CN104646674B - The method and its product of a kind of diamond and metal base produced with combination wearing piece - Google Patents
The method and its product of a kind of diamond and metal base produced with combination wearing piece Download PDFInfo
- Publication number
- CN104646674B CN104646674B CN201410825079.1A CN201410825079A CN104646674B CN 104646674 B CN104646674 B CN 104646674B CN 201410825079 A CN201410825079 A CN 201410825079A CN 104646674 B CN104646674 B CN 104646674B
- Authority
- CN
- China
- Prior art keywords
- diamond
- metal base
- deep hole
- metal
- hole
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Drilling Tools (AREA)
- Earth Drilling (AREA)
Abstract
The method and its product of a kind of diamond and metal base produced with combination wearing piece, deep hole is processed on metal body, diamond particles are put into the deep hole of hard alloy again, and add metal bond materials, the metal base equipped with diamond compound is placed under HTHP again so that the diamond particles in metal base deep hole merge to form polycrystalline diamond body with the inwall of metal base deep hole.Diamond is dissolved into the deep hole of wearing piece idiosome by the present invention by way of glomerocryst, it is totally different from the embedded or welding manner described in foregoing patent, diamond can be very well with wearing piece idiosome be bonded together, be not in the foregoing phenomenon that wearing piece bulk material generation stress can be caused excessive again, the performance of wearing piece can be greatly improved, it is good with polycrystalline diamond effect, the characteristics of polycrystalline diamond and matrix material are tightly combined.
Description
Technical field
The present invention relates to a kind of improvement of wearing piece preparation method, particularly a kind of diamond and the compound system of metal base
Make the method system and its product of wearing piece, can be applied to make the drill bit of various Drillings, or other wearing piece performance improvements.
Background technology：
Now with the more and more higher of mechanization degree, many work are all to take machining mode to substitute traditional hand
Work cooked mode, as drill, plough and mountain on forestry harvesting operation etc. now all using do mechanization operation, or even family
Cleaning work also all starts to use do mechanization operation, and thus the requirement for wearing piece is also more and more, more and more higher；It is at present
The performance for improving wearing piece is made all in the key position of wearing piece using hard metal article in many cases, such as drill bit
Cutting parts, the tip of colter etc., but found in actual job, it is just inadequate using hard alloy or rub proofness,
In this way again it has been proposed that cover polycrystalline diamond on hard alloy, i.e., hard alloy key position in a manner of glomerocryst
Surface covers an at least diamond, further to improve the anti-wear performance of wearing piece；It can be that while compound on hard alloy
Diamond, can obtain comparison high hardness, but when encountering the larger rock or soil layer of hardness, be compounded with the hard of diamond
Matter alloy wear-resisting part wears still quickly, and it is low to show as short life, efficiency, and such sintered carbide ball teeth drill bit has just had a strong impact on broken
Crushed rocks or the effect for digging soil layer.It is exactly to take the hard hard that is pressed into of interference fit to close polycrystalline diamond to also have in addition a kind of
It is golden so easily bulk material to be split in vivo, or very big internal stress is produced, split, why can go out in use
Existing such case, because the hardness of polycrystalline diamond is higher than hard alloy, main body is closed diamond is pressed into described hard
In hole, it is possible to by the cemented carbide body squeeze crack, even if without squeeze crack, the hard alloy spherical-teeth main body is also formed with
Larger internal stress, and shock resistance is influenceed, in addition, diamond solderability is poor, realized essentially by connection is difficult to solder to.Cause
This is necessary to be improved this.
By patent retrieval and do not find there be the patent literature constructed with the present invention, related to the present invention is main
Have following：
1st, Patent No. CN201410290940.9, the invention of entitled " shock resistance diamond hard alloy complex sheet "
Patent, it which disclose a kind of diamond hard alloy complex sheet of new structure.Closed including polycrystalline diamond layer and hard
Auri body, is assembled together using diamond dust and hard alloy substrate, and diamond dust sinters under high pressure and high temperature condition
Form polycrystalline diamond layer and form diamond hard alloy complex sheet with hard alloy substrate；Wherein, the carbide matrix
There is cylindrical boss on the assembly interface of body, boss top end face there are the hemispherical projections filled in dot matrix；The upper edge of the cylindrical boss
It is waveform hierarchic structure with lower edge；Lower edge is than on along big.
