CN104762721A - Double-component flame retardant anti-static fabric and a preparation method thereof - Google Patents
Double-component flame retardant anti-static fabric and a preparation method thereof Download PDFInfo
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Abstract
The invention discloses a double-component flame retardant anti-static fabric and a preparation method thereof. The double-component blended yarn of cotton fibers and moisture absorption and sweat discharge fibers is used as a raw material, conductive fibers and the blended yarns are doubled and twisted to prepare conductive yarns with twist of 25-55 twists per 10 cm; the conductive yarns are woven in the weaving process in a spacing manner to prepare anti-static grid colored cloth; then the blank cloth is dyed and subjected to flame retardant treatment and is dried and cooled to obtain a flame retardant anti-static fabric. The conductive fibers are intercrossed in the warp direction and the weft direction of the fabric, so the phenomenon of falling after breakage of the conductive fibers can be effectively avoided, and the prepared fabric has a good fabric anti-static effect; an assistant is added in flame retardant finishing, the infiltration of a flame retardant into the yarns is facilitated by addition of the assistant, and the prepared fabric has soft handfeel, good service performance and stable flame retardant performance. The preparation flow is short and the process is simple.
Description
Technical field
The invention belongs to technical field of textile fabric, be specifically related to a kind of two component fire-resistant antistatic fabric, the invention still further relates to the preparation method of this pair of component fire-resistant antistatic fabric.
Background technology
Cotton fiber is natural fabric, its moisture pick-up properties is good, cotton fiber goods good permeability, comfortable and easy to wear, soft and warming, therefore cotton fiber has become the main raw material of caused by spinning industrial production, but when the volume of perspiration of people is slightly large, cotton fiber can because of moisture expantion, its fortune declines and is pasted onto on skin, meanwhile, moisture content divergence speed is also comparatively slow, thus causes a kind of cold wet sense to human body.
Terylene is hydrophobic synthetic fibre, its moisture pick-up properties is low, ratio resistance is very high, polyester-cotton fabric wear use procedure can because of friction cause electrostatic phenomenon, lighter electrostatic phenomenon can make clothes attracting dust, or react with human body generation electrostatic, reduce the comfortableness of dress; In drier environment, electrostatic phenomenon may produce spark, and initiation fire causes security incident.On domestic piece market in recent years, surging gradually to moisture absorbing and sweat releasing textiles demand cry, cause the concern of people in the industry, people are by physics and chemistry modification, or both associated methods are implemented to carry out modification to polyster fibre, prepare and can absorb rapidly skin surface moisture and sweat, by diffusion, be delivered to outer field hygroscopic fibre.
In the electrostatic sensitive such as explosion hazard area and precision instrument places such as liquid gasification station, gas station, oil depots; in order to avoid causing full accident because of electrostatic; protection staff's personal safety and national wealth safety; anti-static clothing must be worn; simultaneously; in fire-fighting and industrial production environment, usually require that clothes have the function of fire protection flame retarding.By the blending by a certain percentage of cotton fiber, hygroscopic fibre, achieve between different fiber and have complementary advantages, the fabric woven is endurable, moisture permeability is good.At present, most fabric only possesses electrostatic-proof function separately, and meanwhile, existing fabric is after flame-proof treatment, and feel is partially hard, and finishing technique process is complicated.Therefore, utilize simple technique to arrange fabric, the fabric after arrangement, while having antistatic and anti-flaming function concurrently, meets it and takes requirement, has very important meaning to fabric in the application of special industry.
Summary of the invention
The object of this invention is to provide a kind of two component fire-resistant antistatic fabric, solve the problem that existing fabric can not have antistatic and anti-flaming function concurrently simultaneously.
Another object of the present invention is to provide the preparation method of this pair of component fire-resistant antistatic fabric, solves existing fabric fire-retardant complicated with dyeing finishing technique, the problem that the fabric feel after arrangement is partially hard.
