CN104642704A - Method for preparing sustained release chewing gums - Google Patents
Method for preparing sustained release chewing gums Download PDFInfo
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- CN104642704A CN104642704A CN201410713047.2A CN201410713047A CN104642704A CN 104642704 A CN104642704 A CN 104642704A CN 201410713047 A CN201410713047 A CN 201410713047A CN 104642704 A CN104642704 A CN 104642704A
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- chewing gum
- cyclodextrin
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Abstract
The invention relates to a method for preparing sustained release chewing gums, belonging to the technical field of food production and processing. The sustained release chewing gum is prepared by the following steps: heating hydrated cyclodextrin, adding edible essence, and homogenizing by utilizing a homogenizer; performing spray drying, thereby obtaining cyclodextrin nanometer embedded flavor powder; adding a sweetening agent and pigments into a gum base, performing microwave treatment, mixing with the flavor powder, mashing and mixing, and performing microwave treatment again, thereby obtaining the sustained release chewing gum. According to sustained release of the chewing gum disclosed by the invention, a long-term fresh and pleasant feeling is provided for consumers, and a novel path is provided for producing the sustained release chewing gums.
Description
Technical field
The present invention relates to a kind of preparation method of chewing gum, be specifically related to a kind of preparation method of lasting release flavouring agent chewing gum newly, belong to food production processing technique field.
Background technology
Chewing gum (chewing gum) is one of the most ancient in the world candy.Archaeologist finds, before having historical records, the elder generation of the mankind just like to chew natural resin (resin), and therefrom seek pleasure, this is the most original " chewing gum ".For thousands of years, the people from different geographical culture have the custom of chewing " glue ".As Greeks can clear up tooth, guarantee oral cavity fresh and cool with resin, Indians like the juice chewing trunk, and the Maya in Central America likes to chew tunny gum (chicle).The U.S. and chewing gum have very dark love knot, not only because chewing gum is one of important export trade product of the U.S., and a pride in it or American invention history.The chewing gum that we eat today, just can trace back to 1848.The Supreme Being Ke scholar (John Curtis) of the U.S. had manufactured first for the chewing gum sold and process through processing at that time.1869, Adams (Thomas Adams) produced first chewing gum commodity made with tunny gum.Next year (1870), he releases a kind of with the chewing gum of licorice seasoning " Black Jack ", and chewing gum is changed into strip from bulk sells, popular, also can commercially find so far.Chewing gum was invention in 1906, but first kind chewing gum is but too glutinous, and result can not be sold, until nineteen twenty-eight, the technology making chewing gum improves to some extent finally, successfully squeezes into the market.First batch of chewing gum is peach, " Dubble Bubble " by name.Sugar-free part chewing gum is then appear on the market in the fifties.Make material mainly sugar, syrup, flavouring, softening agent and the matrix of chewing gum today.Be with in Mexico one, just have the habit of chewing wild pear tree juice from ancient times; 1860, peddle after this myron solidifies by the Adams of the U.S., called after " Ji Kulu " (meaning of chewing); Then, he is again by after the elimination of off flavor of Ji Kulu, renames as " Adams natural gum " and mass selling; 1880, the league (unit of length) thunder of the U.S. added sugar, peppermint etc. in natural gum, produced fragrant, pleasantly sweet chewing gum.
Chewing gum be with natural tunny gum or synthetic rubber for matrix, add the candy that a kind of confession that syrup, essence and sweetener etc. are in harmonious proportion compacting is chewed instead of eaten, mainly discharge sweet taste and fragrance for people's fresh breath and leisure.Conventional chewing gum fragrance Flavor release soon, not lastingly, slightly through chewing just very fast release from matrix totally, can not meet the demand that consumer experiences lastingly to fragrance local flavor.Therefore, a kind of chewing gum that can discharge lastingly of manufacture is just necessary.
Chinese invention: 90103527.0 disclose a kind of Flavor release system, and this system can provide flavor intensity and the persistence of improvement.When joining in chewing gum, chewing gum can be made to have required flexibility, being therefore conducive to reducing the consumption of softening agent, this softening agent is normally added with moisture.Delivery systme of the present invention is the compound of flavouring agent and resin, and preferably the two forms solution mixture each other, and the amount of flavouring agent is about 20% to 80% of final delivery systme weight, and namely remainder is resin.Delivery systme of the present invention also can containing many sweeteners to 25% (weight), such as A Xi Suhl method potassium.This invention adopts flavouring agent and resin compounded, time that its local flavor keeps or limited.
