CN104770864A - Heat-clearing and throat-wetting electronic spray solution and preparation method thereof - Google Patents

Heat-clearing and throat-wetting electronic spray solution and preparation method thereof Download PDF

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Publication number
CN104770864A
CN104770864A CN201510075672.3A CN201510075672A CN104770864A CN 104770864 A CN104770864 A CN 104770864A CN 201510075672 A CN201510075672 A CN 201510075672A CN 104770864 A CN104770864 A CN 104770864A
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spire
extract
fresh
mono
dragon well
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CN201510075672.3A
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CN104770864B (en
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华健
欧阳灿
周艳
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Shenzhen Vatican living life science Limited by Share Ltd
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华健
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/70Carbohydrates; Sugars; Derivatives thereof
    • A61K31/7028Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages
    • A61K31/7034Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin
    • A61K31/704Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin attached to a condensed carbocyclic ring system, e.g. sennosides, thiocolchicosides, escin, daunorubicin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/738Rosa (rose)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicinal Preparation (AREA)
  • Tea And Coffee (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a heat-clearing and throat-wetting electronic spray solution and a preparation method thereof. The heat-clearing and throat-wetting electronic spray solution mainly comprises the following ingredients: 0.1-2%w/w of blumea balsamifera (l.) dc. oil, 15-60%w/w of propanediol, 15-60%w/w of glycerol, 0.1-0.3%w/w of mono-ammonium glycyrrhizinate, 1-3%w/w of fresh rosa roxburghii juice, 1-3%w/w of a dragon thin leaf extract and 1-5%w/w of an edible essence. The heat-clearing and throat-wetting electronic spray solution ensures that people can enjoy an emulational smoking effect and the comfort degree and the health of the throat are guaranteed.

Description

Electronic atomized liquid that a kind of heat-clearing wets one's whistle and preparation method thereof
Technical field
The present invention relates to a kind of electronic atomized liquid, particularly electronic atomized liquid of wetting one's whistle of a kind of heat-clearing and preparation method thereof.
Background technology
Along with the reinforcement of whole world Tobacco Control dynamics, and increasing smoker starts to accept and approves electronic cigarette, and electronic cigarette industry achieves develop rapidly.Be that exploitation and the popularization of the Tobacco Control product of representative obtains the active support of the government with electronic cigarette, technical development is irresistible.
Electronic atomized liquid, as technology most crucial in whole electronic cigarette industrial chain, directly decide the security of product, and consumer obtains mouthfeel and quality is experienced the most intuitively.Electronic atomized liquid is that in addition propane diols, glycerine etc. allocate the liquid made, by gasification after the atomizer heating of electronic cigarette for fog is absorbed by the body to a kind of liquid that skims the cream off milk from plant.Modern easily gets angry, and during heat, health is scorching; After having eaten the food of getting angry, aphthae, throat swell and ache; Also have hot-tempered short-tempered, the interior heat of people large, be necessary that developing one can meet craving for tobacco, can wet one's whistle again in heat-clearing, alleviate the electronic atomized liquid of throat's pain.
Blumea oil is China's Guizhou minority nationality medication.The oil that the sublimate belonging to the leaf of feverfew Blumea balsamifera blumea balsamifera (l.) dc. obtains through expression separation.Be the auxiliary product extracting natural borneol product, wherein containing L-Borneol, camphor, volatile oil, grease and other useful compositions, there is the effect of good bactericidal antiphlogistic, clearing heat and detoxicating, swelling and pain relieving.
Mono-ammonium glycyrrhizinate, white powder, has very strong sweet taste, not only has significant curative effect to respiratory diseases such as tracheitis, bronchitis, cough, asthma, and also has special effect to infection of digestive canal, hepatitis B, canker sore, gastric ulcer etc.For multiple toxin as diphtheria toxin, the river moon pig toxin, tetanus toxin and snake venom etc. have stronger detoxicating functions.
Rosa roxburghii, is rich in vitamin C, Cobastab, superoxide dismutase, has effect of maintenance throat.
Add flavoring essence in auxiliary material, play supplemental treatment and improve mouthfeel.The beautiful combination of mono-ammonium glycyrrhizinate, Rosa roxburghii, Dragon Well tea spire and blumea oil, can effectively alleviate abscess of throat, cough, aphtha, asthma etc., and protection throat is healthy.Sour-sweet mouthfeel is more made us sipping and is chewed without end, and spirit is felt well, and is difficult to forget.
