CN104773966B - Preparation method of binding material mix - Google Patents
Preparation method of binding material mix Download PDFInfo
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- CN104773966B CN104773966B CN201510157047.3A CN201510157047A CN104773966B CN 104773966 B CN104773966 B CN 104773966B CN 201510157047 A CN201510157047 A CN 201510157047A CN 104773966 B CN104773966 B CN 104773966B
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Abstract
The invention discloses a preparation method of a binding material mix mainly prepared from aluminum oxygen chamotte. The main raw material of the binding material mix is aluminum oxygen chamotte. The preparation method of the binding material mix mainly prepared from aluminum oxygen chamotte is characterized in that the raw materials (by weight) include aluminum oxygen chamotte, calcined alunite, zinc sulfate, dickite, attapulgus clay, coal ash, zeolite powder, kieselguhr, bentonite, methylcellulose, sodium sulfite, quick lime, sodium tripolyphosphate, borax and calcium chloride. The binding material mix mainly prepared from aluminum oxygen chamotte has the functions of efficient water resistance, moisture resistance, expandability, crack resistance, leak resistance and the like and does not corrode reinforcing steel bars.
Description
Technical field
The present invention relates to a kind of preparation method of Binder Materials mix, the glue especially with aluminum oxide clinker as primary raw material
The preparation method of gel material mix, belongs to building material manufacture field.
Background technology
In engineering, many building basements, roofing, highway, bridge all do not reach design service life, and some engineerings are only
Come into operation several years just by heavy damage it has to be repaired, its main cause is current waterproof material and concrete
Additive generally contains Cl-、K+Ion is overweight, is added in concrete, reacts with active silica in concrete, generates alkali
Silicate gel and produce concrete swelling cracking, here it is common alkali-aggregate reaction in engineering, accelerate to steel bar corrosion simultaneously,
Concrete cracking is led to seep water.
Content of the invention
The purpose of the present invention is to overcome the deficiencies in the prior art, provide one kind have high-effective water-proof, protection against the tide, expansion, cracking resistance,
The preparation method of the Binder Materials mix with aluminum oxide clinker as primary raw material of the function such as impervious.
For achieving the above object, the technical solution used in the present invention is as follows：
A kind of preparation method of Binder Materials mix, with aluminum oxide clinker as primary raw material, its feature exists described mix
In：
Described preparation method step is：
Step (1)：Glue according to 22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite, attapulgite
6 parts of soil, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite, 1.5 parts of methylcellulose, 0.8 part of sodium sulfite,
0.8 part of quick lime, 0.3 part of sodium tripolyphosphate, 0.5 part of Borax, 0.6 part of proportioning of calcium chloride prepares raw material,
Step (2)：22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite are entered in flour mill
Row grinding, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 6 parts of attapulgite clay, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite in grinding
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm in machine,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machine
Tool mixes 1 hour, pours 1.5 parts of methylcellulose, 0.8 part of sodium sulfite, 0.8 part of quick lime, sodium tripolyphosphate 0.3 afterwards into
Part, 0.5 part of Borax, 0.6 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials with aluminum oxide clinker as primary raw material and mix
Close material.
A kind of preparation method of the Binder Materials mix with aluminum oxide clinker as primary raw material, described mix is ripe with alumina
Expect for primary raw material, it is characterized in that：
Described preparation method step is：
Step (1)：Glue according to 24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite, attapulgite
9 parts of soil, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite, 1.5 parts of methylcellulose, 0.9 part of sodium sulfite,
0.9 part of quick lime, 0.4 part of sodium tripolyphosphate, 0.6 part of Borax, 0.7 part of proportioning of calcium chloride prepares raw material,
Step (2)：24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite are entered in flour mill
Row grinding, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 9 parts of attapulgite clay, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite in grinding
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm in machine,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machine
Tool mixes 1 hour, pours 1.5 parts of methylcellulose, 0.9 part of sodium sulfite, 0.9 part of quick lime, sodium tripolyphosphate 0.4 afterwards into
Part, 0.6 part of Borax, 0.7 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials with aluminum oxide clinker as primary raw material and mix
Close material.