2nd, Patent No. CN201410057543.7, it is entitled " to improve the diamond-coated hard alloy of point of a knife intensity
The patent of invention of cutting element ", the diamond-coated hard alloy cutting element for improving point of a knife intensity is which disclose, is carried
Peel resistance between high diamond film and tool base, point of a knife intensity is improved, and improve and resistance to collapse knife and wear resistance.Should
Diamond-coated hard alloy cutting element, have from the tool base of tungsten carbide base carbide alloy and the boundary of diamond film
The part that the metal bound phase of 8 μm of depth is most deep to inside towards tool base is gone by being chemically treated the part being removed
Except metal bound phase region, by near point of a knife（From the maximum region for being no more than 100 μm in point of a knife front end）Rear knife face it is straight
Angular cross section is observed, between the tungsten carbide in metal bound phase region is removed except part and between tungsten carbide and other carbide
With reference to the tungsten carbide crystal boundary beyond crystal boundary, the metal bound phase of 10~300nm thickness is with more than the 50% of tungsten carbide crystal boundary length
Ratio is present, and the chromium for the metal bound phase being present in tungsten carbide crystal boundary is more than 0.21 0.40 relative to the mass ratio of cobalt
Below.
3rd, patent publication No. CN1021288008, entitled " the compound detritus button down-the-hole of polycrystal diamond hard alloy
The patent of invention of drill bit and its manufacturing process ", it which disclose a kind of compound detritus button of polycrystal diamond hard alloy and dive
Drill and its manufacturing process, including hard alloy spherical-teeth main body (1), in described hard alloy spherical-teeth main body (1) at least
Provided with a polycrystalline diamond.Described polycrystalline diamond is polycrystalline diamond short cylindrical (2), is located at described hard alloy
In hole ravine in button main body (1), the length and diameter dimension of described polycrystalline diamond short cylindrical (2) are 1 ~ 50mmX φ
1~φ30mm.The down-the-hold drill bit steel body of required size is obtained by machining mode, then by polycrystal diamond hard alloy
The hard alloy spherical-teeth main body of hard alloy composite ball tooth is fixed in the hole of down-the-hold drill bit steel body, and solid composite teeth is carried out to down-the-hold drill bit steel body
Post-process quality inspection packaging outbound.
Although these above-mentioned patents have been related to application of the diamond in hard alloy, but carefully analyzing to see
Go out, for these patents all without foregoing application mode is changed, wherein patent publication No. is CN1021288008, entitled
The patent of invention of " polycrystal diamond hard alloy composite rock breaking button down-the-hole bit and its manufacturing process " is exactly a kind of typical
Polycrystalline diamond short cylindrical is inlayed by way of being interference fitted or welding and is fixed on described hard alloy spherical-teeth main body
Way in hole, however, such connected mode has following defect：Because the hardness of polycrystalline diamond is higher than hard alloy,
Diamond is being pressed into the hole of described hard alloy spherical-teeth main body, it is possible to squeeze the hard alloy spherical-teeth main body
Split, even if without squeeze crack, the hard alloy spherical-teeth main body is also formed with larger internal stress, and unfavorable shadow is produced to overall performance
Ring, so solved for foregoing diamond in hard alloy using some existing problems still without effective, because
This is necessary to need further to be studied.
The content of the invention
It is an object of the invention to solve current diamond to apply some existing problems in hard alloy, one is proposed
The method and product, this kind of method that the new diamond of kind is combined as wear body with other base materials can effectively solve current Buddha's warrior attendant
Stress is excessive in the described hard alloy of stone press-in, the problem of easily cracking.
Based on above-mentioned imagination, technical scheme proposed by the present invention is：A kind of diamond and metal base complex method, in gold
Deep hole is processed on category base substrate, then diamond particles are put into the deep hole of hard alloy, and adds metal bond materials, then will
Metal base equipped with diamond compound is placed under HTHP so that diamond particles and gold in metal base deep hole
The inwall of category idiosome deep hole merges to form polycrystalline diamond body.
Further, the idiosome that described metal body makes for Hardmetal materials, or the making of high-test metal steel
Idiosome.
Further, described in diamond particles is 0.5 μm ~ 5 μm diadusts, and described metal bond materials are
The cobalt powder powder of the mesh of granularity≤400 or the mixture of nickel powder powder or both；Diadust and metal bond materials are matched somebody with somebody
Than for 100：10—20（Percentage by weight）.
