CN104762019A - Surface polishing agent for battery connection elastic piece and preparation method of surface polishing agent - Google Patents
Surface polishing agent for battery connection elastic piece and preparation method of surface polishing agent Download PDFInfo
- Publication number
- CN104762019A CN104762019A CN201510147425.XA CN201510147425A CN104762019A CN 104762019 A CN104762019 A CN 104762019A CN 201510147425 A CN201510147425 A CN 201510147425A CN 104762019 A CN104762019 A CN 104762019A
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- CN
- China
- Prior art keywords
- surface polishing
- polishing agent
- agent
- shell fragment
- stearate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/14—Other polishing compositions based on non-waxy substances
- C09G1/18—Other polishing compositions based on non-waxy substances on other substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
Abstract
The invention discloses a surface polishing agent for a battery connection elastic piece and a preparation method of a surface polishing agent. In order to overcome the defects of the existing polishing agent, the surface polishing agent is prepared from an inorganic acid, stearate, glycerol, acrylics, a carboxylate compound, sodium allysulfonate, a surfacant, silicon oil, a stabilizer, a defoamer, a wetting agent, a catalyst and a dispersant as well as water by virtue of a certain preparation method. The surface polishing agent for the battery connection elastic piece disclosed by the invention has the advantage of good polishing quality;a polished elastic piece is high in brightness and is not corroded; an abrasive material has good dispersibility; the stability of the composition is good; the defects of the conventional polishing agent are abandoned. The effect of ensuring the polished surface smoothness of the surface polishing agent for the battery connection elastic piece and avoiding corrosion is remarkable. In addition, the preparation method is simple and easy to operate and low in cost.
Description
Technical field
The present invention relates to a kind of rumbling compound and preparation thereof, especially relate to a kind of battery and connect shell fragment surface polishing agent and preparation method thereof.
Background technology
The microstructure of metallic substance directly has influence on the performance and used life of mechanical component, and metallurgical analysis is the important means controlling mechanical component inner quality.At novel material, novel process, in the research and development of product innovation, in the scientific research improving metal products inner quality, all be unable to do without Metallographic Techniques analysis.
In the process that Metallographic Techniques are analyzed, polishing is a very important step, and polishing refers to and utilizes machinery, chemistry or electrochemical effect, workpiece surface roughness is reduced, to obtain the working method of light, flat surface.The object of polishing removes the polishing scratch on metallographic flour milling, and obtain smooth sightingpiston, the height of quality of finish directly determines the quality of metallographic detection faces.Polishing mainly contains mechanical polishing, chemical rightenning and electropolishing, chemical rightenning by chemical reagent, the selective dissolution effect in the uneven region of sample surfaces is eliminated to polishing scratch, corroded a kind of method of leveling, it is simple to operate, do not need by mechanical means, on-the-spot fitness is high, easy to carry, be very suitable for on-the-spot metallographic and make use.
The material that battery connects shell fragment is generally stainless steel and phosphor-copper steel, stainless steel hardness is lower, belong to the metal of more difficult polishing, traditional method is the mode with mechanical polishing and electropolishing, but scene does not often satisfy the requirements, mechanical polishing and electropolishing mode cannot use, therefore, scene makes the metallographic of parts of stainless steel, the chemical rightenning of polishing way selection more for convenience, the stainless steel polishing agent polishing ability that existing chemical rightenning uses, the dispersiveness of abrasive material is bad, composition less stable is comparatively serious to the corrosion phenomenon connecting shell fragment after polishing.
Summary of the invention
Goal of the invention: existing rumbling compound polishing ability, composition less stable, abrasive material dispersiveness are bad in order to solve in prior art, problem serious to the corrosion phenomenon connecting shell fragment after polishing, the present invention proposes high, the corrosion-free phenomenon of a kind of polished shell fragment luminance brightness, abrasive material good dispersity and the good battery of composition stability connects shell fragment surface polishing agent and preparation method thereof.
Technical scheme: to achieve these objectives, the present invention takes following technical scheme: a kind of battery connects shell fragment surface polishing agent, be prepared from by following component according to weighing scale: mineral acid 10-15 part, stearate 20-30 part, glycerine 12-18 part, esters of acrylic acid 12-16 part, carboxylate compounds 5-15 part, sodium allyl sulfonate 5-10 part, tensio-active agent 16-20 part, silicone oil 10-20 part, stablizer 6-8 part, defoamer 10-12 part, wetting agent 5-13 part, catalyzer 3-9 part, dispersion agent 22-28 part, water 20-40 part.
