Summary of the invention
For the defect existed in prior art, the object of the present invention is to provide a kind of cassia seed oral liquid of Chinese wolfberry and preparation method thereof, high to the recovery rate of active component in cassia seed and matrimony vine, product good health care effect.
For reaching above object, the technical scheme that the present invention takes is: a kind of preparation method of cassia seed oral liquid of Chinese wolfberry, comprises the following steps:
S1. take the cassia seed of certain mass, add the pure water of 60 DEG C, soak after 1 hour, then add casein-sodium, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain cassia seed magma;
S2. take the dried fruit of lycium barbarum of certain mass, add pure water, soak after 12 hours, then add casein-sodium and soybean lecithin, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
S3. cassia seed magma and matrimony vine magma are put into refiner, add xanthans, carry out homogenized;
S4. by the solution sterilization after homogenate, filling, cassia seed oral liquid of Chinese wolfberry is namely made.
On the basis of technique scheme, in step S1, the casein-sodium quality added is 0.3 ~ 0.5% of cassia seed quality.
On the basis of technique scheme, in step S1, the casein-sodium quality added is 0.4% of cassia seed quality.
On the basis of technique scheme, in step S2, the casein-sodium quality added is 0.3 ~ 0.4% of dried fruit of lycium barbarum quality, and the soybean lecithin quality added is 0.05 ~ 0.1% of dried fruit of lycium barbarum quality.
On the basis of technique scheme, in step S2, the casein-sodium quality added is 0.33% of dried fruit of lycium barbarum quality, and the soybean lecithin quality added is 0.083% of dried fruit of lycium barbarum quality.
On the basis of technique scheme, in step S3, the xanthans quality added is 0.005 ~ 0.01% of cassia seed magma and matrimony vine magma gross mass.
On the basis of technique scheme, in step S3, the xanthans quality added is 0.0082% of cassia seed magma and matrimony vine magma gross mass.
On the basis of technique scheme, specifically comprise the following steps:
S1. take 500 grams of cassia seeds, add the pure water of 2 liters 60 DEG C, soak after 1 hour, then add 2 grams of casein-sodiums, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain cassia seed magma;
S2. take 600 grams of dried fruit of lycium barbarum, add 3 liters of pure water, soak after 12 hours, then add 2 grams of casein-sodiums and 0.5 gram of soybean lecithin, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
S3. cassia seed magma and matrimony vine magma are put into refiner, add 0.5 gram of xanthans, carry out homogenized;
S4. by the solution sterilization after homogenate, filling, cassia seed oral liquid of Chinese wolfberry is namely made.
On the basis of technique scheme, specifically comprise the following steps:
S1. take 500 grams of cassia seeds, add the pure water of 2 liters 60 DEG C, soak after 1 hour, then add 1.5 grams of casein-sodiums, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain cassia seed magma;
S2. take 600 grams of dried fruit of lycium barbarum, add 3 liters of pure water, soak after 12 hours, then add 1.8 grams of casein-sodiums and 0.3 gram of soybean lecithin, put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
S3. cassia seed magma and matrimony vine magma are put into refiner, add 0.3 gram of xanthans, carry out homogenized;
S4. by the solution sterilization after homogenate, filling, cassia seed oral liquid of Chinese wolfberry is namely made.
A kind of cassia seed oral liquid of Chinese wolfberry, adopts described preparation method to make.
Beneficial effect of the present invention is:
1. the present invention soaks 1 hour with the pure water of 60 DEG C at cassia seed before making beating, and adds casein-sodium, can by the fat-soluble active ingredient emulsification in cassia seed, fully to extract; Before matrimony vine making beating, add casein-sodium and soybean lecithin, by the fat-soluble active ingredient in matrimony vine, can particularly have the luteole emulsification of protection retina effect, fully to extract, high to the recovery rate of active component in cassia seed and matrimony vine.Cassia seed and matrimony vine these two kinds are had the natural health care source conbined usage of good function of improving eyesight by this preparation method, give play to best eyesight-improving health care function effect, can also be improved the health simultaneously, strengthen memory, fall " three is high ", and product good health care effect, often drinks good for health.
2, the oral liquid that obtains of the present invention adopts sterilizing to pack, and has good buffer action to light and air, and effective active can be avoided to go bad, and is easy to store, is easy to carry, can takes by accurate quantification, is very popular a kind of health food edible way.
Detailed description of the invention
The active component of cassia seed comprises Anthraquinones, the naphtho--lipid-soluble active such as pyrrolones, fatty acid composition, and these compounds are insoluble in water, if do not carry out emulsification, direct slurrying, can cause active component content in cassia seed magma low.
