CN104745335A - Resin lens cleaning agent and preparation method thereof - Google Patents
Resin lens cleaning agent and preparation method thereof Download PDFInfo
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- CN104745335A CN104745335A CN201510054658.5A CN201510054658A CN104745335A CN 104745335 A CN104745335 A CN 104745335A CN 201510054658 A CN201510054658 A CN 201510054658A CN 104745335 A CN104745335 A CN 104745335A
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- resin lens
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- deionized water
- cleaning agent
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Abstract
The invention discloses a resin lens cleaning agent. According to 100 parts by weight, the resin lens cleaning agent comprises the following active ingredients: 15-25 parts of N,N-dimethyl formamide (DMF) solution, 0.2-0.3 part of ethylenediamine, 4-6 parts of potassium dihydrogen phosphate-potassium dihydrogen phosphate, 13-20 parts of sodium lauroamphoacetate, 8-12 parts of ethylene glycol solution and the balance of deionized water solution. The preparation method comprises the following steps: placing all the components into a dosing tank, and fully stirring to obtain the resin lens cleaning agent. According to the resin lens cleaning agent, the decontamination rate of the formed lens is not less than 99%, and the resin lens cleaning agent has no damage to the lens; the resin lens cleaning agent is low in wetting degree on the surface of the lens, and the resin lens cleaning agent and the residual contamination on the lens can be separated from the lens from the surface of the lens only by slightly throwing after the lens is cleaned with the resin lens cleaning agent, and the resin lens cleaning agent is not volatilized, decomposed and combusted, and is safe to use, and the resin lens cleaning agent is an environment-friendly alkaline water-soluble liquid cleaning agent without halogenated hydrocarbon.
Description
Technical field
The present invention relates to a kind of clean-out system, be specifically related to a kind of resin lens clean-out system and preparation method thereof.
Background technology
Non-contact ophthalmic lens is very accurate optics, especially epoxy resin eyeglass, crystal eyeglass etc., the coating process of antireflection has been done on its surface, especially after eyeglass is shaping, if surface adhesion oil stain and fingerprint, very large to coating damage, optical property and the image quality of eyeglass can be affected, further injury can be caused to the eyesight of user.Cleaning eyeglass cannot at will use other chemical substances, this is because the chemical of other kinds is not special is cleaning lens design, so clean-out system likely can have certain damage to resin lens and coating, and may not wash clean clearly shaping rear residual resin-lint, fingerprint.The formula of some clean-out system uses ether and alcohol in the past, can leave the oil membrane after ether volatilization after cleaning, can affect to painting anti-reflection layer, as reference Shu Weiguo, and matting, Beijing Aeronautics Research Inst, 1993.
Eyeglass after a procedure, also can be stained with some dusts, also can enclose sweat mark, fruit juice, hair spray, makeup etc., this just needs to use special lens cleaning agent cleaning, seem soft paper handkerchief wiping if used, the wood pulp comprised in paper is than the coating be easier on scratch eyeglass.Before wiping, should guarantee without visible dust granule on eyeglass, to avoid mill presbyopic glasses sheet.Meanwhile, note wiping gimmick, cannot wiping repeatedly back and forth, Ying Cong center to periphery gently along the wiping of same direction.When using clean-out system, should not directly clean-out system be dropped on eyeglass, wiping eyeglass in specialized lens cleaning wiping cloth should be bonded at.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the invention provides a kind of resin lens clean-out system and preparation method thereof, can the dirt such as resin, binding agent, fingerprint, grinding slag that adheres to of Scavenger resin eyeglass or die surface up hill and dale rapidly, to eyeglass or die surface not damaged.
Technical scheme: for solving the problems of the technologies described above, a kind of resin lens clean-out system of the present invention, this resin lens clean-out system based on 100 weight parts comprises the deionized water of DMF (DMF) solution 15 ~ 25 parts, quadrol 0.2 ~ 0.3 part, potassium primary phosphate-dipotassium hydrogen phosphate 4 ~ 6 parts, LAA 13 ~ 20 parts, ethylene glycol solution 8 ~ 12 parts and its surplus.
As preferably, this resin lens clean-out system based on 100 weight parts is the deionized water of DMF (DMF) solution 25 parts, quadrol 0.25 part, potassium primary phosphate-dipotassium hydrogen phosphate 5 parts, LAA 17 parts, ethylene glycol solution 10 parts and its surplus.
