CN104707494A - Preparation device and preparation method for over-saturated hydrogen solution - Google Patents
Preparation device and preparation method for over-saturated hydrogen solution Download PDFInfo
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- CN104707494A CN104707494A CN201510145006.2A CN201510145006A CN104707494A CN 104707494 A CN104707494 A CN 104707494A CN 201510145006 A CN201510145006 A CN 201510145006A CN 104707494 A CN104707494 A CN 104707494A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F21/00—Dissolving
- B01F21/02—Methods
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/20—Mixing gases with liquids
- B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
- B01F23/2319—Methods of introducing gases into liquid media
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/20—Mixing gases with liquids
- B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
- B01F23/233—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
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- Accessories For Mixers (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
The invention discloses a preparation device and a preparation method for an over-saturated hydrogen solution. The preparation device comprises a hydrogen generator, a gas-liquid mixer and a water tank, wherein the hydrogen generator is used for generating a hydrogen source; the gas-liquid mixer is connected with the hydrogen generator; a gas-liquid mixer water absorption flowing branch path and a gas-liquid mixer water drainage flowing branch path are respectively connected between the gas-liquid mixer and the water tank; a gas-liquid mixing flowing loop is formed by the gas-liquid mixer water absorption flowing branch path and a gas-liquid mixer water drainage flowing branch path. By adoption of a method for fully mixing gas with water in a micronano-level diameter gas bubbles; gas-liquid mixed fluid cyclically runs in the gas-liquid mixing flowing loop to quickly form the over-saturated hydrogen solution within two minutes in the water tank, and the mass concentration of hydrogen of the hydrogen solution is not smaller than 2.5ppm; either the prepared hydrogen concentration or the preparation time is higher than that in the prior art, and the preparation efficiency is high.
Description
Technical field
The present invention relates in liquid insufflation gas to the technology of over-saturation state and device, particularly relate to a kind of preparation facilities of over-saturation hydrogen solution, specifically by gas with the mode of micro-nano rank diameter bubble by and the abundant mixing of liquid, to reach the gas device of over-saturation dissolved state and the preparation method of over-saturation hydrogen solution in a liquid under normal temperature and pressure.
Background technology
Hydrogen solution refers to the gas-liquid mixture formed after hydrogen is dissolved in water, adds the pH value that hydrogen does not change former water.Publish Japanese Ohta Shigeo etc. from " nature " magazine in 2007 there is about hydrogen anti-oxidant, anti-inflammatory, anti-apoptotic biological medical effect to report over 7 years, the biological effect of the hydrogen aqueous solution gradually accept by people and approve.Hydrogen solution is because have high biological safety, make common people rouse oneself ground, reverse the effect of pathology damage on one's own initiative and be very convenient to use mode (as: drink/soak), already become one of project that in world wide, medical care market merits attention most.Wherein, over-saturation hydrogen solution is because the high and applied range of preparation difficulty, and biological medical effect is particularly remarkable.
Being current most widely used method by drinking hydrogen water intake hydrogen, is also the safest, the modal forms of hydrogen health-oriented products.But the solubility of hydrogen in water is very low, the even water-fast gas of a kind of indissoluble, (normal temperature is 20 DEG C at normal temperatures and pressures, normal pressure is 101.3Kpa), the saturated meltage of hydrogen of 1L water is 18.2ml or 1.6mg, usually we represent with mass concentration 1.6PPM, in view of hydrogen is difficult to water-soluble characteristic, become people by drinking the obstacle of the aqueous solution of high hydrogen content.
The preparation method drinking hydrogen water comprises the types such as brine electrolysis, hydrogen dissolved water, magnesium metal reaction water.