Summary of the invention
The object of this invention is to provide a kind of preparation method of lasting release chewing gum, the method carries out nanoscale embedding with cyclodextrin to flavor substance, the chewing gum that preparation can discharge lastingly, the chewing gum production method that a kind of Flavor release is more lasting is proposed, to meet the demand that consumer enjoys lastingly to local flavor.
To achieve these goals, the technical solution adopted in the present invention is:
A production method for sustainable Flavor release chewing gum, adds edible essence after being heated by aquation cyclodextrin, utilizes homogenizer to carry out homogeneous process, and then spraying dry obtains cyclodextrin nano embedding flavor powder; In matrix, add sweetener and pigment and carry out microwave treatment, puddle mixing after mixing flavor powder and again microwave treatment make the chewing gum that can discharge lastingly.
Select the cyclodextrin with hydrophobic internal cavities as flavor essence embedding wall material, add flavoring essence under high-pressure homogeneous condition, induce cyclodextrin to the embedding of hydrophobic flavouring agent, concrete grammar is:
In the cyclodextrin solution of 45-60 DEG C of heat treatment 30-50min, add the edible essence of 5-12%, at 8000 turns of homogeneous mixing 5min, spray-driedly obtain flavor powder; Flavor powder mixes with the chewing gum base 1:30-1:45 puddle of microwave treatment, and is 915MHz or 2450MHz by frequency, and power is the microwave of 800-1200W, and process 20-1min, mould molding makes the chewing gum that can discharge lastingly.
A kind of manufacturing process steps that can discharge chewing gum is lastingly as follows:
(1) cyclodextrin and water quality are uniformly mixed 12h than for 1:1-1:5;
(2) heat 30-50min by the cyclodextrin solution 45-60 of step (1) DEG C, and add the edible essence of 5-12%, 8000 turns of homogeneous mixing 5min immediately.
(3) uniform homogeneous blend that step (2) obtains is carried out spraying dry, inlet temperature is 150-180 DEG C, and outlet temperature is 70-90 DEG C, and feed rate is 30-45ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min.
(4) 30g matrix frequency is 915MHz or 2450MHz, and power is the microwave of 800-1200W, and process 1-3min, then adds 1%-3% water and again process 30s-2min.
(5) step (3) and step (4) gained material are mixed with mass ratio 1:30-1:45 puddle, and be 915MHz or 2450MHz by frequency, power is the microwave of 800-1200W, and process 20s-1min, mould molding makes the chewing gum that can discharge lastingly.
Cyclodextrin described in step (1), for alpha-cyclodextrin, beta-schardinger dextrin-and gamma-cyclodextrin one or more;
Edible spices described in step (2) can be the one in solid, liquid and flavor enhancement;
Utilize high-pressure homogeneous cyclodextrin wall material to embed flavor essence, described homogeneous also can be the one in high pressure microjet homogeneous, colloid mill homogeneous and shear and homogenize;
Edible spices described in step (2) is natural tunny gum or synthetic rubber;
Microwave treatment step in step (4) and (5), then microwave is carried out to matrix, add 1%-3% water microwave treatment again, after mixed for flavor powder puddle obtained for step (3), again carry out microwave treatment.
The invention has the beneficial effects as follows:
This method adopts nanometer embedding local flavor fragrance, increases the capacity value of local flavor, extends the Flavor release time, to the lasting freshness of consumer, meet the demand that consumer enjoys lastingly to local flavor.
Detailed description of the invention
Be described in further details the present invention below by example, these examples are only used for the present invention is described, do not limit the scope of the invention;
embodiment 1
1. alpha-cyclodextrin 100g is dissolved in 500r/min in 120ml water and is uniformly mixed 12h;
2. the alpha-cyclodextrin solution 60 DEG C of step 1 is heated 30min, and add the edible essence of 5%, 8000 turns of homogeneous mixing 5min immediately;
3. uniform homogeneous blend step 2 obtained carries out spraying dry, and inlet temperature is 180 DEG C, and outlet temperature is 80 DEG C, and feed rate is 30ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
4. 30g matrix frequency is 915MHz, and power is the microwave treatment 2min of 800W, then adds 1ml water and again processes 1min;
5. flavor powder step 3 obtained and the matrix after step 4 being processed with the mixing of mass ratio 1:30 puddle, and are 915MHz by frequency, and power is the microwave treatment 1min of 800, and mould molding makes the chewing gum that can discharge lastingly.