Further, described HTHP be temperature be 1390-1450 DEG C, pressure is 5300-5800 Mpa.
Further, the deep hole that processed on metal body refers to lead at the position that metal base is easiest to wear
Cross the hole that intermetallic composite coating produces deep hole shape.
Further, described hole be shaped as cylinder or mushroom-shaped or umbrella shape or Pear-Shaped.
Further, it is described that the metal base equipped with diamond compound is placed under HTHP so that in metal
It is that will be loaded with Buddha's warrior attendant that diamond particles in idiosome deep hole, which merge with the inwall of metal base deep hole and to form polycrystalline diamond body,
The metal base of stone micro mist and metal bond materials, is placed in the stove of HTHP, and diadust is housed in metal base
With installing a pressing plate on the hole surface of metal bond materials, pressing plate is provided with a through hole, and through hole faces metal base
Deep hole mouth, then a through hole pressure head being pressed directly into manner of a piston on pressing plate, in 1390-1450 DEG C of temperature, pressure is
Glomerocryst shaping is carried out under 5300-5800 Mpa process conditions so that diamond particles and metal in metal base deep hole
The inwall of idiosome deep hole merges to form polycrystalline diamond body.
Further, described glomerocryst specific make step is as follows：
1st, dispensing：By weight ratio：100 parts of diadust, 10 ~ 20 parts of metal bond materials；
2nd, batch mixing：Material obtained by step 1 is well mixed, forms mixed material；
3rd, purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C,
10 ~ 100Pa of pressure, 4 ~ 6 hours time, obtain prefabricated material；
4th, matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5th, assemble：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6th, glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head in deep hole
Prefabricated material upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature be 1390 ~ 1450 DEG C, pressure be 5300 ~
5800Mpa, time are 10 ~ 20 minutes；
7th, post-process：After the completion of glomerocryst, natural cooling, pressing plate is shed, by the wearing piece containing polycrystal obtained by step 6
Product is produced after carrying out polishing amendment.
A kind of wearing piece produced according to the method described above, including metal base, are provided with deep hole, deep hole on metal base
Interior glomerocryst has polycrystalline diamond body.
Further, described deep hole refers to the position that abrasion is easiest in metal base, is produced by intermetallic composite coating
The hole of deep hole shape.
Further, described deep hole be shaped as cylinder or mushroom-shaped or umbrella shape or Pear-Shaped.
Beneficial effects of the present invention：
Diamond is dissolved into the deep hole of wearing piece idiosome by the present invention by way of glomerocryst, is totally different from above specially
Embedded or welding manner described in profit, the idiosome that diamond can be very well with wearing piece are bonded together, and are not in again
It is foregoing that wearing piece bulk material can be caused to produce the excessive phenomenon of stress, the usability of wearing piece can be greatly improved
Can, there is the characteristics of polycrystalline diamond effect is good, and polycrystalline diamond is tightly combined with matrix material.
Brief description of the drawings
Fig. 1 is the specific embodiment structural representation of the present invention；
Fig. 2 is another specific embodiment structural representation of the present invention；
Fig. 3 is the top view of accompanying drawing 2；
Fig. 4 is another specific embodiment structural representation；
Fig. 5 is the top view of accompanying drawing 4.
Embodiment
Below in conjunction with embodiment and accompanying drawing, the present invention will be further described.
Embodiment one
A kind of modified with composite diamond plug bores tooth, and to be installed on drill bit, it includes setting in revolving body
The carbide drill tooth main body 1 and composite diamond plug 2 put, wherein, the centre of the carbide drill tooth main body 1
With a blind hole（Non- label）, the composite molding of composite diamond plug 2 is in the blind hole, and the composite diamond core
There is transition zone 3, the transition zone 3 is interpenetrated by smart steel stone and hard alloy between rod 2 and the carbide drill tooth main body 1
Formed.
The present invention provides the manufacture method that a kind of modified with composite diamond plug bores tooth again, and it includes following step
Suddenly：
（a）, manufacture carbide drill tooth main body 1；
（b）, centre opens up a blind hole in the carbide drill tooth main body 1；
（c）, smart steel stone particle is placed in the blind hole, the openend of the blind hole is suppressed using top hammer, in high temperature height
It is molded under the conditions of pressure.