The technical solution adopted in the present invention is, a kind of two component fire-resistant antistatic fabric, obtains according to following steps preparation:
Step 1: grey cloth is weaved
Choose the raw material of the two component blended yarn of cotton fiber and hygroscopic fibre as face weave, by conductive filament and blended yarn and twisting obtains conductive yam, in weaving process, interval inweaves conductive yam, obtains antistatic grid grey cloth;
Step 2: dyeing process
Take dyestuff, be dissolved in water, stir, obtain the dye liquor that concentration is 20 ~ 80g/L, regulator solution pH to 4 ~ 7.5, step 1 woven antistatic grid grey cloth is dyeed;
Step 3: flame-proof treatment
Be that 5.5 ~ 7.5:1 takes fire retardant and magnesium chloride in mass ratio, and add appropriate amount of addition agent, be placed in water and dissolve, stir, obtaining concentration is the solution of 135 ~ 175g/L, being poured into by solution pads in groove, and the mode adopting a leaching one to roll is padded step 2 gained painting cloth, and pick-up is 60% ~ 80%;
Step 4: drying and processing
Step 3 was padded the fabric of fire retarding treating liquid through 95 ~ 105 DEG C of oven dry, 180 ~ 200 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
Feature of the present invention is also,
In step 1, raw-materially in two component blended yarn to consist of: cotton fiber 40% ~ 60%, hygroscopic fibre 40% ~ 60%, above each weight percentages of components sum is 100%.
In step 1, conductive filament is the one in nylon based conductive fiber long filament, terylene base conductive fiber long filament or black carbon fiber electrically conductive filament, and the twist of gained conductive yam is 25 ~ 55 sth. made by twisting/10cm.
In step 1, the spacing of antistatic grid grey cloth warp-wise conductive filament is 0.5 ~ 2.0cm, and the spacing of broadwise conductive filament is 0.5 ~ 2.0cm, and fabric warp density range is 50 ~ 200/10cm, and weft count scope is 50 ~ 150/10cm.
In step 3, fire retardant is FPK8002, and auxiliary agent is soluble polyurethane and acetic acid, and the mass ratio of its addition and retardant load level is 1:22 ~ 30.
Another technical scheme of the present invention is, the preparation method of a kind of pair of component fire-resistant antistatic fabric is specifically prepared according to following steps:
Step 1: grey cloth is weaved
Choose the raw material of the two component blended yarn of cotton fiber and hygroscopic fibre as face weave, by conductive filament and blended yarn and twisting obtains conductive yam, in weaving process, interval inweaves conductive yam, obtains antistatic grid grey cloth;
Step 2: dyeing process
Take dyestuff, be dissolved in water, stir, obtain the dye liquor that concentration is 20 ~ 80g/L, regulator solution pH to 4 ~ 7.5, step 1 woven antistatic grid grey cloth is dyeed;
Step 3: flame-proof treatment
Be that 5.5 ~ 7.5:1 takes fire retardant and magnesium chloride in mass ratio, and add appropriate amount of addition agent, be placed in water and dissolve, stir, obtaining concentration is the solution of 135 ~ 175g/L, being poured into by solution pads in groove, and the mode adopting a leaching one to roll is padded step 2 gained painting cloth, and pick-up is 60% ~ 80%;
Step 4: drying and processing
Step 3 was padded the fabric of fire retarding treating liquid through 95 ~ 105 DEG C of oven dry, 180 ~ 200 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
Feature of the present invention is also,
In step 1, raw-materially in two component blended yarn to consist of: cotton fiber 40% ~ 60%, hygroscopic fibre 40% ~ 60%, above each weight percentages of components sum is 100%.
In step 1, conductive filament is the one in nylon based conductive fiber long filament, terylene base conductive fiber long filament or black carbon fiber electrically conductive filament, and the twist of gained conductive yam is 25 ~ 55 sth. made by twisting/10cm.
In step 1, the spacing of antistatic grid grey cloth warp-wise conductive filament is 0.5 ~ 2.0cm, and the spacing of broadwise conductive filament is 0.5 ~ 2.0cm, and fabric warp density range is 50 ~ 200/10cm, and weft count scope is 50 ~ 150/10cm.
In step 3, fire retardant is FPK8002, and auxiliary agent is soluble polyurethane and acetic acid, and the mass ratio of its addition and retardant load level is 1:22 ~ 30.
The invention has the beneficial effects as follows, using the two component blended yarn of cotton/moisture absorbing and sweat releasing and conductive filament as raw material, conductive filament and blended yarn are twisted into conductive yam, conductive filament is woven in fabric exist in the form of a grid, mutually intersect at the warp-wise of fabric and broadwise, the phenomenon come off after effectively avoiding conductive filament to rupture, the fabric anti-static effect of preparation is good; In flame-proof treatment, add auxiliary agent, adding of auxiliary agent is conducive to fire retardant infiltration yarn interior, and obtained fabric is soft, wearability good and fire resistance is stablized; Present invention process flow process is short, and preparation process is easy.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is described in detail.