A preparation method for resin lens clean-out system, comprises the following steps:
(1) take a certain amount of deionized water, join in material-compound tank, start stirrer and stir, open heating system, heating deionized water also controls deionized water temperature;
(2) take a certain amount of DMF (DMF) solution and join material-compound tank, be stirred to solution transparent;
(3) taking a certain amount of potassium primary phosphate-dipotassium hydrogen phosphate joins in material-compound tank, is stirred to solution transparent;
(4) taking a certain amount of LAA joins in material-compound tank, continues Keep agitation 15-20 minute, transparent to solution;
(5) taking a certain amount of quadrol joins in material-compound tank, stirs;
(6) take a certain amount of deionized water and scrub the equipment taking up raw material, then washing lotion is poured in material-compound tank, stir evenly to solution transparent;
(7) taking a certain amount of antifreeze membrane-forming agent ethylene glycol joins in tank, stirs evenly to solution transparent, is cooled to room temperature and can obtains product of the present invention.
As preferably, in described step (1), stirrer stir speed (S.S.) is 35-45r/min.
As preferably, in described step (1), deionized water temperature controls at 55-65 DEG C.
Adding of potassium primary phosphate-dipotassium hydrogen phosphate and LAA, following effect can be played: make the pH value of clean-out system can remain stable, have good provide protection to resin lens and film; LAA can reduce profit surface tension, can increase emulsifying capacity and the emulsifying stability of clean-out system, can increase emulsifying capacity and the emulsifying stability of clean-out system; Solution can be made to have the ability of good suspending power and stable system, can prevent dirt sedimentation again, use temperature and the concentration of preparation clean-out system should be determined by specific experiment.
In the process of this product of preparation, add the antifreeze membrane-forming agent of ethylene glycol, clean-out system also can normally be used under the environment of subzero about 30 DEG C; Quadrol, as sequestrant, can improve the dispersive ability of other compositions, improves washability; DMF (DMF) solution added in the solution, Main Function is make the insoluble substance on resin lens become soluble substance.
Beneficial effect: resin lens clean-out system of the present invention, more than 99% is reached to the eyeglass scrubbing rate after shaping, to eyeglass not damaged, be only about 60%-80% relative to cleaning rate, and have the existing organic solvent of damage to be greatly improved to eyeglass and coating; And the degree of wetting of this product to lens surface is low, under only needing whipping gently several after using this product to clean eyeglass, spot residual on clean-out system and eyeglass just can be made to depart from eyeglass, and clean-out system of the present invention is non-volatile, do not decompose, do not burn, use safety, and this product is a kind of green alkaline water soluble liq clean-out system not containing halohydrocarbon; Operating process is simple, quick, has significant cleaning performance and has the function of protective lens UV resistance coating.
Embodiment
Embodiment 1
Guarantee output zone and equipment clean and dry, material-compound tank is cleaned up and sterilizes, and whole valve closes.The production process of this product is simple mixing.
Take the deionized water of 30 kilograms, add in material-compound tank, start agitator, stir speed (S.S.) is at about 40r/min.Open heating system, deionized water is heated to about 60 DEG C, and keeps constant temperature;
The DMF (DMF) taking 25 kilograms joins in tank, is stirred to solution transparent;
Potassium primary phosphate-the dipotassium hydrogen phosphate taking 6 kilograms joins in tank, is stirred to solution transparent;
The LAA taking 20 kilograms joins in tank, continues Keep agitation 15-20 minute, transparent to solution;
The quadrol taking 0.3 kilogram joins in tank, continues to stir;
The deionized water taking 6.7 kilograms scrubs the equipment taking up raw material, then pours in reaction by washing lotion, stirs evenly to solution transparent;
The antifreeze membrane-forming agent ethylene glycol taking 12 kilograms joins in tank, stirs evenly to solution transparent.
Embodiment 2
Guarantee output zone and equipment clean and dry, material-compound tank is cleaned up and sterilizes, and whole valve closes, stirrer stirring velocity is 45r/min.The production process of this product is the simple mixing of material, and deionized water temperature controls at 55 DEG C.
Formula is: the deionized water of 30 kilograms, the N of 15 kilograms, dinethylformamide (DMF), potassium primary phosphate-the dipotassium hydrogen phosphate of 4 kilograms, the deionized water (for scrubbing the equipment taking up raw material) of 29.8 kilograms, the LAA of 13 kilograms, the quadrol of 0.2 kilogram, the antifreeze membrane-forming agent ethylene glycol of 8 kilograms.
Then according to preparation method's preparing product of embodiment 1.
Embodiment 3
Guarantee output zone and equipment clean and dry, material-compound tank is cleaned up and sterilizes, and all valve closes stirrer stirring velocity is 45r/min.The production process of this product is the simple mixing of material, and deionized water temperature controls at 58 DEG C.
Formula is: the deionized water of 25 kilograms, the N of 17 kilograms, dinethylformamide (DMF), potassium primary phosphate-the dipotassium hydrogen phosphate of 5 kilograms, the deionized water (for scrubbing the equipment taking up raw material) of 27.75 kilograms, the LAA of 15 kilograms, the quadrol of 0.25 kilogram, the antifreeze membrane-forming agent ethylene glycol of 10 kilograms.