Brine electrolysis is the earliest for the hydrogen water of human body, and the brine electrolysis of drinking for the purpose of keeping healthy originates from Japan the earliest.The equipment preparing brine electrolysis is called electrolytic cell, can containing a small amount of hydrogen by the isolated alkaline water of pellicle after electrolysis, the deficiency of brine electrolysis is because drinking water directly carries out electrolysis by electrolytic cell, the pH value of water will change, and the metal electrode direct effect of electrolytic cell and water, the metal ion having trace is separated out, if for drinking, then metal ion can enter in human body with water, more important point is, the aqueous solution of hydrogen efficiency that brine electrolysis mode obtains is very low, does not far reach hydrogen saturation state in aqueous.
Utilize metal and water to produce the chemical reaction of hydrogen and hydroxide at normal temperatures, also can prepare hydrogen water.Many metals such as iron, aluminium, magnesium etc. can react with water and produce hydrogen, but most metal exists, and mouthfeel difference, reaction speed are slow, the shortcoming of overt toxicity.
Summary of the invention
To the present invention is directed in prior art main exist prepare aqueous solution of hydrogen concentration lower, prepare longer shortcoming consuming time, provide preparation facilities of a kind of over-saturation hydrogen solution and preparation method thereof.
In order to solve the problems of the technologies described above, the present invention is solved by following technical proposals:
A kind of preparation facilities of over-saturation hydrogen solution, comprise hydrogen generator, air and liquid mixer, water tank, air and liquid mixer is connected with hydrogen generator pipeline, air and liquid mixer water suction flow branch, air and liquid mixer drain flow branch road is provided with between air and liquid mixer and water tank, air and liquid mixer water suction flow branch is by the water inhaling air liquid mixer in water tank, and the gas and liquid mixture in air and liquid mixer enters in water tank by air and liquid mixer drain flow branch road.Hydrogen generator is pure water type or alkali lye type hydrogen generator.Air and liquid mixer water suction flow branch, air and liquid mixer drain flow branch road is connected between air and liquid mixer and water tank, air and liquid mixer water suction flow branch is used for air and liquid mixer and absorbs water from water tank, air and liquid mixer drain flow branch road is used for the gas and liquid mixture in air and liquid mixer to enter in water tank, and air and liquid mixer water suction flow branch and air and liquid mixer drain flow branch road form mixed gas-liquid flow loop.
Current Japanese hydrogen water prepares hydrogen water concentration range prepared by leading brand AREGA at 1.6 ~ 1.8mg/L, prepare 10 minutes consuming time, and be not less than 2.5mg/L, preparation time based on aqueous solution of hydrogen concentration prepared by the preparation facilities of a kind of over-saturation hydrogen solution of patent of the present invention and only need 2 minutes, no matter be hydrogen water concentration or preparation time, surmount Japanese same category of device highest level comprehensively.
As preferably, air and liquid mixer water suction flow branch is provided with displacement pump, and displacement pump is connected with air and liquid mixer, water tank respectively by pipeline, and water is flow to air and liquid mixer by self-priming by displacement pump after sucking-off in water tank.Displacement pump is membrane pump, and the metered flow of membrane pump is 3 ~ 5L/min.Displacement pump have self-suction strong, start before do not need the advantage of pump priming, the displacement pump that suction capacity is strong, is easy to realize the water in water tank to continue inspiration air and liquid mixer, substantially reduces the preparation time of over-saturation hydrogen solution, and time saving and energy saving energy-conservation again.
As preferably, air and liquid mixer drain flow branch road is provided with vane pump, Voltage release device, and air and liquid mixer, vane pump, Voltage release device, water tank are connected by pipeline successively.The gas and liquid mixture flowed out from air and liquid mixer cuts stirring pressurization formation high pressure high concentration gas-liquid flow repeatedly through vane pump, and high pressure high concentration gas-liquid flow flows through Voltage release device formation over-saturation gas-liquid fluid and flows in water tank.Vane pump is single-stage impeller Vortex pump, and Vortex pump metered flow is 5L/min, and rotating speed is 2900 turns/min.Vane pump Main Function for forming higher-pressure region, and is cut gas-liquid mixed fully by the stirring of impeller; Vane pump without self-suction, but is applicable to gas-liquid delivery, and stirs cutting promotion gas dissolution in water by impeller.Voltage release device Main Function is that the solution of the high pressure high gas-liquid mixed degree flowed out by vane pump is released into atmospheric pressure state by high pressure.
