CN104765342A - Automated polymerized osamine production device and preparation method thereof - Google Patents
Automated polymerized osamine production device and preparation method thereof Download PDFInfo
- Publication number
- CN104765342A CN104765342A CN201510110570.0A CN201510110570A CN104765342A CN 104765342 A CN104765342 A CN 104765342A CN 201510110570 A CN201510110570 A CN 201510110570A CN 104765342 A CN104765342 A CN 104765342A
- Authority
- CN
- China
- Prior art keywords
- reactor
- tank
- osamine
- discharging opening
- polymerization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05B—CONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
- G05B19/00—Programme-control systems
- G05B19/02—Programme-control systems electric
- G05B19/418—Total factory control, i.e. centrally controlling a plurality of machines, e.g. direct or distributed numerical control [DNC], flexible manufacturing systems [FMS], integrated manufacturing systems [IMS], computer integrated manufacturing [CIM]
- G05B19/41875—Total factory control, i.e. centrally controlling a plurality of machines, e.g. direct or distributed numerical control [DNC], flexible manufacturing systems [FMS], integrated manufacturing systems [IMS], computer integrated manufacturing [CIM] characterised by quality surveillance of production
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P90/00—Enabling technologies with a potential contribution to greenhouse gas [GHG] emissions mitigation
- Y02P90/02—Total factory control, e.g. smart factories, flexible manufacturing systems [FMS] or integrated manufacturing systems [IMS]
Abstract
The invention relates to an automated polymerized osamine production device and a preparation method thereof, and belongs to the field of chemicals. According to the technical scheme, the automated polymerized osamine production device comprises four sets of liquid metering tanks with bit material sensors and one set of powder metering tanks, wherein the liquid metering tanks and the powder metering tanks are fixed through a platform support, a discharging opening of the first liquid metering tank and discharging openings of the powder metering tanks are connected with a stirring tank through pipes, a discharging opening of the second liquid metering tank, a discharging opening of the third liquid metering tank and a discharging opening of the fourth liquid metering tank are connected to a reaction still with a temperature sensor and with the heating cooling capacity through pipes. A discharging opening of the stirring tank is connected to the reaction still through a pipe. A connection pipe between the reaction still and the stirring tank is provided with a feeding pump. The middle of the reaction still is further connected with a catalyst feeding opening connected with a catalyst feeding device. A discharging opening of the reaction still is connected to a finished product tank through a pipe. A discharging pump is arranged on the position, between the reaction still and the finished product tank, of the pipe. The automated polymerized osamine production device achieves full automation of the production process, product quality is stable, and no difference exists in different batches.
Description
Technical field
The present invention relates to a kind of polymerization osamine automated production equipment and preparation method thereof, belong to chemical field.
Background technology
Polymerization osamine is as the cement grinding aid raw material of a kind of new life, and it improves the applicability of cement grinding aid and the compatibility of concrete admixture greatly, and application prospect is fine.Lack polymerization osamine automated production equipment in market, and the product homogenisation that common process is produced is poor, batch between the property of there are differences.
Summary of the invention
The object of this patent is to provide a kind of polymerization osamine automated production equipment, realizes production run full-automation, reduces error, the polymerization sugar amine product steady quality produced, indifference between batch.
For achieving the above object, the technical scheme that this patent adopts is: comprise four groups of level meter measuring tanks and the one group of powder metering tank of expecting sensor with position fixed by platform support, first liquid test tank is wherein connected stirred pot with the discharging opening of powder metering tank by pipeline, second liquid test tank, the discharging opening of the 3rd level meter measuring tank and the 4th level meter measuring tank is connected to one by pipeline and has heating cooling power and with the reactor of temperature sensor, the discharging opening of above-mentioned stirred pot is connected to above-mentioned reactor by pipeline, connecting tube between above-mentioned reactor and stirred pot is provided with feeding pump, the middle part of reactor is also connected with a catalyst feeds and connects catalyst feeding device, the discharging opening of reactor is connected to finished pot by pipeline, pipeline between reactor and finished pot is provided with discharging pump, the discharging opening of described level meter measuring tank is provided with pneumatic valve, and the discharging opening of powder metering tank is provided with flap valve, described reactor is three layers, and inside is reaction chamber, and outermost layer is cooling water layer, and middle layer is heat conduction oil reservoir, and the discharging opening of reactor is provided with pneumatic valve, the heat conduction oil reservoir of described reactor is connected to conduction oil pumping plant by pipeline, and cooling water layer is connected to circulating cooling pond by the pipeline being provided with water pump, the pipeline that described powder metering tank discharging opening connects is stainless steel pipes, and described reactor is built with stirring apparatus.