embodiment 2
1. beta-schardinger dextrin-90g is dissolved in 500r/min in 100ml water and is uniformly mixed 12h;
2. the beta-schardinger dextrin-solution 50 DEG C of step 1 is heated 50min, and add the edible essence of 6%, 8000 turns of homogeneous mixing 5min immediately;
3. uniform homogeneous blend step 2 obtained carries out spraying dry, and inlet temperature is 150 DEG C, and outlet temperature is 70 DEG C, and feed rate is 40ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
4. 30g matrix frequency is 2450MHz, and power is the microwave treatment 3min of 100W, then adds 1.5ml water and again processes 1.5min;
5. flavor powder step 3 obtained and the matrix after step 4 being processed with the mixing of mass ratio 1:30 puddle, and are 2450MHz by frequency, and power is the microwave treatment 0.8min of 1000, and mould molding makes the chewing gum that can discharge lastingly.
embodiment 3
1. gamma-cyclodextrin 90g is dissolved in 500r/min in 100ml water and is uniformly mixed 12h;
2. the gamma-cyclodextrin solution 45 DEG C of step 1 is heated 50min, and add the edible essence of 12%, 8000 turns of homogeneous mixing 5min immediately;
3. uniform homogeneous blend step 2 obtained carries out spraying dry, and inlet temperature is 160 DEG C, and outlet temperature is 90 DEG C, and feed rate is 45ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
4. 30g matrix frequency is 2450MHz, and power is the microwave treatment 2min of 100W, then adds 1.5ml water and again processes 1.5min;
5. flavor powder step 3 obtained and the matrix after step 4 being processed with the mixing of mass ratio 1:30 puddle, and are 2450MHz by frequency, and power is the microwave treatment 0.5min of 1200, and mould molding makes the chewing gum that can discharge lastingly.
embodiment 4
1. cyclodextrin 90g is dissolved in 500r/min in 100ml water and is uniformly mixed 12h;
2. the cyclodextrin solution 50 DEG C of step 1 is heated 35min, and add the edible essence of 10%, 8000 turns of homogeneous mixing 5min immediately;
3. uniform homogeneous blend step 2 obtained carries out spraying dry, and inlet temperature is 170 DEG C, and outlet temperature is 75 DEG C, and feed rate is 35ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
4. 30g matrix frequency is 2450MHz, and power is the microwave treatment 0.5min of 1000W, then adds 1.5ml water and again processes 1.5min;
5. flavor powder step 3 obtained and the matrix after step 4 being processed with the mixing of mass ratio 1:45 puddle, and are 2450MHz by frequency, and power is the microwave treatment 20s of 1200, and mould molding makes the chewing gum that can discharge lastingly.
embodiment 5
1. cyclodextrin 90g is dissolved in 500r/min in 100ml water and is uniformly mixed 12h;
2. the cyclodextrin solution 55 DEG C of step 1 is heated 35min, and add the edible essence of 8%, 8000 turns of homogeneous mixing 5min immediately;
3. uniform homogeneous blend step 2 obtained carries out spraying dry, and inlet temperature is 170 DEG C, and outlet temperature is 85 DEG C, and feed rate is 40ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
4. 30g matrix frequency is 2450MHz, and power is the microwave treatment 3min of 800W, then adds 1.5ml water and again processes 1.5min;
5. flavor powder step 3 obtained and the matrix after step 4 being processed with the mixing of mass ratio 1:40 puddle, and are 2450MHz by frequency, and power is the microwave treatment 1min of 800, and mould molding makes the chewing gum that can discharge lastingly.
Claims (7)
1. a preparation method for lasting release chewing gum, is characterized in that: comprise the steps:
Add edible essence after being heated by aquation cyclodextrin, utilize homogenizer to carry out homogeneous process, then spraying dry obtains cyclodextrin nano embedding flavor powder; In matrix, add sweetener and pigment and carry out microwave treatment, puddle mixing after mixing flavor powder and again microwave treatment make the chewing gum that can discharge lastingly.