Summary of the invention
In view of the above problems, the object of the present invention is to provide a kind of can enjoy anti-true smoking effect while, electronic atomized liquid that throat's comfort level and healthy heat-clearing wet one's whistle and preparation method thereof can be ensured again.
For achieving the above object, the electronic atomized liquid that a kind of heat-clearing provided by the invention wets one's whistle, primarily of blumea oil 0.1-2% w/w, propane diols 15-60% w/w, glycerine 15-60% w/w, mono-ammonium glycyrrhizinate 0.1-0.3% w/w, fresh Cili Juice 1-3% w/w and Dragon Well tea spire extract 1-3% w/w, and flavoring essence 1-5% w/w forms.
In some embodiments, blumea oil is feverfew Blumea balsamifera, at the oil that the sublimate of leaf obtains through expression separation.
Mono-ammonium glycyrrhizinate on the basis of glycyrrhizic acid, carries out ammonification obtain Triammonium glycyrrhizinate, then obtain mono-ammonium glycyrrhizinate through acidifying with acetic acid.
Mono-ammonium glycyrrhizinate extraction process flow process is:
(1) glycyrrhizic acid is extracted;
(2) glycyrrhizic acid is extracted;
(3) ammonification obtains Triammonium glycyrrhizinate;
(4) acidifying obtains mono-ammonium glycyrrhizinate;
(5) purifying is carried out to mono-ammonium glycyrrhizinate.So-called purifying, namely by the aggregation of many kinds of substance, by the method effect of physics, chemistry or biological aspect, becomes the process of a class or a kind of material.
In some embodiments, the preparation of fresh Cili Juice comprises following steps:
(1) choose flavous ripe Rosa roxburghii fresh fruit, cleaning, squeezes after draining;
(2) the fresh Cili Juice obtained after squeezing, leaves standstill, and naturally clarifies, chooses supernatant for subsequent use;
In some embodiments, the preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 ~ 1 times of volume, under stirring at 90 ~ 100 DEG C, extract 20 ~ 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
In some embodiments, glycerine is vegetables glycerine.Flavoring essence is one or more in natural fruit essence.Above-mentioned natural fruit essence is blueberry flavor, strawberry essence, flavoring apple essence etc.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 0.1% w/w, propane diols 60% w/w, glycerine 32.6% w/w, mono-ammonium glycyrrhizinate 0.3% w/w, flavoring essence 5% w/w and fresh Cili Juice 1% w/w, and Dragon Well tea spire extract 1% w/w forms.Thus, the electronic atomized liquid that heat-clearing wets one's whistle mainly is applicable to.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 2% w/w, propane diols 30.9% w/w, glycerine 60% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w, fresh Cili Juice 3% w/w, Dragon Well tea spire extract 3% w/w form.Thus, the electronic atomized liquid that heat-clearing wets one's whistle mainly is applicable to.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 1% w/w, propane diols 51.8% w/w, glycerine 40% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w, fresh Cili Juice 2% w/w, Dragon Well tea spire extract 2% w/w form.Thus, the electronic atomized liquid protecting throat's health is mainly applicable to.
Another object of the present invention is to provide the preparation method of the electronic atomized liquid that a kind of heat-clearing wets one's whistle, and concrete steps are as follows:
(1) blumea oil of set weight, mono-ammonium glycyrrhizinate, flavoring essence are added in the propane diols of set weight and the mixture of glycerine, stir;
(2) previously prepared good fresh Cili Juice, Dragon Well tea spire extract are mixed by set weight;
(3) the fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, stir, obtain product.
In some embodiments, in preparation process, a certain amount of nicotine can be added in the component of above-mentioned electronic atomized liquid.I.e. nicotine Homogeneous phase mixing together with the component such as blumea oil, mono-ammonium glycyrrhizinate.
