CN104721098B - A kind of skin Shu Min liquid and its preparation method and application - Google Patents
A kind of skin Shu Min liquid and its preparation method and application Download PDFInfo
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- CN104721098B CN104721098B CN201510181529.2A CN201510181529A CN104721098B CN 104721098 B CN104721098 B CN 104721098B CN 201510181529 A CN201510181529 A CN 201510181529A CN 104721098 B CN104721098 B CN 104721098B
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Abstract
The invention discloses a kind of skin Shu Min liquid and its preparation method and application, belong to cosmetic field.Skin Shu Min liquid in the present invention is for raw material with Herba Dendranthematis indici Herb, wild Caulis Hederae Sinensis stem/leaf, Radix Hamamelidis Mollis stem/leaf, Chamomile/leaf, leaf of Camellia nitidissima Chi, Herba Bryophylli Pinnati stem/leaf six kind of plant, through cleaning, pulverizings, hot water extraction, Kaolin absorption, standing, filter pressing, the step such as ultrafiltration, obtain exquisite compound extracted solution.Skin Shu Min liquid of the present invention is pure galenical, and formula is unique, multiple beneficial factor synergism in 6 kind of plant raw materials, can mediator's body immunity function preferably, improve Dermal microvessel circulation, anti-inflammatory anti-itch, promote the new old replacement of skin, thus suppress and eliminate sensitization source, anaphylaxis of releiving.Production technology is simple, workable, and product is easy to use, both can use as spray, also can make emulsion and directly apply.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of skin Shu Min liquid and its preparation method and application.
Background technology
Skin runs into certain to stimulate, and the anaphylaxiss such as Pruritus, redness, twinge often occur, and the especially crowd of allergic constitution, these anaphylaxiss more often occur, though the disease that is nothing, often make us being difficult to stand, and suffer untold misery.At present, for the treatment mainly corticosteroids medicine of skin allergy, Main Function is the immunoreation suppressing human body, and it not only suppresses to cause irritated abnormal immune reaction, also can suppress normal immunoreation, reduce the resistance of Skin Cell, thus bring out nonallergic dermatitis, skin tumour, bring out melanin deposition, the untoward reaction such as skin abnormality growth, if prolonged application, also can produce drug dependence.Recent domestic studies have found that, the extract of some plants, have mitigation to skin allergy, but more or less all there are some problems, such as leaching process complexity, antiallergic effect extract antiallergic that is single or that have bring again other side effect etc. simultaneously.Therefore, find one and can replace current skin antiallergic common medicine-corticosteroids medicine, and derive from the excellent skin of natural plant extracts, the antiallergic effect sensitizing drug that relaxes and become problem urgently to be resolved hurrily.
Summary of the invention
For overcoming the shortcoming and defect of prior art, one of the object of the invention is to provide a kind of skin Shu Min liquid, and this skin Shu Min liquid forms by the compound extracted solution of following 6 kind of plant is refining: Herba Dendranthematis indici Herb (root, stem, leaf, flower), wild Caulis Hederae Sinensis stem/leaf, Radix Hamamelidis Mollis stem/leaf, Chamomile/leaf, leaf of Camellia nitidissima Chi, Herba Bryophylli Pinnati Herb.
Two of the object of the invention is the preparation method providing a kind of skin Shu Min liquid, concrete preparation process is as follows: 1) take Herba Dendranthematis indici Herb (root, stem, leaf, flower) 10-20kg, wild Caulis Hederae Sinensis stem/leaf 10-20kg, Radix Hamamelidis Mollis stem/leaf 10-18kg, Chamomile/leaf 8-20kg, leaf of Camellia nitidissima Chi 2-10kg, Herba Bryophylli Pinnati stem/leaf 6-15kg, cleans, shreds;
2) by clean, chopping after raw material put into lixiviate pot, add deionized water 500-1500kg, be under agitation warming up to 85 ± 5 DEG C, insulated and stirred lixiviate 6-12 hour, be cooled to 50 DEG C below filtrations afterwards, elimination plant residue, collection extracting solution;
3) ratio adding Kaolin 5-15kg in every 100kg extracting solution in extracting solution adds Kaolin, mix and blend 1 hour, afterwards still aging 18-24 hour;
4) filter press is utilized to remove the impurity such as natural gum, pigment of Kaolin and absorption thereof the standing solidliquid mixture terminating to be formed, gained filtrate again with ceramic super-filtering film or the ultrafiltration of rustless steel tubular ultra-filtration membrane once, obtain clear compound extracted solution, be skin Shu Min liquid of the present invention.