The preparation method of described Binder Materials mix, step（2）Obtaining mixture A granularity size is 0.7mm.
The preparation method of described Binder Materials mix, step（3）Obtaining mixture B granularity size is 0.25mm.
The preparation method of described Binder Materials mix, attapulgite clay composition is（Weight）：56.7%SiO2、16.8%
MgO、 3.4%FeO 、5.5%Fe2O3、9.1%Al2O3, 2.7%CaO, 5.8% loss on ignition.
The preparation method of described Binder Materials mix, dickite composition is（Weight）：61.1%SiO2、31.3%
Al2O3、1.2%Fe2O3, 1.1%CaO, 0.5%MgO, 4.8% loss on ignition.
The preparation method of described Binder Materials mix, fine coal ash component is（Weight）：53.3%SiO2、29.7%
Al2O3、5.3%Fe2O3, 2.1%CaO, 4.8%MgO, 4.8% loss on ignition.
Compared with prior art, the present invention has the advantages that：
The preparation of test specimen：Using cement 282g, the Binder Materials with aluminum oxide clinker as primary raw material prepared are mixed
Close material 18g, sand 750g, water consumption 120ml, and molding 40 × 40 × 160mm test specimen, in 20 ± 2 DEG C of temperature, humidity be 90% with
Maintenance under conditions of upper.
The Binder Materials mix being obtained with aluminum oxide clinker as primary raw material is substituted 6 of cement amount in cement-based material
Quality % mixes in cement-based material, makes 20 pieces of test blocks, and the average index of the properties of 20 pieces of test blocks of detection is：Fineness
(specific surface area)：410m2/kg, setting time：Pre-hardening 115min final set 300min, limited expansion rate：7d-0.024%；28d-
0.015%, comprcssive strength：7d：32.3Mpa；28d：50.3MPa, permeated height ratio：32%, water demand ratio：66%, to reinforcing bar
Action of rust：Non-corroding.The Binder Materials mix with aluminum oxide clinker as primary raw material for building of the present invention has efficiently to be prevented
Water, protection against the tide, expansion, cracking resistance, the function such as impervious, act on to reinforcing bar non-corroding, are the big technological break-through of current architectural waterproof material one.
Specific embodiment
Embodiment 1
A kind of preparation method of the Binder Materials mix with aluminum oxide clinker as primary raw material it is characterised in that：
Described preparation method step is：
Step (1)：Glue according to 22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite, attapulgite
6 parts of soil, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite, 1.5 parts of methylcellulose, 0.8 part of sodium sulfite,
0.8 part of quick lime, 0.3 part of sodium tripolyphosphate, 0.5 part of Borax, 0.6 part of proportioning of calcium chloride prepares raw material,
Step (2)：22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite are entered in flour mill
Row grinding, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 6 parts of attapulgite clay, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite in grinding
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm in machine,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machine
Tool mixes 1 hour, pours 1.5 parts of methylcellulose, 0.8 part of sodium sulfite, 0.8 part of quick lime, sodium tripolyphosphate 0.3 afterwards into
Part, 0.5 part of Borax, 0.6 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials with aluminum oxide clinker as primary raw material and mix
Close material.
Embodiment 2
A kind of preparation method of the Binder Materials mix with aluminum oxide clinker as primary raw material it is characterised in that：
Described preparation method step is：
Step (1)：Glue according to 24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite, attapulgite
9 parts of soil, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite, 1.5 parts of methylcellulose, 0.9 part of sodium sulfite,
0.9 part of quick lime, 0.4 part of sodium tripolyphosphate, 0.6 part of Borax, 0.7 part of proportioning of calcium chloride prepares raw material,
Step (2)：24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite are entered in flour mill
Row grinding, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 9 parts of attapulgite clay, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite in grinding
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm in machine,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machine
Tool mixes 1 hour, pours 1.5 parts of methylcellulose, 0.9 part of sodium sulfite, 0.9 part of quick lime, sodium tripolyphosphate 0.4 afterwards into
Part, 0.6 part of Borax, 0.7 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials with aluminum oxide clinker as primary raw material and mix
Close material.