In some embodiments, the preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 times of volume, under stirring at 90 DEG C, extract 20min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 0.1% w/w, mono-ammonium glycyrrhizinate 0.3% w/w, flavoring essence 5% w/w, propane diols 60% w/w, glycerine 32.6% w/w are mixed;
By prefabricated fresh Cili Juice 1% w/w, Dragon Well tea spire extract 1% w/w mixes;
The fresh Cili Juice mixed and Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
In some embodiments, the preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 1 times of volume, under stirring at 100 DEG C, extract 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 2% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w, propane diols 30.9% w/w, glycerine 60% w/w are mixed;
By prefabricated fresh Cili Juice 3% w/w, Dragon Well tea spire extract 3% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
In some embodiments, the preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.8 times of volume, under stirring at 95 DEG C, extract 25min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 1% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w, propane diols 51.8% w/w, glycerine 40% w/w are mixed;
By prefabricated fresh Cili Juice 2% w/w, Dragon Well tea spire extract 2% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
The invention has the beneficial effects as follows while having and can enjoying anti-true smoking effect, throat's comfort level and healthy effect can be ensured again.Due in electronic atomized liquid respectively containing blumea oil, mono-ammonium glycyrrhizinate, fresh Cili Juice, Dragon Well tea spire extract, and blumea oil energy bactericidal antiphlogistic, clearing heat and detoxicating; Rosa roxburghii has effect of maintenance throat; Adding of mono-ammonium glycyrrhizinate and flavoring essence, delicate fragrance is sweet; The interpolation of Dragon Well tea spire extract, makes electronic atomized liquid glycol micro-pungent, with fragrance striking the nose, oozes into heart spleen effect.Not only can allow electronic cigarette user while enjoyment is swallowed clouds and blown out fog, can experience again a kind of and make us sipping and chew without end between cog to throat, spirit is felt well, unforgettable sensation.In addition, the electronic atomized liquid containing blumea oil, mono-ammonium glycyrrhizinate, fresh Cili Juice, Dragon Well tea spire extract also has clearing heat and detoxicating, bactericidal antiphlogistic, effectively alleviates abscess of throat, cough, aphtha, asthma etc., the effect of protection throat health.Achieve while electronic cigarette user can enjoy anti-true smoking effect, throat's comfort level and healthy effect can be ensured again.
Detailed description of the invention
Below invention is described in further detail.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 0.1-2% w/w, propane diols 15-60% w/w, glycerine 15-60% w/w, mono-ammonium glycyrrhizinate 0.1-0.3% w/w, fresh Cili Juice 1-3% w/w and Dragon Well tea spire extract 1-3% w/w, and flavoring essence 1-5% w/w forms.
Blumea oil is feverfew Blumea balsamifera, at the oil that the sublimate of leaf obtains through expression separation.Wherein blumea oil contains L-Borneol, camphor, volatile oil, grease and other compositions.Blumea balsamifera is that one can be invigorated blood circulation in temperature, dispels rheumatism, desinsection.Control cold-damp diarrhea dysentery, stomachache borborygmus, swelling, arthralgia and myalgia, traumatic injury, the herbal medicine of tinea sore.Its biological scholarship and moral conduct happiness temperature climate, drought-resistant, be suitable for acid ground growth, barren-resistant, side generally relatively more loose, well-drained soil can plant.
Mono-ammonium glycyrrhizinate on the basis of glycyrrhizic acid, carries out ammonification obtain Triammonium glycyrrhizinate, then obtain mono-ammonium glycyrrhizinate through acidifying with acetic acid.
Mono-ammonium glycyrrhizinate extraction process flow process is:
(1) glycyrrhizic acid is extracted;
(2) glycyrrhizic acid is extracted;
(3) ammonification obtains Triammonium glycyrrhizinate;
(4) acidifying obtains mono-ammonium glycyrrhizinate;
(5) purifying is carried out to mono-ammonium glycyrrhizinate.
So-called purifying, namely by the aggregation of many kinds of substance, by the method effect of physics, chemistry or biological aspect, becomes the process of a class or a kind of material.
The preparation of fresh Cili Juice comprises following steps:
(1) choose flavous ripe Rosa roxburghii fresh fruit, cleaning, squeezes after draining;
(2) the fresh Cili Juice obtained after squeezing, leaves standstill, and naturally clarifies, chooses supernatant for subsequent use;
The preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 ~ 1 times of volume, under stirring at 90 ~ 100 DEG C, extract 20 ~ 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Glycerine is vegetables glycerine.Flavoring essence is one or more in pure natural essence.