Polymerization osamine automated production equipment prepares the method for polymerization osamine, and in first liquid test tank, metering water joins in stirred pot, and stirred pot is opened and stirred;
Powder metering tank metering powder material joins in stirred pot, is stirred to powder material and fully dissolves;
Start feeding pump, the solution in stirred pot is evacuated to reactor, when vacuum appears in stirred pot, feeding pump stops;
The pneumatic valve of second liquid test tank metering is opened, and constant weight solution joins in reactor;
Conduction oil pumping plant starts, conduction-oil warming in the middle layer of reactor, stops the work of conduction oil pumping plant when reactor temperature reaches 60 DEG C;
Conduction oil pumping plant continues startup and heats, and the pneumatic valve of the 3rd level meter measuring tank metering is opened, and constant weight solution joins in reactor, and the pneumatic valve of the 4th level meter measuring tank metering is opened, and constant weight solution joins in reactor;
When reactor temperature arrives 60 DEG C, catalyst feeding device starts, and adds catalyzer in reactor;
When reactor temperature arrives 80 DEG C, conduction oil pumping plant quits work, and hydrodynamic(al) is opened and cold water is squeezed into the cooling of reactor cooling water layer from circulating water pool, and when chilling temperature in reactor is to 30 DEG C, water pump stops;
Pneumatic valve under reactor and feeding pump are opened, and by reactor and finished pot connecting tube, are squeezed into by finished product in finished pot;
When there is vacuum in reactor, close the pneumatic valve under feeding pump and reactor.
Polymerization osamine automated production equipment according to claim prepares the method for polymerization osamine, and it is 5 minutes summers, 10 minutes winters that stirred pot adds the mixing time after powder material.
The advantage of this patent is: by metering system, discharging pneumatic valve, and stirring apparatus realizes production run full-automation, reduces error, constant product quality, indifference between batch.
Accompanying drawing explanation
Fig. 1 is the structural drawing of this patent;
Reference numeral: 1, platform support, 2, first liquid test tank, 3, position material sensor, 4, pneumatic valve, 5, powder metering tank, 6, flap valve, 7, stirred pot, 8, feeding pump, 9, reactor, 10, conduction oil pumping plant, 11, discharging pump, 12, catalyst feeding device, 13, water pump, 14, circulating cooling pond, 15, finished pot, 16, second liquid test tank, the 17, the 3rd level meter measuring tank, the 18, the 4th level meter measuring tank.
Embodiment
According to Fig. 1, platform support has the hole of 900mm diameter, each test tank is placed in 900mm hole by the foot support of position material sensor.
Fill raw water with in the level meter measuring tank that powder metering tank batch mixing stirs, this raw water selects tap water, and its excess-three level meter measuring tank is respectively charged into molasses, amino acid solution, alcohol.Pneumatic valve is equipped with in each level meter measuring tank bottom.Powder metering tank bottom dress flap valve.
Stirred pot is that the stainless steel of diameter 2.0*2.5 is made, and with motor vertical shaft reductor and paddle, paddle top is connected with reductor shaft joint, and bottom is contained in the sliding bearing groove bottom stirred pot.Stirred pot discharge pipe establishes feeding pump, and discharge pipe is the PPR pipe road of 63mm, and passes to reactor.Reactor temperature change can show from control terminal and be provided with feedback control loop.Manhole door is arranged at reactor top, for observing the change of material materials inside reaction and adding catalyzer in time.