As preferably, water tank is provided with water tank water sucking mouth, water outlet of water tank, and air and liquid mixer water suction flow branch is connected with water tank by water tank water sucking mouth, and air and liquid mixer drain flow branch road is connected with water tank by water outlet of water tank.
As preferably, between hydrogen generator and air and liquid mixer, be connected with the check valve preventing from liquid from pouring in down a chimney entering hydrogen generator.Check valve can effectively prevent liquid from pouring in down a chimney and enter hydrogen generator, hydrogen generator can be stablized and provide constantly band air pressure hydrogen source gas and hydrogen only can one-way flow.
As preferably, water tank is connected with over-saturation gas-liquid fluid and gets liquid branch road, over-saturation gas-liquid fluid is got liquid branch road and is comprised that normal temperature over-saturation gas-liquid fluid gets liquid branch road, heating over-saturation gas-liquid fluid gets liquid branch road, and normal temperature over-saturation gas-liquid fluid is got liquid branch road and got liquid branch circuit parallel connection with heating over-saturation gas-liquid fluid.
As preferably, normal temperature over-saturation gas-liquid fluid is got liquid branch road and is provided with normal-temperature water and goes out water solenoid valve, normal-temperature water delivery port, and normal-temperature water goes out water solenoid valve and is connected between water tank and normal-temperature water delivery port; Heating over-saturation gas-liquid fluid is got liquid branch road and is provided with hot water effluent's magnetic valve, heater, hot water outlet, and water tank, hot water effluent's magnetic valve, heater, hot water outlet connect successively.Normal-temperature water goes out water solenoid valve and goes out water state by switch electric control normal-temperature water, and hot water effluent's magnetic valve is by switch electric control hot water effluent state.
A preparation method for over-saturation hydrogen solution, preparation process comprises:
A, startup hydrogen generator, generation flow is 200ml/min ~ 500ml/min, air pressure is 0 ~ 4KG, density of hydrogen is the hydrogen source gas of 99.99%, and the outlet air pressure that hydrogen source gas flows out hydrogen generator is 0 ~ 0.4MP;
B, interval started displacement pump after three seconds, and water is flow to air and liquid mixer by self-priming by displacement pump after the sucking-off of water tank water sucking mouth;
C, interval started vane pump after three seconds again, water injects vane pump by air and liquid mixer, the air entry of air and liquid mixer produces the negative pressure of 0 ~ 0.02KG, under the suction of air and liquid mixer air entry end negative pressure generation and the positive pressure of hydrogen generator outflow hydrogen, hydrogen is inhaled into air and liquid mixer and mixes with water, hydrogen exists with air pocket form in water, air pocket diameter is 1mm ~ 1cm, air pocket hydrogen mixes with water and flows to vane pump, repeatedly cut through vane pump again and stir pressurization formation high pressure high concentration gas-liquid mixture fluid, gas-liquid mixture fluid containing a large amount of over-saturation hydrogen flows through Voltage release device, gas-liquid mixture fluid pressure reduces rapidly, the gas-liquid mixture fluid Transient transformation of high pressure conditions is atmospheric pressure state, the hydrogen dissolved under high pressure in water is overflowed in the mode of a large amount of micro-nano bubble at ambient pressure, the gas-liquid mixture fluid forming vaporific micro-nano bubble flows into water tank from water outlet of water tank,
D, gas-liquid mixture fluid run through mixed gas-liquid flow circuit cycle, form over-saturation hydrogen solution in water tank.
As preferably, gas-liquid mixture fluid runs through mixed gas-liquid flow circuit cycle and is no more than two minutes, and in water tank, form over-saturation hydrogen solution, the hydrogen quality concentration of over-saturation hydrogen solution is not less than 2.5ppm.