Embodiment 1 is the electronic atomized liquid that heat-clearing wets one's whistle.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 0.1% w/w, propane diols 60% w/w, glycerine 32.6% w/w, mono-ammonium glycyrrhizinate 0.3% w/w, flavoring essence 5% w/w and fresh Cili Juice 1% w/w, and Dragon Well tea spire extract 1% w/w forms.
Embodiment 2 is the electronic atomized liquid that heat-clearing wets one's whistle.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 2% w/w, propane diols 30.9% w/w, glycerine 60% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w, fresh Cili Juice 3% w/w, Dragon Well tea spire extract 3% w/w form.
Embodiment 3 is the electronic atomized liquid of protection throat health.
The electronic atomized liquid that heat-clearing wets one's whistle, primarily of blumea oil 1% w/w, propane diols 51.8% w/w, glycerine 40% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w, fresh Cili Juice 2% w/w, Dragon Well tea spire extract 2% w/w form.
The electronic atomized liquid that heat-clearing wets one's whistle, it is made up of the blumea oil of set weight, propane diols, glycerine, mono-ammonium glycyrrhizinate, flavoring essence, fresh Cili Juice, Dragon Well tea spire extract.Blumea oil energy bactericidal antiphlogistic, clearing heat and detoxicating; Rosa roxburghii has effect of maintenance throat; Adding of mono-ammonium glycyrrhizinate and flavoring essence, delicate fragrance is sweet; The interpolation of Dragon Well tea spire extract, makes electronic atomized liquid glycol micro-pungent, with fragrance striking the nose, oozes into heart spleen.
A preparation method for the electronic atomized liquid that heat-clearing wets one's whistle, concrete steps are as follows:
(1) blumea oil of set weight, mono-ammonium glycyrrhizinate, flavoring essence are added in the propane diols of set weight and the mixture of glycerine, stir;
(2) previously prepared good fresh Cili Juice, Dragon Well tea spire extract are mixed by set weight;
(3) the fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, stir, obtain product.A certain amount of nicotine can be added in preparation process, also can not add nicotine.
Embodiment 4 is prepared on the basis of embodiment 1.
A preparation method for the electronic atomized liquid that heat-clearing wets one's whistle, is characterized in that, the preparation of described Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 times of volume, under stirring at 90 DEG C, extract 20min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 0.1% w/w, mono-ammonium glycyrrhizinate 0.3% w/w, flavoring essence 5% w/w, propane diols 60% w/w, glycerine 32.6% w/w are mixed;
By prefabricated fresh Cili Juice 1% w/w, Dragon Well tea spire extract 1% w/w mixes;
The fresh Cili Juice mixed and Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
Embodiment 5 is prepared on the basis of embodiment 2.
The preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 1 times of volume, under stirring at 100 DEG C, extract 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 2% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w, propane diols 30.9% w/w, glycerine 60% w/w are mixed;
By prefabricated fresh Cili Juice 3% w/w, Dragon Well tea spire extract 3% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
Embodiment 6 is prepared on the basis of embodiment 3.
The preparation of Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.8 times of volume, under stirring at 95 DEG C, extract 25min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 1% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w, propane diols 51.8% w/w, glycerine 40% w/w are mixed;
By prefabricated fresh Cili Juice 2% w/w, Dragon Well tea spire extract 2% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
Be below the usage data list of electronic atomized liquid:
Table 1 is the different component service condition table of every feed ration 1ml (about 200 mouthfuls).
Table 2 is the different component service condition table of every feed ration 2ml (about 400 mouthfuls).
Above-described is only some embodiments of the present invention.For the person of ordinary skill of the art, without departing from the concept of the premise of the invention, can also make some distortion and improvement, these all belong to the protection domain of invention.

Claims (10)

1. the electronic atomized liquid that wets one's whistle of heat-clearing, it is primarily of blumea oil 0.1-2% w/w, propane diols 15-60% w/w, glycerine 15-60% w/w, mono-ammonium glycyrrhizinate 0.1-0.3% w/w, fresh Cili Juice 1-3% w/w and Dragon Well tea spire extract 1-3% w/w, and flavoring essence 1-5% w/w forms.