The stirring apparatus of reactor is equipped with motor, reductor and paddle, and paddle is fixed on reductor by interlock joint.The discharging opening pneumatic valve of reactor to be fixed on reactor by flange and to be connected with feeding pump by PPR pipe road.In reactor, reacted finished product is evacuated in finished pot by discharging pump by PPR pipe road.
The implementation method of technological process is described below in conjunction with accompanying drawing:
Water is according to the weight blanking of 28wt%, and stirred pot is clicked and opened;
Powder starts the weight blanking by 3 wt %, and abundant stirring and dissolving falls in stirring machine, 5 minutes summers of conputer controlled, 10 minutes winters, stirs and stop after time of arrival;
Feeding pump motor is opened, and be extracted in reactor by the material in stirred pot, when there is vacuum, pump stops automatically;
Second liquid test tank bottom pneumatic valve is opened automatically, and material enters reactor by pipeline, closes when arriving the weight of 40.5 wt %;
When the pneumatic valve of second liquid test tank cuts out, conduction oil pumping plant unlatching work, heat-conducting oil heating reactor, squeezes into reactor by station internal circulation pump and heats, and stops ebullator working on when temperature reaches 60 DEG C;
The pneumatic valve of the 3rd level meter measuring tank starts, and the First Astronautic Research Institute for Measurement and Test needs weight liquid charging stock to flow into reactor by pipeline, when reaching the weight of 22 wt %, automatically closes;
The pneumatic valve of the 4th level meter measuring tank starts, and when reaching the weight of 4wt%, automatically closes;
Conduction oil pumping plant is opened, and when reactor temperature arrives 60 DEG C, the weight percent catalyst of metering 2.5% joins in reactor;
When reactor temperature arrives 80 DEG C, oil pump stops, and water circulating pump is automatically opened and cold water is squeezed into reactor cooling from circulating water pool, and when chilling temperature is to 30 DEG C, cooling-water pump stops automatically;
Pneumatic valve in reactor and discharging pump are opened automatically, by reactor and finished pot connecting tube, squeeze in finished pot.
When there is vacuum in reactor, the pneumatic valve in reactor and discharging pump are closed automatically.
Claims (7)
1. a polymerization osamine automated production equipment, it is characterized in that, comprise by fixing four groups of level meter measuring tanks and the one group of powder metering tank of expecting sensor (3) with position of platform support (1), first liquid test tank (5) is wherein connected stirred pot (7) with the discharging opening of powder metering tank (2) by pipeline, second liquid test tank (16), the discharging opening of the 3rd level meter measuring tank (17) and the 4th level meter measuring tank (18) is connected to one by pipeline and has heating cooling and stirring ability and with the reactor (9) of temperature sensor, the discharging opening of above-mentioned stirred pot (7) is connected to above-mentioned reactor (9) by pipeline, connecting tube between above-mentioned reactor (9) and stirred pot (7) is provided with feeding pump (8), the middle part of reactor (9) is also provided with a catalyst feeds and connects catalyst feeding device (12), the discharging opening of reactor (9) is connected to finished pot (15) by pipeline, pipeline between reactor (9) and finished pot (15) is provided with discharging pump (11).
2. polymerization osamine automated production equipment according to claim 1, is characterized in that, the discharging opening of described each group of level meter measuring tank (2) is provided with pneumatic valve (6), and the discharging opening of powder metering tank is provided with flap valve (4).
3. polymerization osamine automated production equipment according to claim 1, is characterized in that, described reactor (9) is three layers, and inside is reaction chamber, and outermost layer is cooling water layer, and middle layer is heat conduction oil reservoir, and the discharging opening of reactor (9) is provided with pneumatic valve.