Specific glomerocryst making step is as follows：
1st, dispensing：By weight ratio：100 parts of diadust, 10 ~ 13 parts of cobalt powder, silicon：4 ~ 5 parts, cubic boron：
0.8 ~ 1.5 part；
2nd, batch mixing：Material obtained by step 1 is well mixed, forms mixed material；
3rd, purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C,
10 ~ 100Pa of pressure, 4 ~ 6 hours time, obtain prefabricated material；
4th, matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5th, assemble：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6th, glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head in deep hole
Prefabricated material upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature be 1390 ~ 1450 DEG C, pressure be 5300 ~
5800Mpa, time are 10 ~ 20 minutes；
7th, post-process：After the completion of glomerocryst, natural cooling, pressing plate is shed, by the wearing piece containing polycrystal obtained by step 6
Product is produced after carrying out polishing amendment.
Disclosure based on above-mentioned technical proposal, the present invention provide a kind of modified with composite diamond plug and bore toilet article
There is following beneficial effect：The present invention provides a kind of modified with composite diamond plug and bores tooth, the composite diamond core
Composite molding is formed between rod 2 and the carbide drill tooth main body 1, rather than uses interference fit or solder bond, thus, will not
The carbide drill tooth main body 1 is had undesirable effect, in addition, the composite diamond plug 2 is located at the hard alloy
The middle part of tooth main body 1 is bored, so that the modified with composite diamond plug bores tooth and keeps sharp.
Embodiment two
A kind of brill tooth with composite diamond block, including using columned brill tooth main body 1 made of hard alloy and
The boss 202 upwardly extended from the brill tooth main body 201, the top surface of the boss 202 is rectangle working face 205, in the square
Rectangular channel is offered on shape working face 205（Non- label）, composite diamond block 203, and institute have been compounded to form in the rectangular channel
State between composite diamond block 203 and the brill tooth main body 201 formed with one layer of permeable formation 204, the permeable formation 4 is by diamond
Interpenetrate to be formed with hard alloy, be polycrystalline diamond body.The width of the rectangular channel is the width of the rectangle working face 205
The half of degree is to 2/3rds, so as to ensure the intensity of the brill tooth with composite diamond block and sharp.
Specific glomerocryst making step is as follows：
1st, dispensing：By weight ratio：100 parts of diadust, 12 ~ 15 parts of cobalt powder, nickel：2 ~ 3 parts, cubic boron：
0.8 ~ 1.5 part；
2nd, batch mixing：Material obtained by step 1 is well mixed；
3rd, purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C,
10 ~ 100Pa of pressure, 4 ~ 6 hours time, obtain prefabricated material；
4th, matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5th, assemble：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6th, glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head in deep hole
Prefabricated material upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature be 1400 ~ 1450 DEG C, pressure be 5600 ~
5800Mpa, time are 10 ~ 20 minutes；
7th, post-process：After the completion of glomerocryst, natural cooling, pressing plate is shed, by the wearing piece containing polycrystal obtained by step 6
Product is produced after carrying out polishing amendment.
Embodiment three
A kind of brill tooth with more composite diamond plugs, it includes carbide drill tooth main body 301 and more compound
Diamond plug 302, wherein, the carbide drill tooth main body 301 includes the matrix in cylinder setting, by described matrix
First cone boss 304 of upper end extension and the second cone boss 306 extended by the upper end of first cone boss 304,
Formed with annular step surface 305 between first cone boss 304 and second cone boss 304, in the described second cone
The top surface of shape boss 306 is provided with first blind hole（Non- label in figure）, it is multiple in being uniformly provided with the annular step surface 305
Second blind hole（Non- label in figure）, composite diamond plug has been compounded to form in first blind hole and second blind hole
302, and there is transition zone 303, the transition between the composite diamond plug 302 and the carbide drill tooth main body 301
Layer 303 interpenetrates the polycrystalline diamond formed by smart steel stone and hard alloy.In the present embodiment, first blind hole is from institute
The center for stating the top surface of the second cone boss 306 opens up, and second blind hole is equally spaced in first blind hole
Point on center line is on the circumference in the center of circle.