Claims (2)
1. a kind of preparation method of Binder Materials mix, described mix with aluminum oxide clinker as primary raw material it is characterised in that：
Described preparation method step is：
Step (1)：According to 22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite, attapulgite clay 6
Part, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite, 1.5 parts of methylcellulose, 0.8 part of sodium sulfite, calculogenesis
0.8 part of ash, 0.3 part of sodium tripolyphosphate, 0.5 part of Borax, 0.6 part of proportioning of calcium chloride prepares raw material,
Step (2)：22 parts of aluminum oxide clinker, 18 parts of calcined alunite, 9 parts of zinc sulfate, 6 parts of dickite are carried out powder in flour mill
Mill, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 6 parts of attapulgite clay, 6 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 4 parts of bentonite in flour mill
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machinery is mixed
Close 1 hour, pour 1.5 parts of methylcellulose, 0.8 part of sodium sulfite, 0.8 part of quick lime, 0.3 part of sodium tripolyphosphate, boron afterwards into
0.5 part of sand, 0.6 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials mix with aluminum oxide clinker as primary raw material.
2. a kind of preparation method of the Binder Materials mix with aluminum oxide clinker as primary raw material, described mix is with aluminum oxide clinker
For primary raw material it is characterised in that：
Described preparation method step is：
Step (1)：According to 24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite, attapulgite clay 9
Part, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite, 1.5 parts of methylcellulose, 0.9 part of sodium sulfite, calculogenesis
0.9 part of ash, 0.4 part of sodium tripolyphosphate, 0.6 part of Borax, 0.7 part of proportioning of calcium chloride prepares raw material,
Step (2)：24 parts of aluminum oxide clinker, 19 parts of calcined alunite, 9 parts of zinc sulfate, 7 parts of dickite are carried out powder in flour mill
Mill, rotating speed is 120r/min, grinding 6 hours, and obtaining mixture A granularity size is 0.5-1mm,
Step (3)：By 9 parts of attapulgite clay, 9 parts of flyash, 4 parts of zeolite powder, 3 parts of kieselguhr, 3 parts of bentonite in flour mill
Carry out grinding, rotating speed is 100r/min, grinding 2 hours, obtaining mixture B granularity size is 0.2-0.3mm,
Step (4)：By step（2）Obtain mixture A and by step（3）Obtain mixture B and load in mechanical mixer, machinery is mixed
Close 1 hour, pour 1.5 parts of methylcellulose, 0.9 part of sodium sulfite, 0.9 part of quick lime, 0.4 part of sodium tripolyphosphate, boron afterwards into
0.6 part of sand, 0.7 part of calcium chloride, then mechanical mixture 2 hours, obtain the Binder Materials mix with aluminum oxide clinker as primary raw material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510157047.3A CN104773966B (en) | 2014-02-09 | 2014-02-09 | Preparation method of binding material mix |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510157047.3A CN104773966B (en) | 2014-02-09 | 2014-02-09 | Preparation method of binding material mix |
| CN201410045670.5A CN103880321B (en) | 2014-02-09 | 2014-02-09 | A kind of take aluminum oxide clinker as the preparation method of the gelling material mixed material of main raw material |
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| CN201410045670.5A Division CN103880321B (en) | 2014-02-09 | 2014-02-09 | A kind of take aluminum oxide clinker as the preparation method of the gelling material mixed material of main raw material |
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| CN104773966A CN104773966A (en) | 2015-07-15 |