The active component of matrimony vine comprises containing polysaccharide and flavonoids, and these compounds are insoluble in water equally, if do not carry out emulsification, direct slurrying, just fully cannot extract the fat-soluble active ingredient, particularly luteole of matrimony vine, active component content in matrimony vine magma can be caused low.
Casein-sodium is as food additives, security is high, the general permission to use in countries in the world, there is good emulsification, fat-soluble active ingredient in cassia seed or matrimony vine and casein-sodium generation physical reactions, casein-sodium molecule has hydrophilic radical and hydrophobic grouping respectively, hydrophobic group is inserted into fat-soluble active ingredient inside, hydrophilic radical is exposed, thus fat-soluble active ingredient is distributed in water and keeps long-time stable, thus the fat-soluble active ingredient in cassia seed or matrimony vine is extracted in water.In addition, casein-sodium emulsion also can not destroy its stability and functional under l20 DEG C of high-temperature sterilization, can ensure that oral liquid in the end can not occur rotten by Yin Gaowen in sterilization filling process.
The embodiment of the present invention provides a kind of cassia seed oral liquid of Chinese wolfberry and preparation method thereof, and preparation method of the present invention comprises the following steps:
S1. the cassia seed of certain mass is taken, add the pure water of 60 DEG C, soak after 1 hour, add casein-sodium again, can by the fat-soluble active ingredient emulsification in cassia seed, fully to extract, the casein-sodium Functionality, quality and appealing design added elects 0.3 ~ 0.5% of cassia seed quality as, and this addition is better to the fat-soluble active ingredient emulsifying effectiveness in cassia seed; Put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain cassia seed magma.The main component of cassia seed magma comprises Anthraquinones, naphtho--fat-soluble active ingredient such as pyrrolones, fatty acid, comprises amino acids and inorganic elements etc. in addition.In above process, if add casein-sodium after slurrying, then casein-sodium fully cannot contact with cassia seed and carry out emulsification, therefore, must add casein-sodium before cassia seed slurrying, guarantee casein-sodium and cassia seed in pulping process fully contact and carry out emulsification.
S2. the dried fruit of lycium barbarum of certain mass is taken, add pure water, soak after 12 hours, add casein-sodium and soybean lecithin again, casein-sodium and soybean lecithin can by the fat-soluble active ingredients in matrimony vine, particularly there is the luteole emulsification of protection retina effect, fully to extract, the casein-sodium Functionality, quality and appealing design added elects 0.3 ~ 0.4% of dried fruit of lycium barbarum quality as, the soybean lecithin Functionality, quality and appealing design added elects 0.05 ~ 0.1% of dried fruit of lycium barbarum quality as, and this addition is better to the fat-soluble active ingredient emulsifying effectiveness in matrimony vine; Put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma.Containing all active components of matrimony vine in matrimony vine magma, comprise LBP-X class and the large active component of flavonoids two, in addition containing multivitamin and amino acid and the composition such as carrotene, luteole.
S3. cassia seed magma and matrimony vine magma are put into refiner, add xanthans, carry out homogenized, xanthans is the stabilizing agent of oral liquid, ensure that oral liquid there will not be precipitation in a long time, the xanthans Functionality, quality and appealing design added elects 0.005 ~ 0.01% of cassia seed magma and matrimony vine magma gross weight as, and stablizing effect is now best;
S4. by the solution sterilization after homogenate, filling, cassia seed oral liquid of Chinese wolfberry of the present invention is namely made.
Below in conjunction with 3 embodiments, the present invention is described in further detail.
Embodiment 1:
Cassia seed oral liquid of Chinese wolfberry is prepared by following process:
Step 101. takes 500 grams of cassia seeds, add the pure water of 2 liters 60 DEG C, soak after 1 hour, add 2 grams of casein-sodiums (the casein-sodium quality added is 0.4% of cassia seed quality) again, put into beater slurrying, slurries are filtered, is filtered to without after precipitation, obtains cassia seed magma;
Step 102. takes 600 grams of dried fruit of lycium barbarum, add 3 liters of pure water, soak after 12 hours, (the casein-sodium quality added is 0.33% of dried fruit of lycium barbarum quality to add 2 grams of casein-sodiums and 0.5 gram of soybean lecithin again, the soybean lecithin quality added is 0.083% of dried fruit of lycium barbarum quality), put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
Cassia seed magma after filtration and matrimony vine magma are put into refiner by step 103., add 0.5 gram of xanthans (the xanthans quality added is 0.0082% of cassia seed magma and matrimony vine magma gross weight), carry out homogenized;
Step 104., by the solution sterilization after homogenate, filling, namely makes cassia seed oral liquid of Chinese wolfberry.