Further, described mineral acid is complex acid.
Further, described stearate is water-based stearate.
Further, described water-based stearate is one or both in water-based calcium stearate, water-based aluminum stearate, water-based zinc stearate.
Further, described carboxylate compounds is one or both in phenyl dicarboxylic acid compound, tricarboxylic acid compound.
Further, described tensio-active agent is amphoteric ionic surfactant.
Further, described amphoteric ionic surfactant is amino acid type amphoteric ionogenic surfactant.
Further, described stablizer is compound stablizer, is specially the mixture of triphenyl phosphite and aluminium salt.
Further, the carrier of described catalyzer is diatomite, and catalytic active component is Ni or Pd.
Further, described defoamer is higher alcohols defoamer.
Further, described dispersion agent is macromolecule dispersing agent.
Above-mentioned battery connects the preparation method of shell fragment surface polishing agent, it is characterized in that comprising the following steps:
(1) by the mineral acid of required weight, stearate, carboxylate compounds, sodium allyl sulfonate, stablizer, catalyzer and defoamer mixing and stirring post-heating to 70-80 DEG C, insulation 15-18min after be cooled to room temperature;
(2) with dispersion agent, tensio-active agent, glycerine, silicone oil and wetting agent, esters of acrylic acid is scattered in water, makes dispersion liquid;
(3) insulation 10-20min when adding dispersion liquid that step (2) makes and be heated to 90 DEG C in the solvent made by step (1), is cooled to room temperature and obtains required battery and connect shell fragment surface polishing agent after continuing to be heated to 100 DEG C while stirring after being incubated 40-60min.
Beneficial effect: a kind of battery provided by the invention connects shell fragment surface polishing agent and preparation method thereof, for the defect that existing rumbling compound exists, by mineral acid, stearate, glycerine, esters of acrylic acid, carboxylate compounds, sodium allyl sulfonate, tensio-active agent, silicone oil, stablizer, defoamer, wetting agent, catalyzer part, dispersion agent part, and water is made according to certain preparation method, battery of the present invention connects shell fragment surface polishing agent, not only there is the advantage that quality of finish is good, polished shell fragment luminance brightness is high, corrosion-free phenomenon, abrasive material good dispersity and composition stability has better abandoned the defective of traditional rumbling compound, what connect the glazed surface planeness of shell fragment surface polishing agent and the phenomenon that is corroded for battery avoids Be very effective, in addition its preparation method is simple to operation, with low cost.
Embodiment
Embodiment 1:
A kind of battery connects shell fragment surface polishing agent, be prepared from by following component according to weighing scale: mineral acid 10 parts, stearate 20 parts, glycerine 12 parts, esters of acrylic acid 12 parts, carboxylate compounds 5 parts, sodium allyl sulfonate 5 parts, 16 parts, tensio-active agent, silicone oil 10 parts, stablizer 6 parts, defoamer 10 parts, wetting agent 5 parts, catalyzer 3 parts, dispersion agent 22 parts, 20 parts, water.
Wherein, described mineral acid is complex acid; Described stearate is that water-based stearate is specially water-based calcium stearate and water-based aluminum stearate mass ratio is the mixture of 1:3; Described carboxylate compounds is phenyl dicarboxylic acid compound; Described tensio-active agent is amino acid type amphoteric ionogenic surfactant; Described stablizer is compound stablizer, is specially the mixture of triphenyl phosphite and aluminium salt; The carrier of described catalyzer is diatomite, and catalytic active component is Ni; Described defoamer is higher alcohols defoamer; Described dispersion agent is macromolecule dispersing agent.
Above-mentioned battery connects the preparation method of shell fragment surface polishing agent, it is characterized in that comprising the following steps:
(1) by the mineral acid of required weight, stearate, carboxylate compounds, sodium allyl sulfonate, stablizer, catalyzer and defoamer mixing and stirring post-heating to 70 DEG C, after insulation 15min, room temperature is cooled to;
(2) with dispersion agent, tensio-active agent, glycerine, silicone oil and wetting agent, esters of acrylic acid is scattered in water, makes dispersion liquid;
(3) insulation 10min when adding dispersion liquid that step (2) makes and be heated to 90 DEG C in the solvent made by step (1), is cooled to room temperature and obtains required battery and connect shell fragment surface polishing agent after continuing to be heated to 100 DEG C while stirring after being incubated 40min.