Three of the object of the invention is the application providing a kind of skin Shu Min liquid, can be made into liquid spray and is directly sprayed on skin allergy position, or makes emulsion and coat skin allergy position.
The present invention has following advantage and effect relative to prior art:
1. skin Shu Min liquid of the present invention is pure galenical, formula is unique, primary raw material is from being in semi-tropical Guangxi Fangcheng Port Shiwan Dashan area, the wherein Camellia nitidissima Chi glycoside of leaf of Camellia nitidissima Chi, JINHUA polysaccharide, the Herba Dendranthematis indici glycoside of Flos Chrysanthemi Indici, Herba Dendranthematis indici polypeptide, the sterol of Herba Bryophylli Pinnati, glucoside and organic acid, the tannin of Radix Hamamelidis Mollis, butterfat, the flavone of Chamomile, Herba Tagetis Patulae polysaccharide, hederin (the Hederacoside C of Caulis Hederae Sinensis, helexin) and the synergistic result of alkaloid multiple-factor, can mediator's body immunity function preferably, suppress to cause irritated abnormal immune reaction, strengthen normal immunity, improve Dermal microvessel circulation, promote the new old replacement of skin, improve skin microenvironment, anti-inflammatory anti-itch, promote skin repair, thus suppress and eliminate sensitization source, to releive anaphylaxis.
2. skin Shu Min liquid preparing process of the present invention is simple, not high to equipment requirements, can accomplish scale production simultaneously.
3. skin Shu Min liquid of the present invention is easy to use, both can use as spray, also can make emulsion and directly apply.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
Embodiment 1
Take Herba Dendranthematis indici Herb 15kg, wild Caulis Hederae Sinensis stem/leaf 15kg, Radix Hamamelidis Mollis stem/leaf 12kg, Chamomile/leaf 15kg, leaf of Camellia nitidissima Chi 6kg, Herba Bryophylli Pinnati stem/leaf 11kg, clean, shred, put into lixiviate pot, add deionized water 800kg, be under agitation heated to 80 DEG C, insulated and stirred lixiviate 8 hours, be cooled to less than 50 DEG C filtrations afterwards, removing plant residue.The ratio that filtrate adds Kaolin 5kg in every 100kg adds Kaolin, stirs 60 minutes, terminates latter still aging 18 hours, utilizes filter press to remove the impurity such as natural gum, pigment of high soil and absorption thereof.Filtrate uses Ceramic excessive filtration membrane ultrafiltration once again, removes fine particles, obtains the compound extracted solution of clear, be skin Shu Min liquid of the present invention.
Embodiment 2
Take Herba Dendranthematis indici Herb 10kg, wild Caulis Hederae Sinensis stem/leaf 11kg, Radix Hamamelidis Mollis stem/leaf 18kg, Chamomile/leaf 10kg, leaf of Camellia nitidissima Chi 3kg, Herba Bryophylli Pinnati stem/leaf 7kg, clean, shred, put into lixiviate pot, add deionized water 500kg, be under agitation heated to 85 DEG C, insulated and stirred lixiviate 10 hours, be cooled to less than 50 DEG C filtrations afterwards, removing plant residue.The ratio that filtrate adds Kaolin 10kg in every 100kg adds Kaolin, stirs 60 minutes, terminates latter still aging 20 hours, utilizes filter press to remove the impurity such as natural gum, pigment of high soil and absorption thereof.Filtrate uses Ceramic excessive filtration membrane ultrafiltration once again, removes fine particles, obtains the compound extracted solution of clear, be skin Shu Min liquid of the present invention.
