 | 2021-03-12 | 山东海奥斯生物科技有限公司 | Preparation method of fresh collagen casing |
| CN112931578A (en) * | 2021-02-05 | 2021-06-11 | 天津科技大学 | Preparation method of nanocellulose reinforced collagen casing |
| CN113475557A (en) * | 2021-07-14 | 2021-10-08 | 江南大学 | Preparation method of fried type collagen casing |
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