4. polymerization osamine automated production equipment according to claim 3, it is characterized in that, the heat conduction oil reservoir of described reactor is connected to conduction oil pumping plant (10) by pipeline, and cooling water layer is connected to circulating cooling pond (14) by the pipeline being provided with water pump (13)
Polymerization osamine automated production equipment according to claim 1, is characterized in that, the pipeline that described powder metering tank discharging opening connects is stainless steel pipes.
5. polymerization osamine automated production equipment according to claim 1, is characterized in that, described reactor (9) is built with stirring apparatus.
6. polymerization osamine automated production equipment according to claim 1 prepares a method for polymerization osamine, it is characterized in that, in first liquid test tank, metering water joins in stirred pot, and stirred pot is opened and stirred;
Powder metering tank metering powder material joins in stirred pot, is stirred to powder material and fully dissolves;
Start feeding pump, the solution in stirred pot is evacuated to reactor, when vacuum appears in stirred pot, feeding pump stops;
The pneumatic valve of second liquid test tank metering is opened, and constant weight solution joins in reactor;
Conduction oil pumping plant starts, conduction-oil warming in the middle layer of reactor, stops the work of conduction oil pumping plant when reactor temperature reaches 60 DEG C;
Conduction oil pumping plant continues startup and heats, and the pneumatic valve of the 3rd level meter measuring tank metering is opened, and constant weight solution joins in reactor, and the pneumatic valve of the 4th level meter measuring tank metering is opened, and constant weight solution joins in reactor;
When reactor temperature arrives 60 DEG C, catalyst feeding device starts, and adds catalyzer in reactor;
When reactor temperature arrives 80 DEG C, conduction oil pumping plant quits work, and hydrodynamic(al) is opened and cold water is squeezed into the cooling of reactor cooling water layer from circulating water pool, and when chilling temperature in reactor is to 30 DEG C, water pump stops;
Pneumatic valve under reactor and feeding pump are opened, and by reactor and finished pot connecting tube, are squeezed into by finished product in finished pot;
When there is vacuum in reactor, close the pneumatic valve under feeding pump and reactor.
7. polymerization osamine automated production equipment according to claim 6 prepares the method for polymerization osamine, and it is 5 minutes summers, 10 minutes winters that stirred pot adds the mixing time after powder material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510110570.0A CN104765342A (en) | 2015-03-13 | 2015-03-13 | Automated polymerized osamine production device and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510110570.0A CN104765342A (en) | 2015-03-13 | 2015-03-13 | Automated polymerized osamine production device and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104765342A true CN104765342A (en) | 2015-07-08 |
Family
ID=53647250
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510110570.0A Pending CN104765342A (en) | 2015-03-13 | 2015-03-13 | Automated polymerized osamine production device and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104765342A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105169981A (en) * | 2015-08-12 | 2015-12-23 | 东莞兆舜有机硅科技股份有限公司 | Production method of electronic-pouring sealant |
| CN106807507A (en) * | 2017-01-20 | 2017-06-09 | 广州立之力机械设备有限公司 | A kind of coating products automatic assembly line |
| CN108864352A (en) * | 2018-07-20 | 2018-11-23 | 江西安德力高新科技有限公司 | A kind of polyhydroxy modified acroleic acid production system and its control method |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040024146A1 (en) * | 2000-10-25 | 2004-02-05 | Friedersdorf Chris B. | Processes and apparatus for continuous solution polymerization |
| CN103102369A (en) * | 2013-02-06 | 2013-05-15 | 扬州晨化科技集团有限公司 | Production method for diethyl ethanephosphonate |