Embodiment 3
Take Herba Dendranthematis indici Herb 20kg, wild Caulis Hederae Sinensis stem/leaf 18kg, Radix Hamamelidis Mollis stem/leaf 16kg, Chamomile/leaf 20kg, leaf of Camellia nitidissima Chi 9kg, Herba Bryophylli Pinnati stem/leaf 15kg, clean, shred, put into lixiviate pot, add deionized water 1300kg, be under agitation heated to 90 DEG C, insulated and stirred lixiviate 12 hours, be cooled to less than 50 DEG C filtrations afterwards, removing plant residue.The ratio that filtrate adds Kaolin 15kg in every 100kg adds Kaolin, stirs 60 minutes, terminates latter still aging 24 hours, utilizes filter press to remove the impurity such as natural gum, pigment of high soil and absorption thereof.Filtrate uses the ultrafiltration of rustless steel tubular ultra-filtration membrane once again, removes fine particles, obtains the compound extracted solution of clear, be skin Shu Min liquid of the present invention.
Reference examples 1: commercially available corticosteroids medicine (antiallergic water)
Reference examples 2
Herba Dendranthematis indici Herb 20kg, wild Caulis Hederae Sinensis stem/leaf 20kg, Radix Hamamelidis Mollis stem/leaf 16kg, other three kind of plant amounts of components are 0, deionized water 400kg, and other condition and preparation process are with reference to embodiment 1.
Reference examples 3
Chamomile/leaf 15kg, leaf of Camellia nitidissima Chi 8kg, Herba Bryophylli Pinnati stem/leaf 12kg, other three kind of plant amounts of components are 0, deionized water 320kg, and other condition and preparation process are with reference to embodiment 1.
One, experimental technique:
This experiment is divided into matched group and experimental group, experimental group is plant extraction liquid of the present invention (see embodiment 1-3 and following table 1), matched group 1 is commercially available antiallergic water (reference examples 1), matched group 2(reference examples 2) for decreasing the extracting solution of three kinds of compositions, matched group 3(reference examples 3) for having deducted other three kinds of compositions and having have adjusted the extracting solution of other component ratios.
Collect 100 volunteer's trial edition products observed result after 7 days.
Described allergic symptom is: face redness, pruritus, decortication, drying, pain
Table 1
Two, experimental result (improving degree percentage rate, X people/100 people, following table 2)
Table 2
Visible according to above-mentioned experimental result, the effect of skin Shu Min liquid of the present invention anti-skin allergy is obviously better than commercially available antiallergic water, and the synergism of 6 kind of plant components, the product more obtained than the combination of Activities of Some Plants component also has better effect.
Claims (4)
1. a preparation method for skin Shu Min liquid, its preparation process is as follows:
1) take Herba Dendranthematis indici Herb 10-20kg, wild Caulis Hederae Sinensis stem/leaf 10-20kg, Radix Hamamelidis Mollis stem/leaf 10-18kg, Chamomile/leaf 8-20kg, leaf of Camellia nitidissima Chi 2-10kg, Herba Bryophylli Pinnati stem/leaf 6-15kg, clean, shred;
2) by clean, chopping after raw material put into lixiviate pot, add deionized water 500-1500kg, be under agitation warming up to 85 ± 5 DEG C, insulated and stirred lixiviate 6-12 hour, be cooled to 50 DEG C below filtrations afterwards, elimination plant residue, collection extracting solution;
3) ratio adding Kaolin 5-15kg in every 100kg extracting solution in extracting solution adds Kaolin, mix and blend 1 hour, afterwards still aging 18-24 hour;
4) filter press is utilized to remove natural gum, the pigment impurity of Kaolin and absorption thereof the standing solidliquid mixture terminating to be formed, gained filtrate again with ceramic super-filtering film or the ultrafiltration of rustless steel tubular ultra-filtration membrane once, obtain clear compound extracted solution, be skin Shu Min liquid.