Embodiment 1
Step 1: take cotton fiber 60Kg, hygroscopic fibre 40Kg, carries out blending, and obtained number is two component blended yarns of 80/2, the specification that two component blended yarn and Japanese Zhong Fang company are produced is the conductive filament of 20D/3F and twists with the fingers, the obtained twist is the conductive yam of 25 sth. made by twisting/10cm, and use air-jet loom to weave, in weaving process, interval inweaves conductive yam, obtained antistatic grid grey cloth, wherein, the spacing of warp-wise conductive filament is 0.5cm, and the spacing of broadwise conductive filament is 2.0cm;
Step 2: take 1Kg dyestuff, is dissolved in water, is stirred, regulator solution pH to 4, dyes to step 1 woven antistatic grid grey cloth;
Step 3: take 5.5Kg fire retardant FPK8002,1Kg magnesium chloride, 0.15Kg soluble polyurethane and 0.1Kg acetic acid respectively, be placed in 50L water and dissolve, obtain solution; Being poured into by solution pads in groove, pads step 2 gained painting cloth, and pick-up is 60%;
Step 4: step 3 was padded the fabric of fire retarding treating liquid through 95 DEG C of oven dry, 200 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
Embodiment 2
Step 1: take cotton fiber 40Kg, hygroscopic fibre 60Kg, carries out blending, and obtained number is two component blended yarns of 80/2, the specification that two component blended yarn and Japanese Zhong Fang company are produced is the conductive filament of 20D/3F and twists with the fingers, the obtained twist is the conductive yam of 45 sth. made by twisting/10cm, and use air-jet loom to weave, in weaving process, interval inweaves conductive yam, obtained antistatic grid grey cloth, wherein, the spacing of warp-wise conductive filament is 1.2cm, and the spacing of broadwise conductive filament is 0.9cm;
Step 2: take 2.5Kg dyestuff, is dissolved in water, is stirred, regulator solution pH to 5.5, dyes to step 1 woven antistatic grid grey cloth;
Step 3: take 6.25Kg fire retardant FPK8002,1Kg magnesium chloride, 0.15Kg soluble polyurethane and 0.1Kg acetic acid respectively, be placed in 50L water and dissolve, obtain solution; Being poured into by solution pads in groove, pads step 2 gained painting cloth, and pick-up is 80%;
Step 4: step 3 was padded the fabric of fire retarding treating liquid through 100 DEG C of oven dry, 190 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
Embodiment 3
Step 1: take cotton fiber 50Kg, hygroscopic fibre 50Kg, carries out blending, and obtained number is two component blended yarns of 80/2, the specification that two component blended yarn and Japanese Zhong Fang company are produced is the conductive filament of 20D/3F and twists with the fingers, the obtained twist is the conductive yam of 55 sth. made by twisting/10cm, and use air-jet loom to weave, in weaving process, interval inweaves conductive yam, obtained antistatic grid grey cloth, wherein, the spacing of warp-wise conductive filament is 2.0cm, and the spacing of broadwise conductive filament is 0.5cm;
Step 2: take 4Kg dyestuff, is dissolved in water, is stirred, regulator solution pH to 7.5, dyes to step 1 woven antistatic grid grey cloth;
Step 3: take 7.5Kg fire retardant FPK8002,1Kg magnesium chloride, 0.15Kg soluble polyurethane and 0.1Kg acetic acid respectively, be placed in 50L water and dissolve, obtain solution; Being poured into by solution pads in groove, pads step 2 gained painting cloth, and pick-up is 70%;
Step 4: step 3 was padded the fabric of fire retarding treating liquid through 105 DEG C of oven dry, 180 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
The two component fire-resistant antistatic fabric of embodiment of the present invention gained, under environment temperature is (20 ± 2) DEG C, relative humidity (65 ± 4) % condition, test its point-to-point resistance, anti-flammability, air penetrability, water-fastness COLOR FASTNESS, colour fastness to rubbing, ultimate strength and tearing brute force, all reach the requirement of fabric taking; Wherein, flame retardant effect and the antistatic performance of fabric are better: oxygen index (OI) more than 30, and damage below length 150mm, below after flame time 5s, glow time below 5s, more than ultimate strength 450N, TEAR STRENGTH more than 25N, water-fastness; The B level requirement that the anti-flammability of fabric is up to state standards in GB 8965.1-2009, static electricity resistance stabilizability reaches the A level requirement in standard GB/T 12014-2009.
