CN104695050A - Textile fiber material and preparation method thereof - Google Patents
Textile fiber material and preparation method thereof Download PDFInfo
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- CN104695050A CN104695050A CN201510101126.2A CN201510101126A CN104695050A CN 104695050 A CN104695050 A CN 104695050A CN 201510101126 A CN201510101126 A CN 201510101126A CN 104695050 A CN104695050 A CN 104695050A
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Abstract
The invention discloses a textile fiber material and a preparation method thereof. The textile fiber material comprises the following components in parts by weight: 80-88 parts of chitin, 20-35 parts of hydroxymethyl cellulose, 10-15 parts of poly-dimethyl siloxane divalent quaternary ammonium salt, 5-12 parts of polyving akohol, 1-3 parts of sodium tartrate, 1-2 parts of hexamethylcyclotrisiloxane and 0.5-1 part of polyvinylpyrrolidone. The invention also provides a preparation method of the textile fiber material.
Description
Technical field
The invention belongs to textile material field, particularly a kind of textile fiber material and preparation method thereof.
Background technology
Countries in the world all using development new material as developing the economy, the importance of Promote Technology.The market scale of current global tencel product more than hundred billion dollars, one of novel " strategic pillar industry " of becoming textile industry.
Textile fabric can be divided into natural fabric and chemical fibre.Wherein, chemical fibre comprises regenerated fiber, synthetic fiber and inorfil.
A kind of production method of cellulose-containing textile material is disclosed in Chinese patent CN1331767A, owing to needing to use a large amount of crosslinking agents in that patent, although crosslinking agent can make fiber have good mechanical strength, but crosslinking agent to the contaminative of environment and environmental stability poor, the mechanical property that material keeps lasting can not be made.
Summary of the invention
For above-mentioned demand, the object of this invention is to provide a kind of textile fiber material and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of textile fiber material, be made up of the component comprising following weight portion:
Chitin 80-88 part,
Carboxymethyl Cellulose 20-35 part,
Dimethyl silicone polymer two quaternary amine 10-15 part,
Polyvinyl alcohol 5-12 part,
Sodium tartrate 1-3 part,
Hexamethyl cyclotrisiloxane 1-2 part,
Polyvinylpyrrolidone 0.5-1 part.
The number-average molecular weight of described polyvinyl alcohol is 6000-8000.
Described component also comprises pigment 0-0.5 weight portion.
A preparation method for textile fiber material, the method comprises the following steps:
(1) by chitin 80-88 weight portion, Carboxymethyl Cellulose 20-35 weight portion, dimethyl silicone polymer two quaternary amine 10-15 weight portion, polyvinyl alcohol 5-12 weight portion, hexamethyl cyclotrisiloxane 1-2 weight portion, polyvinylpyrrolidone 0.5-1 weight portion and pigment 0-0.5 weight portion;
(2) add in high pressure homogenizer, add sodium tartrate 1-3 weight portion, mix, melting at 305-330 DEG C, carry out spinning with the spinning speed of 1500-2000m/min, by tractive process, obtained textile fiber material.
The pressure of high pressure homogenizer described in step 2 is 17-20Mpa.
Compared with prior art, beneficial effect of the present invention:
(1) textile fiber material of the present invention is with chitin and Carboxymethyl Cellulose for main raw material, and obtained fibrous material has good processability, and mechanical strength is high.
(2) of the present invention owing to adding dimethyl silicone polymer two quaternary amine and hexamethyl cyclotrisiloxane, there is good submissive performance, effectively can reduce the friction between fiber, reduce the generation of balling-up and electrostatic phenomenon, and certain ageing resistace can be had.