2. the electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 1, it is characterized in that, described blumea oil is feverfew Blumea balsamifera, at the oil that the sublimate of leaf obtains through expression separation;
Described mono-ammonium glycyrrhizinate on the basis of glycyrrhizic acid, carries out ammonification obtain Triammonium glycyrrhizinate, then obtain mono-ammonium glycyrrhizinate through acidifying with acetic acid;
Described mono-ammonium glycyrrhizinate extraction process flow process is:
(1) glycyrrhizic acid is extracted;
(2) glycyrrhizic acid is extracted;
(3) ammonification obtains Triammonium glycyrrhizinate;
(4) acidifying obtains mono-ammonium glycyrrhizinate;
(5) purifying is carried out to mono-ammonium glycyrrhizinate.
3. the electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 1, it is characterized in that, the preparation of described fresh Cili Juice comprises following steps:
(1) choose flavous ripe Rosa roxburghii fresh fruit, cleaning, squeezes after draining;
(2) the fresh Cili Juice obtained after squeezing, leaves standstill, and naturally clarifies, chooses supernatant for subsequent use.
4. the electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 1, it is characterized in that, the preparation of described Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 ~ 1 times of volume, under stirring at 90 ~ 100 DEG C, extract 20 ~ 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use.
5. the electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 1, it is primarily of blumea oil 2% w/w, propane diols 30.9% w/w, glycerine 60% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w and fresh Cili Juice 3% w/w, and Dragon Well tea spire extract 3% w/w forms.
6. the electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 1, it is primarily of blumea oil 1% w/w, propane diols 51.8% w/w, glycerine 40% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w and fresh Cili Juice 2% w/w, and Dragon Well tea spire extract 2% w/w forms.
7. the preparation method of the electronic atomized liquid that a kind of heat-clearing according to claim 1-6 any one wets one's whistle, concrete steps are as follows:
(1) blumea oil of set weight, mono-ammonium glycyrrhizinate, flavoring essence are added in the propane diols of set weight and the mixture of glycerine, stir;
(2) previously prepared good fresh Cili Juice, Dragon Well tea spire extract are mixed by set weight;
(3) the fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, stir, obtain product.
8. the preparation method of electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 7, it is characterized in that, the preparation of described Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.5 times of volume, under stirring at 90 DEG C, extract 20min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 0.1% w/w, mono-ammonium glycyrrhizinate 0.3% w/w, flavoring essence 5% w/w, propane diols 60% w/w, glycerine 32.6% w/w are mixed;
By prefabricated fresh Cili Juice 1% w/w, Dragon Well tea spire extract 1% w/w mixes;
The fresh Cili Juice mixed and Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
9. the preparation method of electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 7, it is characterized in that, the preparation of described Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 1 times of volume, under stirring at 100 DEG C, extract 30min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 2% w/w, mono-ammonium glycyrrhizinate 0.1% w/w, flavoring essence 1% w/w, propane diols 30.9% w/w, glycerine 60% w/w are mixed;
By prefabricated fresh Cili Juice 3% w/w, Dragon Well tea spire extract 3% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
10. the preparation method of electronic atomized liquid that wets one's whistle of a kind of heat-clearing according to claim 7, it is characterized in that, the preparation of described Dragon Well tea spire extract comprises following steps:
(1) choose fresh Dragon Well tea spire, clean, put into mixer, stir broken;
(2) add the pure water of 0.8 times of volume, under stirring at 95 DEG C, extract 25min;
(3) filter, filtrate is separated through centrifuge, gets supernatant for subsequent use;
Blumea oil 1% w/w, mono-ammonium glycyrrhizinate 0.2% w/w, flavoring essence 3% w/w, propane diols 51.8% w/w, glycerine 40% w/w are mixed;
By prefabricated fresh Cili Juice 2% w/w, Dragon Well tea spire extract 2% w/w mixes;
The fresh Cili Juice mixed, Dragon Well tea spire extract are added in propane diols containing blumea oil, mono-ammonium glycyrrhizinate, flavoring essence and glycerol mixture, mix and obtain product.
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CN115887575A (en) * 2022-05-27 2023-04-04 国润生物科技(深圳)有限公司 Functional composition with effects of moistening lung and clearing throat and preparation method thereof

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