In the preparation process of the two component fire-resistant antistatic fabric of the present invention, the twist of the quality of conductive filament, the amount of inweaving and conductive yam directly affects the antistatic performance of fabric, under the condition of the same amount of inweaving of same conductive silk, when the twist of conductive yam is excessive or the too small twist that all can affect fabric antistatic performance conductive yam is greater than 60 sth. made by twisting/10cm, fabric antistatic performance is unstable; The twist of conductive yam is when 25 ~ 55 sth. made by twisting/10cm, and fabric antistatic performance is stablized; When the twist of conductive yam is less than 25 sth. made by twisting/10cm, fabric antistatic performance is stablized, but affects fabric outward appearance and feel.According to the environment for use of fabric, coordinate grid weave to inweave appropriate conductive yam, thus prepare the good and good antistatic fabric of appearance of fabrics feel of antistatic performance.
The present invention adds a small amount of auxiliary agent rolling in material, the adding of auxiliary agent be conducive to fire retardant and penetrate into fabric, it is made to adhere to each filamentary surface in the yarn, after drying, the fiber surface of yarn interior can be retained in, part fire retardant is coated in fabric face, makes its surface form fire-retardant tunic, improves COLOR FASTNESS and the flame retardant effect of fabric further; Auxiliary agent penetrates into yarn interior, can increase the adhesion strength in yarn between filament, makes its boundling of uniting, and strengthens brute force and the anti-wear performance of fabric.
Claims (10)
1. a two component fire-resistant antistatic fabric, is characterized in that, obtains according to following steps preparation:
Step 1: grey cloth is weaved
Choose the raw material of the two component blended yarn of cotton fiber and hygroscopic fibre as face weave, by conductive filament and blended yarn and twisting obtains conductive yam, in weaving process, interval inweaves conductive yam, obtains antistatic grid grey cloth;
Step 2: dyeing process
Take dyestuff, be dissolved in water, stir, obtain the dye liquor that concentration is 20 ~ 80g/L, regulator solution pH to 4 ~ 7.5, step 1 woven antistatic grid grey cloth is dyeed;
Step 3: flame-proof treatment
Be that 5.5 ~ 7.5:1 takes fire retardant and magnesium chloride in mass ratio, and add appropriate amount of addition agent, be placed in water and dissolve, stir, obtaining concentration is the solution of 135 ~ 175g/L, being poured into by solution pads in groove, and the mode adopting a leaching one to roll is padded step 2 gained painting cloth, and pick-up is 60% ~ 80%;
Step 4: drying and processing
Step 3 was padded the fabric of fire retarding treating liquid through 95 ~ 105 DEG C of oven dry, 180 ~ 200 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
2. a kind of two component fire-resistant antistatic fabric according to claim 1, it is characterized in that, in step 1, raw-materially in two component blended yarn to consist of: cotton fiber 40% ~ 60%, hygroscopic fibre 40% ~ 60%, above each weight percentages of components sum is 100%.
3. a kind of two component fire-resistant antistatic fabric according to claim 1, it is characterized in that, in step 1, conductive filament is the one in nylon based conductive fiber long filament, terylene base conductive fiber long filament or black carbon fiber electrically conductive filament, and the twist of gained conductive yam is 25 ~ 55 sth. made by twisting/10cm.
4. a kind of two component fire-resistant antistatic fabric according to claim 1, it is characterized in that, in step 1, the spacing of antistatic grid grey cloth warp-wise conductive filament is 0.5 ~ 2.0cm, the spacing of broadwise conductive filament is 0.5 ~ 2.0cm, fabric warp density range is 50 ~ 200/10cm, and weft count scope is 50 ~ 150/10cm.
5. a kind of two component fire-resistant antistatic fabric according to claim 1, it is characterized in that, in step 3, fire retardant is FPK8002, and auxiliary agent is soluble polyurethane and acetic acid, and the mass ratio of its addition and retardant load level is 1:22 ~ 30.