(3) textile fiber material of the present invention, its preparation method is simple, is easy to suitability for industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) by chitin 80kg, Carboxymethyl Cellulose 20kg, dimethyl silicone polymer two quaternary amine 10kg, polyvinyl alcohol 5kg, hexamethyl cyclotrisiloxane 1kg, polyvinylpyrrolidone 0.5kg;
(2) add in high pressure homogenizer, under 17Mpa pressure, add sodium tartrate 1kg, mix, melting at 305 DEG C, carry out spinning with the spinning speed of 1500m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Embodiment 2
(1) by chitin 88kg, Carboxymethyl Cellulose 20kg, dimethyl silicone polymer two quaternary amine 10kg, polyvinyl alcohol 5kg, hexamethyl cyclotrisiloxane 1kg, polyvinylpyrrolidone 0.5kg;
(2) add in high pressure homogenizer, under 17Mpa pressure, add sodium tartrate 1kg, mix, melting at 305 DEG C, carry out spinning with the spinning speed of 1500m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Embodiment 3
(1) by chitin 88kg, Carboxymethyl Cellulose 20kg, dimethyl silicone polymer two quaternary amine 10kg, polyvinyl alcohol 5kg, hexamethyl cyclotrisiloxane 2kg, polyvinylpyrrolidone 1kg;
(2) add in high pressure homogenizer, under 20Mpa pressure, add sodium tartrate 3kg, mix, melting at 330 DEG C, carry out spinning with the spinning speed of 2000m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Embodiment 4
(1) by chitin 80kg, Carboxymethyl Cellulose 35kg, dimethyl silicone polymer two quaternary amine 15kg, polyvinyl alcohol 10kg, hexamethyl cyclotrisiloxane 1.5kg, polyvinylpyrrolidone 0.8kg;
(2) add in high pressure homogenizer, under 20Mpa pressure, add sodium tartrate 3kg, mix, melting at 305-330 DEG C, carry out spinning with the spinning speed of 2000m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Embodiment 5
(1) by chitin 80kg, Carboxymethyl Cellulose 35kg, dimethyl silicone polymer two quaternary amine 12kg, polyvinyl alcohol 12kg, hexamethyl cyclotrisiloxane 1.5kg, polyvinylpyrrolidone 0.8kg and ultramarine 0.5kg;
(2) add in high pressure homogenizer, under 18Mpa pressure, add sodium tartrate 2kg, mix, melting at 320 DEG C, carry out spinning with the spinning speed of 1800m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Embodiment 6
(1) by chitin 88kg, Carboxymethyl Cellulose 35kg, dimethyl silicone polymer two quaternary amine 10kg, polyvinyl alcohol 5kg, hexamethyl cyclotrisiloxane 2kg, polyvinylpyrrolidone 1kg;
(2) add in high pressure homogenizer, under 20Mpa pressure, add sodium tartrate 1kg, mix, melting at 310 DEG C, carry out spinning with the spinning speed of 1800m/min, by tractive process, obtained textile fiber material.
The performance test results of obtained textile fiber material is as shown in table 1.
Comparative example
(1) by polypropylene 100kg, Carboxymethyl Cellulose 35kg, n-butyl isocyanate 10kg, polyvinyl alcohol 5kg, polyvinylpyrrolidone 1kg;
(2) add in high pressure homogenizer, under 20Mpa pressure, add natrium citricum 1kg, mix, melting at 310 DEG C, carry out spinning with the spinning speed of 1500m/min, by tractive process, obtained textile fiber material.
Table 1
| Test event | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Comparative example |
| Stretching experiment (N) | 371 | 410 | 415 | 402 | 389 | 421 | 201 |
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (5)
1. a textile fiber material, is characterized in that, is made up of the component comprising following weight portion:
2. textile fiber material according to claim 1, is characterized in that, the number-average molecular weight of described polyvinyl alcohol is 6000-8000.
3. textile fiber material according to claim 1, is characterized in that, described component also comprises pigment 0-0.5 weight portion.
4. a preparation method for textile fiber material, is characterized in that, the method comprises the following steps:
(1) by chitin 80-88 weight portion, Carboxymethyl Cellulose 20-35 weight portion, dimethyl silicone polymer two quaternary amine 10-15 weight portion, polyvinyl alcohol 5-12 weight portion, hexamethyl cyclotrisiloxane 1-2 weight portion, polyvinylpyrrolidone 0.5-1 weight portion and pigment 0-0.5 weight portion;
(2) add in high pressure homogenizer, add sodium tartrate 1-3 weight portion, mix, melting at 305-330 DEG C, carry out spinning with the spinning speed of 1500-2000m/min, by tractive process, obtained textile fiber material.