| CN104773966B true CN104773966B (en) | 2017-02-22 |
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| CN201510157047.3A Active CN104773966B (en) | 2014-02-09 | 2014-02-09 | Preparation method of binding material mix |
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| CN201410045670.5A Expired - Fee Related CN103880321B (en) | 2014-02-09 | 2014-02-09 | A kind of take aluminum oxide clinker as the preparation method of the gelling material mixed material of main raw material |
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| CN106746874A (en) * | 2015-11-20 | 2017-05-31 | 甘肃曼特睿尔公路材料研发有限责任公司 | A kind of cement additire and preparation method thereof |
| CN107601987A (en) * | 2017-10-09 | 2018-01-19 | 安徽新瑞重工股份有限公司 | A kind of precast floor slab special cracking resistant concrete |
| CN108793790A (en) * | 2018-09-03 | 2018-11-13 | 浙江新都水泥有限公司 | A method of cement being prepared in rotary kiln using quick lime |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051032A (en) * | 1989-10-17 | 1991-05-01 | 中国建筑材料科学研究院 | Rapid hardening agent of concrete |
| KR20020052828A (en) * | 2000-12-26 | 2002-07-04 | 신현준 | Refractory composition |
| CN1990413A (en) * | 2005-12-27 | 2007-07-04 | 尹小林 | Synthesis-reactivation technique for preparing inorganic coagulation material |
| CN102584089A (en) * | 2012-03-05 | 2012-07-18 | 河南理工大学 | Formula for enhanced accelerating agent |
| CN102863171A (en) * | 2012-10-09 | 2013-01-09 | 遵义市恒新化工有限公司 | Cement concrete accelerator |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100276795B1 (en) * | 1998-06-12 | 2001-02-01 | 이헌구 | Manufacturing method of waterproofing agent for concrete with excellent waterproofing |
| CN103435286B (en) * | 2013-08-28 | 2015-02-04 | 欧阳湘新 | Method for producing accelerating agent by using red mud |
-
2014
- 2014-02-09 CN CN201410045670.5A patent/CN103880321B/en not_active Expired - Fee Related
- 2014-02-09 CN CN201510157047.3A patent/CN104773966B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051032A (en) * | 1989-10-17 | 1991-05-01 | 中国建筑材料科学研究院 | Rapid hardening agent of concrete |
| KR20020052828A (en) * | 2000-12-26 | 2002-07-04 | 신현준 | Refractory composition |
| CN1990413A (en) * | 2005-12-27 | 2007-07-04 | 尹小林 | Synthesis-reactivation technique for preparing inorganic coagulation material |
| CN102584089A (en) * | 2012-03-05 | 2012-07-18 | 河南理工大学 | Formula for enhanced accelerating agent |
| CN102863171A (en) * | 2012-10-09 | 2013-01-09 | 遵义市恒新化工有限公司 | Cement concrete accelerator |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103880321A (en) | 2014-06-25 |
| CN103880321B (en) | 2016-01-20 |
| CN104773966A (en) | 2015-07-15 |
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| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Huang Guochun Inventor after: Yu Heng Inventor after: Xi Yajie Inventor before: Huang Xiaoxian |
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| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20170103 Address after: 226601 Haian, Jiangsu, Haian County town, Nanhai Road, No. 88, No. Applicant after: Nantong Kodak building materials limited-liability company Address before: 100003 Beijing Meteor Garden District, building 2, unit 301, room, room 1, No. 2 Applicant before: Huang Xiaoxian |
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| CP01 | Change in the name or title of a patent holder |
Address after: 226601 No.88 Nanhai Avenue, Hai'an town, Hai'an County, Nantong City, Jiangsu Province Patentee after: Nantong Keda Building Materials Technology Co.,Ltd. Address before: 226601 No.88 Nanhai Avenue, Hai'an town, Hai'an County, Nantong City, Jiangsu Province Patentee before: NANTONG KEDA BUILDING MATERIALS Co.,Ltd. |