6. a preparation method for two component fire-resistant antistatic fabric, is characterized in that, specifically prepare according to following steps:
Step 1: grey cloth is weaved
Choose the raw material of the two component blended yarn of cotton fiber and hygroscopic fibre as face weave, by conductive filament and blended yarn and twisting obtains conductive yam, in weaving process, interval inweaves conductive yam, obtains antistatic grid grey cloth;
Step 2: dyeing process
Take dyestuff, be dissolved in water, stir, obtain the dye liquor that concentration is 20 ~ 80g/L, regulator solution pH to 4 ~ 7.5, step 1 woven antistatic grid grey cloth is dyeed;
Step 3: flame-proof treatment
Be that 5.5 ~ 7.5:1 takes fire retardant and magnesium chloride in mass ratio, and add appropriate amount of addition agent, be placed in water and dissolve, stir, obtaining concentration is the solution of 135 ~ 175g/L, being poured into by solution pads in groove, and the mode adopting a leaching one to roll is padded step 2 gained painting cloth, and pick-up is 60% ~ 80%;
Step 4: drying and processing
Step 3 was padded the fabric of fire retarding treating liquid through 95 ~ 105 DEG C of oven dry, 180 ~ 200 DEG C bake after, cooling, obtain fire-resistant antistatic fabric.
7. the preparation method of a kind of pair of component fire-resistant antistatic fabric according to claim 6, it is characterized in that, in step 1, raw-materially in two component blended yarn to consist of: cotton fiber 40% ~ 60%, hygroscopic fibre 40% ~ 60%, above each weight percentages of components sum is 100%.
8. the preparation method of a kind of pair of component fire-resistant antistatic fabric according to claim 6, it is characterized in that, in step 1, conductive filament is the one in nylon based conductive fiber long filament, terylene base conductive fiber long filament or black carbon fiber electrically conductive filament, and the twist of gained conductive yam is 25 ~ 55 sth. made by twisting/10cm.
9. the preparation method of a kind of pair of component fire-resistant antistatic fabric according to claim 6, it is characterized in that, in step 1, the spacing of antistatic grid grey cloth warp-wise conductive filament is 0.5 ~ 2.0cm, the spacing of broadwise conductive filament is 0.5 ~ 2.0cm, fabric warp density range is 50 ~ 200/10cm, and weft count scope is 50 ~ 150/10cm.
10. the preparation method of a kind of pair of component fire-resistant antistatic fabric according to claim 6, it is characterized in that, in step 3, fire retardant is FPK8002, and auxiliary agent is soluble polyurethane and acetic acid, and the mass ratio of its addition and retardant load level is 1:22 ~ 30.
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| CN107268131A (en) * | 2017-06-07 | 2017-10-20 | 丹阳市斯鲍特体育用品有限公司 | A kind of fencing metallic plastron fabric is twisted thread with conductive silver fiber |
| CN110565238A (en) * | 2019-09-29 | 2019-12-13 | 陕西锦澜科技有限公司 | Cotton-nylon blended fabric of anti-static moisture-absorption sweat-discharge jean and preparation method thereof |
| CN110629361A (en) * | 2019-09-29 | 2019-12-31 | 陕西锦澜科技有限公司 | Moisture-absorbing, sweat-releasing, anti-static and anti-ultraviolet cotton-nylon blended fabric and preparation method thereof |
| CN110656420A (en) * | 2019-09-29 | 2020-01-07 | 陕西锦澜科技有限公司 | Anti-static moisture-absorbing sweat-discharging cotton-nylon blended fabric and preparation method thereof |
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| CN107268131A (en) * | 2017-06-07 | 2017-10-20 | 丹阳市斯鲍特体育用品有限公司 | A kind of fencing metallic plastron fabric is twisted thread with conductive silver fiber |
| CN110565238A (en) * | 2019-09-29 | 2019-12-13 | 陕西锦澜科技有限公司 | Cotton-nylon blended fabric of anti-static moisture-absorption sweat-discharge jean and preparation method thereof |
| CN110629361A (en) * | 2019-09-29 | 2019-12-31 | 陕西锦澜科技有限公司 | Moisture-absorbing, sweat-releasing, anti-static and anti-ultraviolet cotton-nylon blended fabric and preparation method thereof |
| CN110656420A (en) * | 2019-09-29 | 2020-01-07 | 陕西锦澜科技有限公司 | Anti-static moisture-absorbing sweat-discharging cotton-nylon blended fabric and preparation method thereof |
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| CN104762721B (en) | 2016-08-24 |
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