Then according to preparation method's step preparing product of embodiment 1.
Embodiment 4
Guarantee output zone and equipment clean and dry, material-compound tank is cleaned up and sterilizes, and all valve closes stirrer stirring velocity is 45r/min.The production process of this product is the simple mixing of material, and deionized water temperature controls at 60 DEG C.
Formula is: the deionized water of 30 kilograms, the N of 25 kilograms, dinethylformamide (DMF), potassium primary phosphate-the dipotassium hydrogen phosphate of 5 kilograms, the deionized water (for scrubbing the equipment taking up raw material) of 15.75 kilograms, the LAA of 15 kilograms, the quadrol of 0.25 kilogram, the antifreeze membrane-forming agent ethylene glycol of 9 kilograms.
Then according to preparation method's step preparing product of embodiment 1.
Embodiment 5
Guarantee output zone and equipment clean and dry, material-compound tank is cleaned up and sterilizes, and all valve closes stirrer stirring velocity is 44r/min.The production process of this product is the simple mixing of material, and deionized water temperature controls at 62 DEG C.
Formula is: the deionized water of 30 kilograms, the N of 24 kilograms, dinethylformamide (DMF), potassium primary phosphate-the dipotassium hydrogen phosphate of 4 kilograms, the deionized water (for scrubbing the equipment taking up raw material) of 19.7 kilograms, the LAA of 13 kilograms, the quadrol of 0.3 kilogram, the antifreeze membrane-forming agent ethylene glycol of 9 kilograms.Then according to preparation method's step preparing product of embodiment 1.
Conclusion
Through the cleaning to resin lens after shaping, the cleaning performance of clean-out system prepared by embodiment 1 ~ 5 is all more than 80%, especially the cleaning performance of embodiment 1 and 4 is more than 99%, illustrates that DMF (DMF) plays a significant role in this clean-out system.Resin lens surface after cleaning is without dirts such as resin chip, binding agent, fingerprints, impact be there is no on the shaping rear painting anti-reflection coating of eyeglass, the resin lens after coating is cleaned, there is no clean-out system and remain, and to coating not damaged, be the optimal qualified product of cleaning resin lens.
Cleaning performance
Can the dirt such as resin, binding agent, fingerprint, grinding slag that adheres to of Scavenger resin eyeglass or die surface up hill and dale rapidly, to eyeglass or die surface not damaged.
Applicable object
1, the cleaning after resin lens grinding is applicable to;
2, the cleaning of the shaping rear glass grinding tool of resin lens is applicable to.
Using method
1, ultrasonic cleaning, immersion can be adopted, close the method cleanings such as spray;
2, use stoste cleaning, ultrasonic wave, immersion way cleaning, time general recommendations is 1-3 minute, and use temperature is generally 40-60 DEG C, and user can determine the optimal clean time according to test.
Safeguard
1, when cleaning performance obviously declines, can supplement stoste, its cleansing power will recover as before.
2, as floating in cleaning liquid level have a lot of greasy dirt, greasy dirt can be skimmed.
3, as cleansing power can not reach original level after supplementing, then that can abandon more renews liquid.
Precaution
1, this product can not be used in combination with other clean-out system.
If 2 are splashed in eye accidentally, rinse well with clear water immediately.
The above is only the preferred embodiment of the present invention; be noted that for those skilled in the art; under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. a resin lens clean-out system, it is characterized in that: this resin lens clean-out system based on 100 weight parts comprises the deionized water solution of the deionized water composition of DMF (DMF) solution 15 ~ 25 parts, quadrol 0.2 ~ 0.3 part, potassium primary phosphate-dipotassium hydrogen phosphate 4 ~ 6 parts, LAA 13 ~ 20 parts, ethylene glycol solution 8 ~ 12 parts and its surplus.
2. resin lens clean-out system according to claim 1, it is characterized in that: this resin lens clean-out system based on 100 weight parts is the deionized water solution of the deionized water composition of DMF (DMF) solution 25 parts, quadrol 0.25 part, potassium primary phosphate-dipotassium hydrogen phosphate 5 parts, LAA 17 parts, ethylene glycol solution 10 parts and its surplus.
3. a preparation method for resin lens clean-out system, is characterized in that, comprises the following steps:
(1) take a certain amount of deionized water, join in material-compound tank, start stirrer and stir, open heating system, heating deionized water also controls deionized water temperature;
(2) taking a certain amount of DMF (DMF) solution joins in material-compound tank, is stirred to solution transparent;
(3) taking a certain amount of potassium primary phosphate-dipotassium hydrogen phosphate joins in material-compound tank, is stirred to solution transparent;
(4) taking a certain amount of LAA joins in material-compound tank, continues Keep agitation 15-20 minute, transparent to solution;
(5) taking a certain amount of quadrol joins in material-compound tank, stirs;
(6) take a certain amount of deionized water and scrub the equipment taking up raw material, then washing lotion is poured in material-compound tank, stir evenly to solution transparent;
(7) taking a certain amount of antifreeze membrane-forming agent ethylene glycol joins in tank, stirs evenly to solution transparent, is cooled to room temperature and can obtains product of the present invention.