2. the preparation method of a kind of lasting release chewing gum according to claim 1, is characterized in that: specifically comprise following steps:
(1) cyclodextrin and water quality are uniformly mixed 12h than for 1:1-1:5;
(2) heat 30-50min by the cyclodextrin solution 45-60 of step (1) DEG C, and add the edible essence of 5-12%, 8000 turns of homogeneous mixing 5min immediately;
(3) uniform homogeneous blend that step (2) obtains is carried out spraying dry, inlet temperature is 150-180 DEG C, and outlet temperature is 70-90 DEG C, and feed rate is 30-45ml/min, and air mass flow is 100kg/h, and atomizer velocity is 240r/min;
(4) 30g matrix frequency is 915MHz or 2450MHz, and power is the microwave of 800-1200W, and process 1-3min, then adds 1%-3% water and again process 30s-2min;
(5) mix with mass ratio 1:30-1:45 puddle by step (3) with by step (4) gained material, and be 915MHz or 2450MHz by frequency, power is the microwave of 800-1200W, and process 20s-1min, mould molding makes the chewing gum that can discharge lastingly.
3. the preparation method of a kind of lasting release chewing gum according to claim 2, is characterized in that: the cyclodextrin described in step (1) be alpha-cyclodextrin, beta-schardinger dextrin-and gamma-cyclodextrin one or more.
4. the preparation method of a kind of lasting release chewing gum according to claim 2, is characterized in that: the edible spices described in step (2) can for the one in solid, liquid and flavor enhancement.
5. the preparation method of a kind of lasting release chewing gum according to claim 2, is characterized in that: utilize high-pressure homogeneous cyclodextrin wall material to embed flavor essence, described homogeneous is the one in high pressure microjet homogeneous, colloid mill homogeneous and shear and homogenize.
6. the preparation method of a kind of lasting release chewing gum according to claim 2, is characterized in that: the edible spices described in step (2) is natural tunny gum or synthetic rubber.
7. the preparation method of a kind of lasting release chewing gum according to claim 2, it is characterized in that: the microwave treatment step in step (4) and (5), again microwave is carried out to matrix, add 1%-3% water microwave treatment again, after mixed for flavor powder puddle obtained for step (3), again carry out microwave treatment.
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| CN201410713047.2A CN104642704A (en) | 2014-12-02 | 2014-12-02 | Method for preparing sustained release chewing gums |
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| CN201410713047.2A CN104642704A (en) | 2014-12-02 | 2014-12-02 | Method for preparing sustained release chewing gums |
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| CN104642704A true CN104642704A (en) | 2015-05-27 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221592A (en) * | 2017-07-10 | 2019-01-18 | 郑登峰 | A kind of novel vitamin C chewing gum and its processing method |
| CN110810850A (en) * | 2019-10-22 | 2020-02-21 | 陕西科技大学 | Chewing artificial feeding special medical purpose electrolyte formula food and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070316A (en) * | 1991-08-02 | 1993-03-31 | 栗原良枝 | Chewing gum and manufacture method thereof |
| CN101502294A (en) * | 2008-02-04 | 2009-08-12 | 冷博 | Chewing gum containing microencapsulated natural sweetening agent |
| CN101558811A (en) * | 2008-04-16 | 2009-10-21 | 冷博 | Chewing gum containing encapsulization sweetening agent |
| CN103690610A (en) * | 2013-12-31 | 2014-04-02 | 南方医科大学 | Chewing gum capable of clearing heat from throat and preparation method of chewing gum |
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2014
- 2014-12-02 CN CN201410713047.2A patent/CN104642704A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070316A (en) * | 1991-08-02 | 1993-03-31 | 栗原良枝 | Chewing gum and manufacture method thereof |
| CN101502294A (en) * | 2008-02-04 | 2009-08-12 | 冷博 | Chewing gum containing microencapsulated natural sweetening agent |
| CN101558811A (en) * | 2008-04-16 | 2009-10-21 | 冷博 | Chewing gum containing encapsulization sweetening agent |
| CN103690610A (en) * | 2013-12-31 | 2014-04-02 | 南方医科大学 | Chewing gum capable of clearing heat from throat and preparation method of chewing gum |
Non-Patent Citations (1)
| Title |
|---|
| 高福成 等: "《食品工程高新技术》", 30 April 2009 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221592A (en) * | 2017-07-10 | 2019-01-18 | 郑登峰 | A kind of novel vitamin C chewing gum and its processing method |
| CN110810850A (en) * | 2019-10-22 | 2020-02-21 | 陕西科技大学 | Chewing artificial feeding special medical purpose electrolyte formula food and preparation method thereof |
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Application publication date: 20150527 |
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