Embodiment 2:
Cassia seed oral liquid of Chinese wolfberry is prepared by following process:
Step 201. takes 500 grams of cassia seeds, add the pure water of 2 liters 60 DEG C, soak after 1 hour, add 1.5 grams of casein-sodiums (the casein-sodium quality added is 0.3% of cassia seed quality) again, put into beater slurrying, slurries are filtered, is filtered to without after precipitation, obtains cassia seed magma;
Step 202. takes 600 grams of dried fruit of lycium barbarum, add 3 liters of pure water, soak after 12 hours, (the casein-sodium quality added is 0.3% of dried fruit of lycium barbarum quality to add 1.8 grams of casein-sodiums and 0.3 gram of soybean lecithin again, the soybean lecithin quality added is 0.05% of dried fruit of lycium barbarum quality), put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
Cassia seed magma after filtration and matrimony vine magma are put into refiner by step 203., add 0.3 gram of xanthans (the xanthans quality added is 0.005% of cassia seed magma and matrimony vine magma gross weight), carry out homogenized;
Step 204., by the solution sterilization after homogenate, filling, namely makes cassia seed oral liquid of Chinese wolfberry.
Embodiment 3:
Cassia seed oral liquid of Chinese wolfberry is prepared by following process:
Step 301. takes 500 grams of cassia seeds, add the pure water of 2 liters 60 DEG C, soak after 1 hour, add 2.5 grams of casein-sodiums (the casein-sodium quality added is 0.5% of cassia seed quality) again, put into beater slurrying, slurries are filtered, is filtered to without after precipitation, obtains cassia seed magma;
Step 302. takes 600 grams of dried fruit of lycium barbarum, add 3 liters of pure water, soak after 12 hours, (the casein-sodium quality added is 0.4% of dried fruit of lycium barbarum quality to add 2.4 grams of casein-sodiums and 0.6 gram of soybean lecithin again, the soybean lecithin quality added is 0.1% of dried fruit of lycium barbarum quality), put into beater slurrying, slurries are filtered, be filtered to without after precipitation, obtain matrimony vine magma;
Cassia seed magma after filtration and matrimony vine magma are put into refiner by step 303., add 0.61 gram of xanthans (the xanthans quality added is 0.01% of cassia seed magma and matrimony vine magma gross weight), carry out homogenized;
Step 304., by the solution sterilization after homogenate, filling, namely makes cassia seed oral liquid of Chinese wolfberry.
Comparative example:
Cassia seed oral liquid of Chinese wolfberry is prepared by following process:
Step 401. takes 500 grams of cassia seeds, adds the pure water of 2 liters 60 DEG C, soaks after 1 hour, puts into beater slurrying, filter slurries, is filtered to without after precipitation, obtains cassia seed magma;
Step 402. takes 600 grams of dried fruit of lycium barbarum, adds 3 liters of pure water, soaks after 12 hours, puts into beater slurrying, filter slurries, is filtered to without after precipitation, obtains matrimony vine magma;
Cassia seed magma after filtration and matrimony vine magma are put into refiner by step 403., add 0.5 gram of xanthans and carry out homogenized;
Step 404., by the solution sterilization after homogenate, filling, namely makes cassia seed oral liquid of Chinese wolfberry.
Can be found by the cassia seed magma in detection embodiment 1 ~ 3 and comparative example and the active component in matrimony vine magma:
Most important active component in the cassia seed magma that the embodiment of the present invention 1 ~ 3 is obtained, cassia seed fat-soluble active ingredient content is 1% ~ 3%; Do not add casein-sodium in comparative example, direct slurrying, in the cassia seed magma that comparative example obtains, the content of cassia seed fat-soluble active ingredient only has 0.1% ~ 0.3%.Through comparative analysis: in the cassia seed magma that the embodiment of the present invention 1 ~ 3 is obtained, the content of cassia seed fat-soluble active ingredient is approximately 10 times of comparative example, effectively can improve the recovery rate of active component in cassia seed.
Most important active component in the matrimony vine magma that the embodiment of the present invention 1 ~ 3 is obtained, luteole content is greater than 0.01%; Casein-sodium and soybean lecithin is not added, direct slurrying, hardly containing luteole in the matrimony vine magma that comparative example is obtained in comparative example.Through comparative analysis: the embodiment of the present invention 1 ~ 3 effectively can improve the recovery rate of active component in matrimony vine.
The present invention is not limited to above-mentioned embodiment, and for those skilled in the art, under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications are also considered as within protection scope of the present invention.The content be not described in detail in this description belongs to the known prior art of professional and technical personnel in the field.