As preferably, gas-liquid mixture fluid is 2 ~ 5 liters/min at the flow velocity that mixed gas-liquid flow circuit cycle is run, and before Voltage release device release of pressure, pressure is not less than 0.2MPa.
The present invention is owing to have employed above technical scheme, there is significant technique effect: adopt gas with micro-nano rank diameter bubble and the well-mixed mode of water, gas-liquid mixture fluid to be operated in two minutes by mixed gas-liquid flow circuit cycle and in water tank, forms over-saturation hydrogen solution fast and the hydrogen quality concentration of over-saturation hydrogen solution is not less than 2.5ppm, be no matter the hydrogen water concentration of preparation or preparation time is all better than prior art, and preparation efficiency is high.
Accompanying drawing explanation
Fig. 1 is the structural representation of the preparation facilities embodiment of a kind of over-saturation hydrogen of the present invention solution.
The toponym that in accompanying drawing, each number designation refers to is as follows: 1-hydrogen generator, 2-displacement pump, 3-vane pump, 4-water tank, 5-air and liquid mixer, 6-Voltage release device, 7-heater, 8-check valve, 9-normal-temperature water go out water solenoid valve, 10-hot water effluent magnetic valve, 11-water tank water sucking mouth, 12-water outlet of water tank, 13-hot water outlet, 14-normal-temperature water delivery port.
Detailed description of the invention
Below in conjunction with accompanying drawing and embodiment, the present invention is described in further detail.
Embodiment 1
A kind of preparation facilities of over-saturation hydrogen solution, as shown in Figure 1, comprise hydrogen generator 1, air and liquid mixer 5, water tank 4, air and liquid mixer 5 is connected with hydrogen generator 1 pipeline, be provided with air and liquid mixer between air and liquid mixer 5 and water tank 4 to absorb water flow branch, air and liquid mixer drain flow branch road, air and liquid mixer water suction flow branch is by the water inhaling air liquid mixer in water tank 4, and the gas and liquid mixture in air and liquid mixer 5 enters in water tank 4 by air and liquid mixer drain flow branch road.Hydrogen generator is pure water type hydrogen generator.
Air and liquid mixer water suction flow branch is provided with displacement pump 2, and displacement pump 2 is connected with air and liquid mixer 5, water tank 4 respectively by pipeline, and water is flow to air and liquid mixer 5 by self-priming by displacement pump 2 after sucking-off in water tank 4.Displacement pump is membrane pump, and the metered flow of membrane pump is 5L/min.
Air and liquid mixer 5 drain flow branch road is provided with vane pump 3, Voltage release device 6, and air and liquid mixer 5, vane pump 3, Voltage release device 6, water tank 4 are connected by pipeline successively.The gas and liquid mixture flowed out from air and liquid mixer 5 cuts stirring pressurization formation high pressure high concentration gas-liquid flow repeatedly through vane pump 3, and high pressure high concentration gas-liquid flow flows through Voltage release device 6 and formed in over-saturation gas-liquid fluid inflow water tank 4.Gas-liquid mixed flows into vane pump 3, in vane pump 3 pump chamber, gas liquid mixture moves in a circle with impeller on the one hand, dish out to periphery from impeller central under the influence of centrifugal force on the one hand, gas liquid mixture obtains pressure energy and speed energy from impeller, when gas liquid mixture flows to pump head leakage fluid dram, partial velocity can change static pressure energy into.Vane pump is single-stage impeller Vortex pump, and Vortex pump metered flow is 5L/min, and rotating speed is 2900 turns/min.
Water tank 4 is provided with water tank water sucking mouth 11, water outlet of water tank 12, and air and liquid mixer water suction flow branch is connected with water tank 4 by water tank water sucking mouth 11, and air and liquid mixer drain flow branch road is connected with water tank 4 by water outlet of water tank 12.