2. preparation method as claimed in claim 1, is characterized in that: in step 1) each plant material preferably the amount of taking be Herba Dendranthematis indici Herb 10kg, wild Caulis Hederae Sinensis stem/leaf 11kg, Radix Hamamelidis Mollis stem/leaf 18kg, Chamomile/leaf 10kg, leaf of Camellia nitidissima Chi 3kg, Herba Bryophylli Pinnati stem/leaf 7kg.
3. preparation method as claimed in claim 1, is characterized in that: the ratio adding Kaolin 10kg in every 100kg extracting solution in step 3) in extracting solution adds Kaolin.
4. the skin Shu Min liquid that as described in as arbitrary in claims 1 to 3, method obtains.
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106798686A (en) * | 2015-11-26 | 2017-06-06 | 上海优莱美生物科技有限公司 | A kind of creams of moisturizing Shu Min of not silicate-containing oil and preparation method thereof |
| PL421457A1 (en) * | 2017-04-28 | 2018-11-05 | Isn Pharma Spółka Z Ograniczoną Odpowiedzialnością | Skin care composition |
| CN107213057A (en) * | 2017-06-06 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | A kind of preparation method of Camellia nitidissima whitening emulsion |
| CN107174560B (en) * | 2017-06-26 | 2020-04-17 | 上海新高姿化妆品有限公司 | Mild moisturizing and relieving cleansing water and preparation method thereof |
| CN110051571A (en) * | 2018-09-18 | 2019-07-26 | 广州青岚生物科技有限公司 | A kind of pharmaceutical composition of sun-proof reparation |
| CN112137930B (en) * | 2020-10-21 | 2021-06-01 | 广州颜芝堡化妆品有限公司 | Skin allergy-relieving solid spray and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1847266A (en) * | 2005-04-15 | 2006-10-18 | 三达工业技术（厦门）有限公司 | Girasole synanthrin producing process based on two-stage ultrafiltering technology |
| CN101496772A (en) * | 2008-01-31 | 2009-08-05 | 姜宁 | Anti-aging allergy-releasing composition containing plant effective ingredient |
| CN103027867A (en) * | 2011-09-30 | 2013-04-10 | 天津市中科健新材料技术有限公司 | Finishing liquor applied on wet tissue and available for after-sun makeup removal and repair |
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2015
- 2015-04-17 CN CN201510181529.2A patent/CN104721098B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1847266A (en) * | 2005-04-15 | 2006-10-18 | 三达工业技术（厦门）有限公司 | Girasole synanthrin producing process based on two-stage ultrafiltering technology |
| CN101496772A (en) * | 2008-01-31 | 2009-08-05 | 姜宁 | Anti-aging allergy-releasing composition containing plant effective ingredient |
| CN103027867A (en) * | 2011-09-30 | 2013-04-10 | 天津市中科健新材料技术有限公司 | Finishing liquor applied on wet tissue and available for after-sun makeup removal and repair |
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Inventor after: Xu Guofeng Inventor before: Zhang Aiping |
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Effective date of registration: 20160505 Address after: 510627 Guangdong city of Guangzhou province Tianhe District Whampoa Road West, No. 601 and Suzhou court 3 Building Patentee after: Xu Guofeng Address before: 510730 No. 39, Ying Jie Avenue, Guangzhou Free Trade Zone, Guangdong Patentee before: Guangzhou Cooway Biotechnology Co.,Ltd. |
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Effective date of registration: 20170608 Address after: 510000, Guangdong, Guangzhou province Tianhe District Whampoa Avenue West 76, decimating 3904 Patentee after: Guangdong Yan Bao Biotechnology Co., Ltd. Address before: 510627 Guangdong city of Guangzhou province Tianhe District Whampoa Road West, No. 601 and Suzhou court 3 Building Patentee before: Xu Guofeng |