Specific glomerocryst making step is as follows：
1st, dispensing：By weight ratio：100 parts of diadust, 15 ~ 17 parts of cobalt powder, silicon：1.8 ~ 2.5 parts；
2nd, batch mixing：Material obtained by step 1 is well mixed；
3rd, purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C,
10 ~ 100Pa of pressure, 4 ~ 6 hours time, obtain prefabricated material；
4th, matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5th, assemble：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6th, glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head in deep hole
Prefabricated material upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature be 1400 ~ 1450 DEG C, pressure be 5600 ~
5800Mpa, time are 10 ~ 20 minutes；
7th, post-process：After the completion of glomerocryst, natural cooling, pressing plate is shed, by the wearing piece containing polycrystal obtained by step 6
Product is produced after carrying out polishing amendment.
It can be seen from above-described embodiment that the present invention relates to a kind of diamond and metal base complex method, in metal
Deep hole is processed on base substrate, then diamond particles are put into the deep hole of hard alloy, and adds metal bond materials, then will dress
The metal base for having diamond compound is placed under HTHP so that diamond particles and metal in metal base deep hole
The inwall of idiosome deep hole merges to form polycrystalline diamond body.
Further, the idiosome that described metal body makes for Hardmetal materials, or the making of high-test metal steel
Idiosome.
Further, described in diamond particles is 0.5 μm ~ 5 μm diadusts, and described metal bond materials are
The cobalt powder powder of the mesh of granularity≤400 or the mixture of nickel powder powder or both；Diadust and metal bond materials are matched somebody with somebody
Than for 100：10—20（Percentage by weight）.
Further, described HTHP be temperature be 1400-1450 DEG C, pressure is 5600-5800 Mpa.
Further, the deep hole that processed on metal body refers to lead at the position that metal base is easiest to wear
Cross the hole that intermetallic composite coating produces deep hole shape.
Further, described hole be shaped as cylinder or mushroom-shaped or umbrella shape or Pear-Shaped.
Further, it is described that the metal base equipped with diamond compound is placed under HTHP so that in metal
It is that will be loaded with Buddha's warrior attendant that diamond particles in idiosome deep hole, which merge with the inwall of metal base deep hole and to form polycrystalline diamond body,
The metal base of stone micro mist and metal bond materials, is placed in the stove of HTHP, and diadust is housed in metal base
With installing a pressing plate on the hole surface of metal bond materials, pressing plate is provided with a through hole, and through hole faces metal base
Deep hole mouth, then a through hole pressure head being pressed directly into manner of a piston on pressing plate, in 1390-1450 DEG C of temperature, pressure is
Glomerocryst shaping is carried out under 5300-5800 Mpa process conditions so that diamond particles and metal in metal base deep hole
The inwall of idiosome deep hole merges to form polycrystalline diamond body.
Further, described glomerocryst specific make step is as follows：
1st, dispensing：By weight ratio：100 parts of diadust, 10 ~ 20 parts of metal bond materials；
2nd, batch mixing：Material obtained by step 1 is well mixed, forms mixed material；
3rd, purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C,
10 ~ 100Pa of pressure, 4 ~ 6 hours time, obtain prefabricated material；
4th, matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5th, assemble：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6th, glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head in deep hole
Prefabricated material upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature be 1390 ~ 1450 DEG C, pressure be 5300 ~
5800Mpa, time are 10 ~ 20 minutes；
7th, post-process：After the completion of glomerocryst, natural cooling, pressing plate is shed, by the wearing piece containing polycrystal obtained by step 6
Product is produced after carrying out polishing amendment.
It will be apparent that above in conjunction with accompanying drawing to the present invention carried out exemplary description, it is clear that realization of the invention not by
The limitation of aforesaid way, if the various improvement of technical solution of the present invention progress are employed, or the not improved structure by the present invention
Think and technical scheme is directly used in other occasions, within the scope of the present invention.