5. the preparation method of textile fiber material according to claim 4, is characterized in that, the pressure of high pressure homogenizer described in step 2 is 17-20Mpa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510101126.2A CN104695050B (en) | 2015-03-06 | 2015-03-06 | A kind of textile fiber material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510101126.2A CN104695050B (en) | 2015-03-06 | 2015-03-06 | A kind of textile fiber material and preparation method thereof |
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| CN104695050A true CN104695050A (en) | 2015-06-10 |
| CN104695050B CN104695050B (en) | 2016-11-23 |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1546754A (en) * | 2003-12-04 | 2004-11-17 | 东南大学 | Twisted ultra-fine nanometer fiber film material and preparing method thereof |
| CN1908258A (en) * | 2006-08-10 | 2007-02-07 | 中国科学院广州化学研究所 | Phase-change energy-storage ultra-fine composite fiber and preparation method and application thereof |
| CN1958890A (en) * | 2006-11-08 | 2007-05-09 | 中国科学院广州化学研究所 | Heat storaging, thermoregulated superfine composite fibre of possessing kernel / shell structure, and preparation method |
| CN101864615A (en) * | 2009-04-15 | 2010-10-20 | 中国纺织科学研究院 | Blend fiber of chitin or derivative thereof and polyvinyl alcohol and manufacture method thereof |
| CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
| CN102959150A (en) * | 2010-07-02 | 2013-03-06 | 宝洁公司 | Filaments comprising an ingestible active agent nonwoven webs and methods for making same |
| CN103044627A (en) * | 2012-12-27 | 2013-04-17 | 苏州大学 | Pilling resistant agent emulsion for wool fabrics and preparation method thereof |
| CN104389047A (en) * | 2014-11-18 | 2015-03-04 | 太仓市宏亿化纤有限公司 | Antibacterial and mildew-proof textile fabric and preparation method thereof |
-
2015
- 2015-03-06 CN CN201510101126.2A patent/CN104695050B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1546754A (en) * | 2003-12-04 | 2004-11-17 | 东南大学 | Twisted ultra-fine nanometer fiber film material and preparing method thereof |
| CN1908258A (en) * | 2006-08-10 | 2007-02-07 | 中国科学院广州化学研究所 | Phase-change energy-storage ultra-fine composite fiber and preparation method and application thereof |
| CN1958890A (en) * | 2006-11-08 | 2007-05-09 | 中国科学院广州化学研究所 | Heat storaging, thermoregulated superfine composite fibre of possessing kernel / shell structure, and preparation method |
| CN101864615A (en) * | 2009-04-15 | 2010-10-20 | 中国纺织科学研究院 | Blend fiber of chitin or derivative thereof and polyvinyl alcohol and manufacture method thereof |
| CN102959150A (en) * | 2010-07-02 | 2013-03-06 | 宝洁公司 | Filaments comprising an ingestible active agent nonwoven webs and methods for making same |
| CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
| CN103044627A (en) * | 2012-12-27 | 2013-04-17 | 苏州大学 | Pilling resistant agent emulsion for wool fabrics and preparation method thereof |
| CN104389047A (en) * | 2014-11-18 | 2015-03-04 | 太仓市宏亿化纤有限公司 | Antibacterial and mildew-proof textile fabric and preparation method thereof |
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| CN104695050B (en) | 2016-11-23 |
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Effective date of registration: 20210827 Address after: 151600 Qinggang light industrial park, Suihua City, Heilongjiang Province Patentee after: HEILONGJIANG PULUOPU TEXTILE Co.,Ltd. Address before: 215200 Hengfan Bridge Road, Songling Town, Wujiang District, Suzhou City, Jiangsu Province Patentee before: SUZHOU AILIFANG CLOTHING Co.,Ltd. |
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