Embodiment 2:
A kind of battery connects shell fragment surface polishing agent, is prepared from: mineral acid 15 parts, stearate 30 parts, glycerine 18 parts, esters of acrylic acid 16 parts, carboxylate compounds 15 parts, sodium allyl sulfonate 10 parts, 20 parts, tensio-active agent, silicone oil 20 parts, stablizer 8 parts, defoamer 12 parts, wetting agent 13 parts, catalyzer 9 parts, dispersion agent 28 parts, 40 parts, water according to weighing scale by following component.
Wherein, described mineral acid is complex acid; Described stearate is water-based aluminum stearate and water-based zinc stearate mass ratio is the mixture of 2:1; Described carboxylate compounds is tricarboxylic acid compound; Described tensio-active agent is amino acid type amphoteric ionogenic surfactant; Described stablizer is compound stablizer, is specially the mixture of triphenyl phosphite and aluminium salt; The carrier of described catalyzer is diatomite, and catalytic active component is Pd; Described defoamer is higher alcohols defoamer; Described dispersion agent is macromolecule dispersing agent.
Above-mentioned battery connects the preparation method of shell fragment surface polishing agent, it is characterized in that comprising the following steps:
(1) by the mineral acid of required weight, stearate, carboxylate compounds, sodium allyl sulfonate, stablizer, catalyzer and defoamer mixing and stirring post-heating to 80 DEG C, after insulation 18min, room temperature is cooled to;
(2) with dispersion agent, tensio-active agent, glycerine, silicone oil and wetting agent, esters of acrylic acid is scattered in water, makes dispersion liquid;
(3) insulation 20min when adding dispersion liquid that step (2) makes and be heated to 90 DEG C in the solvent made by step (1), is cooled to room temperature and obtains required battery and connect shell fragment surface polishing agent after continuing to be heated to 100 DEG C while stirring after being incubated 60min.
Embodiment 3:
A kind of battery connects shell fragment surface polishing agent, be prepared from by following component according to weighing scale: mineral acid 13 parts, stearate 25 parts, glycerine 15 parts, esters of acrylic acid 14 parts, carboxylate compounds 10 parts, sodium allyl sulfonate 8 parts, 18 parts, tensio-active agent, silicone oil 15 parts, stablizer 7 parts, defoamer 11 parts, wetting agent 9 parts, catalyzer 6 parts, dispersion agent 25 parts, 300 parts, water.
Wherein, described mineral acid is complex acid; Described stearate is water-based zinc stearate; Described tensio-active agent is amino acid type amphoteric ionogenic surfactant; Described stablizer is compound stablizer, is specially the mixture of triphenyl phosphite and aluminium salt; The carrier of described catalyzer is diatomite, and catalytic active component is Ni; Described defoamer is higher alcohols defoamer; Described dispersion agent is macromolecule dispersing agent.
Above-mentioned battery connects the preparation method of shell fragment surface polishing agent, it is characterized in that comprising the following steps:
(1) by the mineral acid of required weight, stearate, carboxylate compounds, sodium allyl sulfonate, stablizer, catalyzer and defoamer mixing and stirring post-heating to 75 DEG C, after insulation 17min, room temperature is cooled to;
(2) with dispersion agent, tensio-active agent, glycerine, silicone oil and wetting agent, esters of acrylic acid is scattered in water, makes dispersion liquid;
(3) insulation 15min when adding dispersion liquid that step (2) makes and be heated to 90 DEG C in the solvent made by step (1), is cooled to room temperature and obtains required battery and connect shell fragment surface polishing agent after continuing to be heated to 100 DEG C while stirring after being incubated 50min.
A kind of battery of above-described embodiment 1-3 is used to connect the rumbling compound of shell fragment surface polishing agent and preparation method thereof preparation, through connecting the polishing test of shell fragment to battery, result shows, more traditional rumbling compound is compared, the polishing effect that battery of the present invention connects shell fragment surface polishing agent is good, battery connects shell fragment without aculea phenomenon, planeness is good, corrosion-free, in addition, not only there is the advantage that quality of finish is good, polished shell fragment luminance brightness is high, corrosion-free phenomenon, abrasive material good dispersity and composition stability is better, the connection shell fragment scrap rate of polishing reduces more than 90%, abandon the defective of traditional rumbling compound, in addition its preparation method is simple to operation, with low cost, there is very strong practicality.
It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, can also make some improvement, these improvement also should be considered as protection scope of the present invention.