Claims (1)
1. a kind of diamond and metal base complex method, process deep hole, then diamond particles are put on metal body
In the deep hole of hard alloy, and metal bond materials are added, then the metal base equipped with diamond compound is placed in high temperature height
Pressure so that the diamond particles in metal base deep hole merge to form polycrystalline diamond with the inwall of metal base deep hole
Body；Characterized in that, the deep hole that processed on metal body is that the position that abrasion is easiest in metal base passes through gold
Category processing and fabricating goes out the hole of deep hole shape, and described hole is shaped as cylinder or mushroom-shaped or umbrella shape or Pear-Shaped；Institute
That states is placed in the metal base equipped with diamond compound under HTHP so that the diamond in metal base deep hole
It is that will be loaded with diadust and metal bond materials that grain, which merges with the inwall of metal base deep hole and to form polycrystalline diamond body,
Metal base, be placed in the stove of HTHP, and in hole table of the metal base equipped with diadust and metal bond materials
One pressing plate is installed on face, pressing plate is provided with a through hole, and through hole faces the deep hole mouth of metal base, then by a pressure head with
The mode of piston is pressed directly into the through hole on pressing plate, and the prefabricated material upper surface in deep hole is directly born against by pressure head, in temperature
1400 ~ 1450 DEG C, pressure is progress glomerocryst shaping under 5600-5800 Mpa process conditions so that in metal base deep hole
Diamond particles merge to form polycrystalline diamond body with the inwall of metal base deep hole；Described metal body is hard alloy
The idiosome that material makes, or the idiosome that high-test metal steel make；Described is that 0.5 μm ~ 5 μm diamonds are micro- in diamond particles
Powder, described metal bond materials are the cobalt powder powder of the mesh of granularity≤400 or the mixture of nickel powder powder or both；Diamond
The proportioning percentage by weight of micro mist and metal bond materials is 100：10—20；Described glomerocryst specific make step is as follows：
1）Dispensing：By weight ratio：100 parts of diadust, 10 ~ 20 parts of metal bond materials；
2）Batch mixing：Material obtained by step 1 is well mixed, forms mixed material；
3）Purified treatment：The mixed material that step 2 is obtained, is put into vacuum drying oven and is handled, temperature：830 ~ 860 DEG C, pressure
10 ~ 100Pa, 4 ~ 6 hours time, obtain prefabricated material；
4）Matrix material pre-processes：The metal base surface that will act as matrix material deoils, removes removing oxide layer；
5）Assembling：The prefabricated material that step 3 is obtained is inserted in the deep hole of metal base, and is compacted with press；
6）Glomerocryst：The metal base that step 5 is obtained, is placed in sintering furnace, and is directly born against by pressure head prefabricated in deep hole
To expect upper surface, carry out HTHP glomerocryst sintering, glomerocryst sintering temperature is 1400 ~ 1450 DEG C, and pressure is 5600 ~ 5800Mpa, when
Between be 10 ~ 20 minutes；
7）Post processing：After the completion of glomerocryst, natural cooling, pressing plate is shed, the wearing piece containing polycrystal obtained by step 6 is carried out
Product is produced after polishing amendment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410825079.1A CN104646674B (en) | 2014-12-27 | 2014-12-27 | The method and its product of a kind of diamond and metal base produced with combination wearing piece |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410825079.1A CN104646674B (en) | 2014-12-27 | 2014-12-27 | The method and its product of a kind of diamond and metal base produced with combination wearing piece |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104646674A CN104646674A (en) | 2015-05-27 |
| CN104646674B true CN104646674B (en) | 2018-01-12 |
Family
ID=53238596
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410825079.1A Active CN104646674B (en) | 2014-12-27 | 2014-12-27 | The method and its product of a kind of diamond and metal base produced with combination wearing piece |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104646674B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105671398B (en) * | 2016-01-29 | 2017-07-11 | 柳州市安龙机械设备有限公司 | The processing method of hard alloy rock drilling tooth |
| CN109351999B (en) * | 2018-09-20 | 2020-04-10 | 航天材料及工艺研究所 | Drilling method for high-hardness fiber-reinforced ceramic matrix composite part |