4. the preparation method of resin lens clean-out system according to claim 3, is characterized in that: in described step (1), stirrer stir speed (S.S.) is 35-45r/min.
5. the preparation method of resin lens clean-out system according to claim 3, is characterized in that: in described step (1), deionized water temperature controls at 55-65 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054658.5A CN104745335B (en) | 2015-02-02 | 2015-02-02 | A kind of resin lens abluent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054658.5A CN104745335B (en) | 2015-02-02 | 2015-02-02 | A kind of resin lens abluent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104745335A true CN104745335A (en) | 2015-07-01 |
| CN104745335B CN104745335B (en) | 2016-06-08 |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105013784A (en) * | 2015-07-02 | 2015-11-04 | 苏州永创达电子有限公司 | Optical glass cleaning method |
| CN106085635A (en) * | 2016-06-02 | 2016-11-09 | 瑞安市智造科技有限公司 | A kind of lens cleaning agent and preparation method thereof |
| CN106381241A (en) * | 2016-08-30 | 2017-02-08 | 东兴华鸿光学科技有限公司 | Cleaning degerming cream for glasses lenses |
| CN107987986A (en) * | 2017-12-19 | 2018-05-04 | 山东联星能源集团有限公司 | The flexible detergent and application method of a kind of high performance military helmet |
| CN109021756A (en) * | 2018-07-02 | 2018-12-18 | 中山大学 | A kind of preparation method of the superoleophobic anti-pollution layer of resin lens |
| CN109161290A (en) * | 2018-09-06 | 2019-01-08 | 中山大学 | A kind of preparation method of organic glass anti-pollution layer |
| CN109266463A (en) * | 2018-09-27 | 2019-01-25 | 镇江奥视达光学有限公司 | A kind of cleaning agent of concave lens and preparation method thereof |
| CN110257187A (en) * | 2019-07-09 | 2019-09-20 | 上海伟星光学有限公司 | A kind of polyurethane eyeglass antibacterial cleaning agent and its manufacturing method |
| CN112662489A (en) * | 2020-12-15 | 2021-04-16 | 广东红日星实业有限公司 | Resin lens cleaning agent and preparation method thereof |
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| CN1418942A (en) * | 2001-11-14 | 2003-05-21 | 金元振 | Detergent for high molecular synthetic resin spectacle lens and moulding die |
| CN1732021A (en) * | 2002-11-18 | 2006-02-08 | 眼力健有限公司 | Multi purpose contact lens care compositions including propylene glycol or glycerin |
| CN103992770A (en) * | 2013-02-18 | 2014-08-20 | 杨晓虹 | Glasses fog-resisting cleaning dual-purpose agent and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105013784A (en) * | 2015-07-02 | 2015-11-04 | 苏州永创达电子有限公司 | Optical glass cleaning method |
| CN106085635A (en) * | 2016-06-02 | 2016-11-09 | 瑞安市智造科技有限公司 | A kind of lens cleaning agent and preparation method thereof |
| CN106381241A (en) * | 2016-08-30 | 2017-02-08 | 东兴华鸿光学科技有限公司 | Cleaning degerming cream for glasses lenses |
| CN107987986A (en) * | 2017-12-19 | 2018-05-04 | 山东联星能源集团有限公司 | The flexible detergent and application method of a kind of high performance military helmet |
| CN109021756A (en) * | 2018-07-02 | 2018-12-18 | 中山大学 | A kind of preparation method of the superoleophobic anti-pollution layer of resin lens |
| CN109161290A (en) * | 2018-09-06 | 2019-01-08 | 中山大学 | A kind of preparation method of organic glass anti-pollution layer |
| CN109266463A (en) * | 2018-09-27 | 2019-01-25 | 镇江奥视达光学有限公司 | A kind of cleaning agent of concave lens and preparation method thereof |
| CN110257187A (en) * | 2019-07-09 | 2019-09-20 | 上海伟星光学有限公司 | A kind of polyurethane eyeglass antibacterial cleaning agent and its manufacturing method |
| CN112662489A (en) * | 2020-12-15 | 2021-04-16 | 广东红日星实业有限公司 | Resin lens cleaning agent and preparation method thereof |
| CN112662489B (en) * | 2020-12-15 | 2021-10-26 | 广东红日星实业有限公司 | Resin lens cleaning agent and preparation method thereof |
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| CN104745335B (en) | 2016-06-08 |
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