CN104726853A - Optical copper surface delustring blackening treatment method - Google Patents

Optical copper surface delustring blackening treatment method Download PDF

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Publication number
CN104726853A
CN104726853A CN201310703599.0A CN201310703599A CN104726853A CN 104726853 A CN104726853 A CN 104726853A CN 201310703599 A CN201310703599 A CN 201310703599A CN 104726853 A CN104726853 A CN 104726853A
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China
Prior art keywords
workpiece
clear water
treatment
oxide treatment
carries out
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Pending
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CN201310703599.0A
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Chinese (zh)
Inventor
王永朝
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Suzhou Is Closed And Is Forever Become Accurate Hardware Factory
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Suzhou Is Closed And Is Forever Become Accurate Hardware Factory
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Priority to CN201310703599.0A priority Critical patent/CN104726853A/en
Publication of CN104726853A publication Critical patent/CN104726853A/en
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Abstract

An optical copper surface delustring blackening treatment method relates to the technical field of metal surface treatment, and is characterized by including the following steps: placing a workpiece in anhydrous ethanol for soaking treatment; cleaning by an ultrasonic cleaning machine; putting into a liquid oxidizing salt for first oxidation treatment; again cleaning by the anhydrous ethanol and the ultrasonic cleaning machine; again putting into the liquid oxidizing salt for secondary oxidation treatment; putting into 100 DEG C pure water and anhydrous ethanol for soaking treatment; and finally passing through drying equipment to dry and wipe. The average pass rate of the product is more than 95%, the product color is uniformly matte, and the delustring effect is ideal.

Description

A kind of optics copper surface dulling blackening process method
Technical field:
The present invention relates to field of metal surface treatment technology, be specifically related to a kind of optics copper surface dulling blackening process method.
Background technology:
Domestic in optical device shading at present, the electrochemical reaction blackening adopted when carrying out delustring process to copper surface, but product surface color disunity, extinction effect is undesirable.
Summary of the invention:
The object of this invention is to provide a kind of optics copper surface dulling blackening process method, its product average qualification rate reaches more than 95%, and the unified shaping Asia of product colour is photochromic, and extinction effect is desirable.
In order to solve the problem existing for background technology, the present invention is by the following technical solutions: its treatment process comprises following steps:
(1) workpiece is placed in the dehydrated alcohol under normal temperature condition after foam washing process 30-40s, then rinses well with clear water;
(2) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(3), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, more fully clean up with the clear water that flows, namely complete first time oxide treatment;
(4) under normal temperature condition, the workpiece completing first time oxide treatment is put into dehydrated alcohol and processes 5-8s, when the micro-yellow of surface presentation or grey black, more fully clean up with the clear water that flows;
(5) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(6), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, until workpiece surface present black gray expandable or complete black time, more fully to clean up with the clear water that flows, namely complete second time oxide treatment;
(7) workpiece completing second time oxide treatment is put in the pure water of 100 DEG C and soaked 30-40min;
(8) by after carrying out immersion treatment 15-25s in workpiece dehydrated alcohol, then workpiece is put into drying plant and dry (temperature is no more than 200 DEG C);
(9) workpiece of oven dry is placed on non-dust cloth and wipes the floating ash in surface, namely complete production.
Described liquid oxidation salt adopts the aqueous solution containing 20-30wt% copper blackout salt.
The present invention has following beneficial effect: its product average qualification rate reaches more than 95%, and the unified shaping Asia of product colour is photochromic, and extinction effect is desirable.
Embodiment:
This embodiment is by the following technical solutions: optics copper surface dulling blackening process method comprises following steps:
(1) workpiece is placed in the dehydrated alcohol under normal temperature condition after foam washing process 30-40s, then rinses well with clear water;
(2) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(3), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, more fully clean up with the clear water that flows, namely complete first time oxide treatment;
(4) under normal temperature condition, the workpiece completing first time oxide treatment is put into dehydrated alcohol and processes 5-8s, when the micro-yellow of surface presentation or grey black, more fully clean up with the clear water that flows;
(5) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(6), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, until workpiece surface present black gray expandable or complete black time, more fully to clean up with the clear water that flows, namely complete second time oxide treatment;
(7) workpiece completing second time oxide treatment is put in the pure water of 100 DEG C and soaked 30-40min;
(8) by after carrying out immersion treatment 15-25s in workpiece dehydrated alcohol, then workpiece is put into drying plant and dry (temperature is no more than 200 DEG C);
(9) workpiece of oven dry is placed on non-dust cloth and wipes the floating ash in surface, namely complete production.
Described liquid oxidation salt adopts the aqueous solution containing 20-30wt% copper blackout salt.
This embodiment has following beneficial effect: its product average qualification rate reaches more than 95%, and the unified shaping Asia of product colour is photochromic, and extinction effect is desirable.

Claims (2)

1. an optics copper surface dulling blackening process method, is characterized in that its treatment process comprises following steps:
(1) workpiece is placed in the dehydrated alcohol under normal temperature condition after foam washing process 30-40s, then rinses well with clear water;
(2) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(3), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, more fully clean up with the clear water that flows, namely complete first time oxide treatment;
(4) under normal temperature condition, the workpiece completing first time oxide treatment is put into dehydrated alcohol and processes 5-8s, when the micro-yellow of surface presentation or grey black, more fully clean up with the clear water that flows;
(5) under normal temperature condition, workpiece is put into after Ultrasonic Cleaners carries out cleaning 5-10s, then rinse well with flowing clear water;
(6), reach the condition of 110-120 DEG C in temperature under, workpiece is put into after liquid oxidation salt carries out oxide treatment 30-35s, until workpiece surface present black gray expandable or complete black time, more fully to clean up with the clear water that flows, namely complete second time oxide treatment;
(7) workpiece completing second time oxide treatment is put in the pure water of 100 DEG C and is soaked 30-40min:
(8) by after carrying out immersion treatment 15-25s in workpiece dehydrated alcohol, then workpiece is put into drying plant dry, bake out temperature is no more than 200 DEG C;
(9) workpiece of oven dry is placed on non-dust cloth and wipes the floating ash in surface, namely complete production.
2. a kind of optics copper surface dulling blackening process method according to claim 1, is characterized in that described liquid oxidation salt adopts the aqueous solution containing 20-30wt% copper blackout salt.
CN201310703599.0A 2013-12-20 2013-12-20 Optical copper surface delustring blackening treatment method Pending CN104726853A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310703599.0A CN104726853A (en) 2013-12-20 2013-12-20 Optical copper surface delustring blackening treatment method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310703599.0A CN104726853A (en) 2013-12-20 2013-12-20 Optical copper surface delustring blackening treatment method

Publications (1)

Publication Number Publication Date
CN104726853A true CN104726853A (en) 2015-06-24

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105039952A (en) * 2015-06-29 2015-11-11 北京鼎臣超导科技有限公司 Passivating blackening liquid for nickel-plated surface of neodymium-iron-boron magnet and application of passivating blackening liquid
CN108754552A (en) * 2018-05-04 2018-11-06 瑞声科技(新加坡)有限公司 Roll copper darkening ring piece preparation method and calendering copper darkening ring piece
CN112111734A (en) * 2020-06-28 2020-12-22 宁波博曼特工业有限公司 Copper product blackening process
CN112363359A (en) * 2020-11-10 2021-02-12 昆山丘钛微电子科技有限公司 Light shielding sheet and extinction processing method thereof
WO2021134293A1 (en) * 2019-12-30 2021-07-08 诚瑞光学(常州)股份有限公司 Light shield component and blackening method therefor

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002322568A (en) * 2001-04-25 2002-11-08 Fumiko Inoue Method for coloring copper product
CN101994111A (en) * 2010-10-29 2011-03-30 王宏 Extinction blackening method of surface of optical stainless steel
CN102154638A (en) * 2011-03-21 2011-08-17 厦门大学 Brass part blackening solution and preparation method and application thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002322568A (en) * 2001-04-25 2002-11-08 Fumiko Inoue Method for coloring copper product
CN101994111A (en) * 2010-10-29 2011-03-30 王宏 Extinction blackening method of surface of optical stainless steel
CN102154638A (en) * 2011-03-21 2011-08-17 厦门大学 Brass part blackening solution and preparation method and application thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
灰机 00毛0: ""HA铜发黑工艺"", 《百度文库》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105039952A (en) * 2015-06-29 2015-11-11 北京鼎臣超导科技有限公司 Passivating blackening liquid for nickel-plated surface of neodymium-iron-boron magnet and application of passivating blackening liquid
CN105039952B (en) * 2015-06-29 2017-08-25 北京鼎臣超导科技有限公司 A kind of passivation hair blackening liquid and its application for neodymium iron boron magnetic body nickel plating surface
CN108754552A (en) * 2018-05-04 2018-11-06 瑞声科技(新加坡)有限公司 Roll copper darkening ring piece preparation method and calendering copper darkening ring piece
WO2021134293A1 (en) * 2019-12-30 2021-07-08 诚瑞光学(常州)股份有限公司 Light shield component and blackening method therefor
CN112111734A (en) * 2020-06-28 2020-12-22 宁波博曼特工业有限公司 Copper product blackening process
CN112363359A (en) * 2020-11-10 2021-02-12 昆山丘钛微电子科技有限公司 Light shielding sheet and extinction processing method thereof

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Application publication date: 20150624