The check valve 8 preventing from liquid from pouring in down a chimney entering hydrogen generator 1 is connected with between hydrogen generator 1 and air and liquid mixer 5.
Water tank 4 is connected with over-saturation gas-liquid fluid and gets liquid branch road, over-saturation gas-liquid fluid is got liquid branch road and is comprised that normal temperature over-saturation gas-liquid fluid gets liquid branch road, heating over-saturation gas-liquid fluid gets liquid branch road, and normal temperature over-saturation gas-liquid fluid is got liquid branch road and got liquid branch circuit parallel connection with heating over-saturation gas-liquid fluid.
Normal temperature over-saturation gas-liquid fluid is got liquid branch road and is provided with normal-temperature water and goes out water solenoid valve 9, normal-temperature water delivery port 14, and normal-temperature water goes out water solenoid valve 9 and is connected between water tank 4 and normal-temperature water delivery port 14; Heating over-saturation gas-liquid fluid is got liquid branch road and is provided with hot water effluent's magnetic valve 10, heater 7, hot water outlet 13, and water tank 4, hot water effluent's magnetic valve 10, heater 7, hot water outlet 13 connect successively.
A preparation method for over-saturation hydrogen solution, preparation process comprises:
A, startup hydrogen generator 1, generation flow is 200ml/min ~ 500ml/min, air pressure is 0 ~ 4KG, density of hydrogen is the hydrogen source gas of 99.99%, and the outlet air pressure that hydrogen source gas flows out hydrogen generator 1 is 0 ~ 0.4MP;
B, interval start displacement pump 2 in three seconds afterwards, and water is flow to air and liquid mixer 5 by self-priming by displacement pump 2 after the sucking-off of water tank water sucking mouth 11;
C, interval starts vane pump 3 in three seconds afterwards again, water injects vane pump 3 by air and liquid mixer 5, the air entry of air and liquid mixer 5 produces the negative pressure of 0 ~ 0.02KG, the suction produced in air and liquid mixer 5 air entry end negative pressure and under hydrogen generator 1 flows out the positive pressure of hydrogen, hydrogen is inhaled into air and liquid mixer 5 and mixes with water, hydrogen exists with air pocket form in water, air pocket diameter is 1mm ~ 1cm, air pocket hydrogen mixes with water and flows to vane pump 3, repeatedly cut through vane pump 3 again and stir pressurization formation high pressure high concentration gas-liquid mixture fluid, gas-liquid mixture fluid containing a large amount of over-saturation hydrogen flows through Voltage release device 6, gas-liquid mixture fluid pressure reduces rapidly, the gas-liquid mixture fluid Transient transformation of high pressure conditions is atmospheric pressure state, the hydrogen dissolved under high pressure in water is overflowed in the mode of a large amount of micro-nano bubble at ambient pressure, the gas-liquid mixture fluid forming vaporific micro-nano bubble flows into water tank 4 from water outlet of water tank 12,
D, gas-liquid mixture fluid run through mixed gas-liquid flow circuit cycle, form over-saturation hydrogen solution in water tank 4.
Gas-liquid mixture fluid runs through mixed gas-liquid flow circuit cycle and is no more than two minutes, and in water tank 4, form over-saturation hydrogen solution, the hydrogen quality concentration of over-saturation hydrogen solution is not less than 2.5ppm.
Gas-liquid mixture fluid is 2 ~ 5 liters/min at the flow velocity that mixed gas-liquid flow circuit cycle is run, and before Voltage release device 6 release of pressure, pressure is not less than 0.2MPa.
In a word, the foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to the covering scope of patent of the present invention.
Claims (10)
1. the preparation facilities of an over-saturation hydrogen solution, it is characterized in that: comprise hydrogen generator (1), air and liquid mixer (5), water tank (4), air and liquid mixer (5) is connected with hydrogen generator (1) pipeline, be provided with air and liquid mixer between air and liquid mixer (5) and water tank (4) to absorb water flow branch, air and liquid mixer drain flow branch road, air and liquid mixer water suction flow branch is by the water inhaling air liquid mixer in water tank (4), gas and liquid mixture in air and liquid mixer (5) enters in water tank (4) by air and liquid mixer drain flow branch road.
2. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 1, it is characterized in that: air and liquid mixer water suction flow branch is provided with displacement pump (2), and displacement pump (2) is connected with air and liquid mixer (5), water tank (4) respectively by pipeline.
3. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 1, it is characterized in that: air and liquid mixer (5) drain flow branch road is provided with vane pump (3), Voltage release device (6), air and liquid mixer (5), vane pump (3), Voltage release device (6), water tank (4) are connected by pipeline successively.
4. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 1, it is characterized in that: water tank (4) is provided with water tank water sucking mouth (11), water outlet of water tank (12), air and liquid mixer water suction flow branch is connected with water tank (4) by water tank water sucking mouth (11), and air and liquid mixer drain flow branch road is connected with water tank (4) by water outlet of water tank (12).
5. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 1, is characterized in that: be connected with the check valve (8) preventing from liquid from pouring in down a chimney entering hydrogen generator (1) between hydrogen generator (1) and air and liquid mixer (5).
6. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 1 or 2 or 3, it is characterized in that: water tank (4) is connected with over-saturation gas-liquid fluid and gets liquid branch road, over-saturation gas-liquid fluid is got liquid branch road and is comprised that normal temperature over-saturation gas-liquid fluid gets liquid branch road, heating over-saturation gas-liquid fluid gets liquid branch road, and normal temperature over-saturation gas-liquid fluid is got liquid branch road and got liquid branch circuit parallel connection with heating over-saturation gas-liquid fluid.
7. the preparation facilities of a kind of over-saturation hydrogen solution according to claim 6, it is characterized in that: normal temperature over-saturation gas-liquid fluid is got liquid branch road and is provided with normal-temperature water and goes out water solenoid valve (9), normal-temperature water delivery port (14), and normal-temperature water goes out water solenoid valve (9) and is connected between water tank (4) and normal-temperature water delivery port (14); Heating over-saturation gas-liquid fluid is got liquid branch road and is provided with hot water effluent's magnetic valve (10), heater (7), hot water outlet (13), and water tank (4), hot water effluent's magnetic valve (10), heater (7), hot water outlet (13) connect successively.
8. a preparation method for over-saturation hydrogen solution, comprises the preparation facilities of the over-saturation hydrogen solution described in claim, it is characterized in that: preparation process comprises:
A, startup hydrogen generator (1), generation flow is 200ml/min ~ 500ml/min, air pressure is 0 ~ 4KG, density of hydrogen is the hydrogen source gas of 99.99%, and the outlet air pressure that hydrogen source gas flows out hydrogen generator (1) is 0 ~ 0.4MP;
B, interval start displacement pump (2) after two to six seconds, water is flow to air and liquid mixer (5) by self-priming by displacement pump (2) after water tank water sucking mouth (11) sucking-off;
C, interval starts vane pump (3) after two to six seconds again, water injects vane pump (3) by air and liquid mixer (5), the air entry of air and liquid mixer (5) produces the negative pressure of 0 ~ 0.02KG, under the suction of air and liquid mixer (5) air entry end negative pressure generation and the positive pressure of hydrogen generator (1) outflow hydrogen, hydrogen is inhaled into air and liquid mixer (5) and mixes with water, hydrogen exists with air pocket form in water, air pocket diameter is 1mm ~ 1cm, air pocket hydrogen mixes with water and flows to vane pump (3), repeatedly cut through vane pump (3) again and stir pressurization formation high pressure high concentration gas-liquid mixture fluid, gas-liquid mixture fluid containing a large amount of over-saturation hydrogen flows through Voltage release device (6), gas-liquid mixture fluid pressure reduces rapidly, the gas-liquid mixture fluid Transient transformation of high pressure conditions is atmospheric pressure state, the hydrogen dissolved in water is overflowed in the mode of a large amount of micro-nano bubble at ambient pressure, the gas-liquid mixture fluid forming vaporific micro-nano bubble flows into water tank (4) from water outlet of water tank (12),
D, gas-liquid mixture fluid run through mixed gas-liquid flow circuit cycle, form over-saturation hydrogen solution in water tank (4).
9. the preparation method of a kind of over-saturation hydrogen solution according to claim 8, it is characterized in that: gas-liquid mixture fluid runs through mixed gas-liquid flow circuit cycle and is no more than two minutes, in water tank (4), form over-saturation hydrogen solution, the hydrogen quality concentration of over-saturation hydrogen solution is not less than 2.5ppm.
10. the preparation method of a kind of over-saturation hydrogen solution according to claim 8, it is characterized in that: gas-liquid mixture fluid is 2 ~ 5 liters/min at the flow velocity that mixed gas-liquid flow circuit cycle is run, before Voltage release device (6) release of pressure, pressure is not less than 0.2MPa.
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510145006.2A CN104707494A (en) | 2015-03-30 | 2015-03-30 | Preparation device and preparation method for over-saturated hydrogen solution |
| CN201510924605.4A CN106000136A (en) | 2015-03-30 | 2015-12-11 | Preparation device of supersaturated hydrogen solution and preparation method thereof |
| CN201510924641.0A CN106000137A (en) | 2015-03-30 | 2015-12-11 | Preparation device of gas solution and method for improving solubility of gas in liquid |
| TW105109811A TWI630953B (en) | 2015-03-30 | 2016-03-29 | Device for preparing gas solution and method for improving solubility of gas in liquid |
| PCT/CN2016/077678 WO2016155608A1 (en) | 2015-03-30 | 2016-03-29 | Device for preparing gas solution and method for improving gas solubility in liquid |
| TW105126512A TW201722547A (en) | 2015-03-30 | 2016-08-19 | Device for preparing gas solution and method for improving gas solubility in liquid capable of preparing high concentration supersaturated hydrogen solution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510145006.2A CN104707494A (en) | 2015-03-30 | 2015-03-30 | Preparation device and preparation method for over-saturated hydrogen solution |
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| CN104707494A true CN104707494A (en) | 2015-06-17 |
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| CN201510145006.2A Pending CN104707494A (en) | 2015-03-30 | 2015-03-30 | Preparation device and preparation method for over-saturated hydrogen solution |
| CN201510924605.4A Withdrawn CN106000136A (en) | 2015-03-30 | 2015-12-11 | Preparation device of supersaturated hydrogen solution and preparation method thereof |
| CN201510924641.0A Withdrawn CN106000137A (en) | 2015-03-30 | 2015-12-11 | Preparation device of gas solution and method for improving solubility of gas in liquid |
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| CN201510924605.4A Withdrawn CN106000136A (en) | 2015-03-30 | 2015-12-11 | Preparation device of supersaturated hydrogen solution and preparation method thereof |
| CN201510924641.0A Withdrawn CN106000137A (en) | 2015-03-30 | 2015-12-11 | Preparation device of gas solution and method for improving solubility of gas in liquid |
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| CN106000137A (en) * | 2015-03-30 | 2016-10-12 | 上海纳诺巴伯纳米科技有限公司 | Preparation device of gas solution and method for improving solubility of gas in liquid |
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2015
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- 2015-12-11 CN CN201510924605.4A patent/CN106000136A/en not_active Withdrawn
- 2015-12-11 CN CN201510924641.0A patent/CN106000137A/en not_active Withdrawn
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2016
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Also Published As
| Publication number | Publication date |
|---|---|
| CN106000136A (en) | 2016-10-12 |
| TW201709973A (en) | 2017-03-16 |
| CN106000137A (en) | 2016-10-12 |
| TW201722547A (en) | 2017-07-01 |
| TWI630953B (en) | 2018-08-01 |
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