| CN103769030A (en) * | 2014-02-20 | 2014-05-07 | 枣庄市荣宝莱建材科技发展有限公司 | Automatic production equipment for polycarboxylate superplasticizer |
| CN103926902A (en) * | 2014-04-24 | 2014-07-16 | 枣庄市荣宝莱建材科技发展有限公司 | Multifunctional automatic control device for cement and commercial concrete admixture production |
| CN203916657U (en) * | 2014-05-15 | 2014-11-05 | 吴持跃 | Chemical reaction kettle feed arrangement |
| CN204631573U (en) * | 2015-03-13 | 2015-09-09 | 枣庄市荣宝莱建材科技发展有限公司 | Polymerization osamine automated production equipment |
-
2015
- 2015-03-13 CN CN201510110570.0A patent/CN104765342A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040024146A1 (en) * | 2000-10-25 | 2004-02-05 | Friedersdorf Chris B. | Processes and apparatus for continuous solution polymerization |
| CN103102369A (en) * | 2013-02-06 | 2013-05-15 | 扬州晨化科技集团有限公司 | Production method for diethyl ethanephosphonate |
| CN103769030A (en) * | 2014-02-20 | 2014-05-07 | 枣庄市荣宝莱建材科技发展有限公司 | Automatic production equipment for polycarboxylate superplasticizer |
| CN103926902A (en) * | 2014-04-24 | 2014-07-16 | 枣庄市荣宝莱建材科技发展有限公司 | Multifunctional automatic control device for cement and commercial concrete admixture production |
| CN203916657U (en) * | 2014-05-15 | 2014-11-05 | 吴持跃 | Chemical reaction kettle feed arrangement |
| CN204631573U (en) * | 2015-03-13 | 2015-09-09 | 枣庄市荣宝莱建材科技发展有限公司 | Polymerization osamine automated production equipment |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105169981A (en) * | 2015-08-12 | 2015-12-23 | 东莞兆舜有机硅科技股份有限公司 | Production method of electronic-pouring sealant |
| CN106807507A (en) * | 2017-01-20 | 2017-06-09 | 广州立之力机械设备有限公司 | A kind of coating products automatic assembly line |
| CN108864352A (en) * | 2018-07-20 | 2018-11-23 | 江西安德力高新科技有限公司 | A kind of polyhydroxy modified acroleic acid production system and its control method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206008688U (en) | A kind of circular response kettle | |
| CN104765342A (en) | Automated polymerized osamine production device and preparation method thereof | |
| CN204631573U (en) | Polymerization osamine automated production equipment | |
| CN213055700U (en) | Rice milling emery roller resin liquid weighing device | |
| CN105642216A (en) | Movable adjustable-stirring-radius reaction kettle | |
| CN207667629U (en) | A kind of safe and efficient alkoxylating catalyst preparation system | |
| CN104446098A (en) | Automatic production technology equipment for polycarboxylic acid water-reducing agent | |
| CN202387244U (en) | Vacuum mixing, concentrating and crystallizing device | |
| CN205413010U (en) | Adjustable reation kettle of portable stirring radius | |
| CN206328403U (en) | One primary yeast enzymatic vessel | |
| CN206801873U (en) | Double-fluid grouting machine | |
| CN202062507U (en) | Two-stage mixing and stirring device for concrete water reducers | |
| CN110283086B (en) | Method and device for continuously producing m-aminophenol | |
| CN209276529U (en) | A kind of vertical multi-stage anaerobic reactor | |
| CN204412108U (en) | A kind of for preserved beancurd juice produce dissolve equipment | |
| CN104577035B (en) | Vacuum electrolyte-filling device for lead-acid storage battery | |
| CN207405181U (en) | The enzymatic isolation method of a kind of retort and its composition prepares the process units of Tagatose | |
| CN206289027U (en) | A kind of acid-base neutralization reaction kettle that can make full use of resource | |
| CN215428363U (en) | Nano fracturing fluid adding and mixing device | |
| CN211562967U (en) | Leather levelling agent apparatus for producing | |
| CN213791069U (en) | Automatic batching system | |
| CN104959069B (en) | Many liquid multichannel mixing arrangements | |
| CN211562968U (en) | Leather auxiliary agent reation kettle | |
| CN212092212U (en) | Lubricating oil heat preservation mediation cauldron | |
| CN212377771U (en) | Ring canal system for simulating influence of temperature on resistance of paste delivery pipeline |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150708 |
|
| WD01 | Invention patent application deemed withdrawn after publication |