Claims (12)
1. a battery connects shell fragment surface polishing agent, it is characterized in that being prepared from by following component according to weighing scale: mineral acid 10-15 part, stearate 20-30 part, glycerine 12-18 part, esters of acrylic acid 12-16 part, carboxylate compounds 5-15 part, sodium allyl sulfonate 5-10 part, tensio-active agent 16-20 part, silicone oil 10-20 part, stablizer 6-8 part, defoamer 10-12 part, wetting agent 5-13 part, catalyzer 3-9 part, dispersion agent 22-28 part, water 20-40 part.
2. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described mineral acid is complex acid.
3. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described stearate is water-based stearate.
4. battery according to claim 3 connects shell fragment surface polishing agent, it is characterized in that: described water-based stearate is one or both in water-based calcium stearate, water-based aluminum stearate, water-based zinc stearate.
5. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described carboxylate compounds is one or both in phenyl dicarboxylic acid compound, tricarboxylic acid compound.
6. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described tensio-active agent is amphoteric ionic surfactant.
7. battery according to claim 4 connects shell fragment surface polishing agent, it is characterized in that: described amphoteric ionic surfactant is amino acid type amphoteric ionogenic surfactant.
8. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described stablizer is compound stablizer, is specially the mixture of triphenyl phosphite and aluminium salt.
9. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: the carrier of described catalyzer is diatomite, and catalytic active component is Ni or Pd.
10. battery according to claim 1 connects shell fragment surface polishing agent, it is characterized in that: described defoamer is higher alcohols defoamer.
11. batteries according to claim 1 connect shell fragment surface polishing agent, it is characterized in that: described dispersion agent is macromolecule dispersing agent.
12. 1 kinds of batteries according to claim 1 connect the preparation method of shell fragment surface polishing agent, it is characterized in that comprising the following steps:
(1) by the mineral acid of required weight, stearate, carboxylate compounds, sodium allyl sulfonate, stablizer, catalyzer and defoamer mixing and stirring post-heating to 70-80 DEG C, insulation 15-18min after be cooled to room temperature;
(2) with dispersion agent, tensio-active agent, glycerine, silicone oil and wetting agent, esters of acrylic acid is scattered in water, makes dispersion liquid;
(3) insulation 10-20min when adding dispersion liquid that step (2) makes and be heated to 90 DEG C in the solvent made by step (1), is cooled to room temperature and obtains required battery and connect shell fragment surface polishing agent after continuing to be heated to 100 DEG C while stirring after being incubated 40-60min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510147425.XA CN104762019A (en) | 2015-04-01 | 2015-04-01 | Surface polishing agent for battery connection elastic piece and preparation method of surface polishing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510147425.XA CN104762019A (en) | 2015-04-01 | 2015-04-01 | Surface polishing agent for battery connection elastic piece and preparation method of surface polishing agent |
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| CN104762019A true CN104762019A (en) | 2015-07-08 |
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| CN201510147425.XA Pending CN104762019A (en) | 2015-04-01 | 2015-04-01 | Surface polishing agent for battery connection elastic piece and preparation method of surface polishing agent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114107973A (en) * | 2021-12-02 | 2022-03-01 | 贵州华烽电器有限公司 | Surface treatment method for corrugated elastic sheet of electric connector |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101654599A (en) * | 2009-07-03 | 2010-02-24 | 江苏海迅实业集团股份有限公司 | Chemical mechanical polishing composite of stainless steel surface polishing |
| CN103642398A (en) * | 2013-11-28 | 2014-03-19 | 上海航天精密机械研究所 | Polishing liquid for stainless steel material and use thereof |
| CN104194648A (en) * | 2014-09-10 | 2014-12-10 | 句容金猴机械研究所有限公司 | Stainless steel material polishing agent for mechanical equipment and preparation method of stainless steel material polishing agent |
-
2015
- 2015-04-01 CN CN201510147425.XA patent/CN104762019A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101654599A (en) * | 2009-07-03 | 2010-02-24 | 江苏海迅实业集团股份有限公司 | Chemical mechanical polishing composite of stainless steel surface polishing |
| CN103642398A (en) * | 2013-11-28 | 2014-03-19 | 上海航天精密机械研究所 | Polishing liquid for stainless steel material and use thereof |
| CN104194648A (en) * | 2014-09-10 | 2014-12-10 | 句容金猴机械研究所有限公司 | Stainless steel material polishing agent for mechanical equipment and preparation method of stainless steel material polishing agent |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114107973A (en) * | 2021-12-02 | 2022-03-01 | 贵州华烽电器有限公司 | Surface treatment method for corrugated elastic sheet of electric connector |
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Application publication date: 20150708 |
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