| CN111872375B (en) * | 2020-07-17 | 2022-07-05 | 苏州思珀利尔工业技术有限公司 | Preparation method of cobalt powder coated diamond pellet, cobalt powder coated diamond and application thereof |
| CN111997530A (en) * | 2020-09-15 | 2020-11-27 | 广东钜鑫新材料科技股份有限公司 | Artificial diamond hard alloy composite sheet |
| CN112658340B (en) * | 2020-12-17 | 2022-08-16 | 乐清大勇新工具有限公司 | Drill bit and machining process thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101168230A (en) * | 2006-10-27 | 2008-04-30 | 河南富耐克超硬材料有限公司 | Method for manufacturing ultra-hard composite blade |
| CN102794447A (en) * | 2012-06-13 | 2012-11-28 | 河南省亚龙金刚石制品有限公司 | Anti-impact diamond layer, diamond composite sheet and preparation method for diamond composite sheet |
| CN104002092A (en) * | 2014-06-06 | 2014-08-27 | 河南省亚龙金刚石制品有限公司 | PDC rolling wheel for metal surface processing and preparation method of PDC rolling wheel |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59120388A (en) * | 1982-12-27 | 1984-07-11 | Toyota Motor Corp | Wear resistant composite sintered member |
| JPS62142704A (en) * | 1985-12-18 | 1987-06-26 | Sumitomo Electric Ind Ltd | Composite sintered material |
| US5662720A (en) * | 1996-01-26 | 1997-09-02 | General Electric Company | Composite polycrystalline diamond compact |
| CN102155167A (en) * | 2011-03-24 | 2011-08-17 | 中南大学 | Polycrystalline diamond-hard alloy composite rock-breaking button |
| CN202194661U (en) * | 2011-08-26 | 2012-04-18 | 河南四方达超硬材料股份有限公司 | Polycrystalline diamond enhanced type cutting pick |
| CN202970486U (en) * | 2012-12-12 | 2013-06-05 | 江汉石油钻头股份有限公司 | Thermal arrest polycrystalline diamond clad sheet |
-
2014
- 2014-12-27 CN CN201410825079.1A patent/CN104646674B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101168230A (en) * | 2006-10-27 | 2008-04-30 | 河南富耐克超硬材料有限公司 | Method for manufacturing ultra-hard composite blade |
| CN102794447A (en) * | 2012-06-13 | 2012-11-28 | 河南省亚龙金刚石制品有限公司 | Anti-impact diamond layer, diamond composite sheet and preparation method for diamond composite sheet |
| CN104002092A (en) * | 2014-06-06 | 2014-08-27 | 河南省亚龙金刚石制品有限公司 | PDC rolling wheel for metal surface processing and preparation method of PDC rolling wheel |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104646674A (en) | 2015-05-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104646674B (en) | The method and its product of a kind of diamond and metal base produced with combination wearing piece | |
| JP4903134B2 (en) | Cutting tool insert | |
| US8267204B2 (en) | Methods of forming polycrystalline diamond cutting elements, cutting elements, and earth-boring tools carrying cutting elements | |
| CA2588331C (en) | Thermally stable ultra-hard material compact constructions | |
| JP3648205B2 (en) | Oil drilling tricone bit insert chip, manufacturing method thereof, and oil digging tricon bit | |
| CN105328588B (en) | Anti abrasive tool, the method for forming wear resistant tools and wear-resisting drilling tool | |
| US20100104874A1 (en) | High pressure sintering with carbon additives | |
| JP6316936B2 (en) | Carbide structure and method for producing the same | |
| CN103953286B (en) | Welded high-matrix diamond core bit and manufacturing method thereof | |
| US9771497B2 (en) | Methods of forming earth-boring tools | |
| CA2806924C (en) | Polycrystalline diamond cutting element and method of using same | |
| CA2656913C (en) | Pdc cutters with enhanced working surfaces adjacent a cavity | |
| ZA201101040B (en) | Composite cutter substrate to mitigate residual stress | |
| JPS62111093A (en) | Lock-bit with abrasion-resistant insert | |
| US20190055788A1 (en) | Polycrystalline Diamond Cutting Elements Having lead or Lead Alloy Additions | |
| CN109590475A (en) | A kind of preparation method of big cutter head for cutting the big saw blade of high-hardness stone and the big cutter head | |
| CN104399992B (en) | Manufacturing method of double-cutting impregnated insert | |
| JP2896749B2 (en) | Drilling bit and manufacturing method thereof | |
| CN104499948A (en) | Double-cutting impregnated diamond segment | |
| JP2012515846A (en) | Polishing insert | |
| CN206592075U (en) | A kind of composite polycrystal-diamond of high-fire resistance energy | |
| CN109322666A (en) | A kind of sandwiched gradient distribution diadust strengthened pick | |
| CN209083284U (en) | A kind of sandwiched gradient distribution diadust strengthened pick | |
| US11680449B2 (en) | Polycrystalline diamond compact with increased leaching surface area and method of leaching a polycrystalline diamond compact | |
| CN106029608A (en) | Polycrystalline super hard construction and method of making |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |