CN104621189A - Disinfectant containing leaf mustard seed extract - Google Patents
Disinfectant containing leaf mustard seed extract Download PDFInfo
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- CN104621189A CN104621189A CN201410699974.3A CN201410699974A CN104621189A CN 104621189 A CN104621189 A CN 104621189A CN 201410699974 A CN201410699974 A CN 201410699974A CN 104621189 A CN104621189 A CN 104621189A
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- juncea seeds
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- leaf mustard
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Abstract
The invention discloses a disinfectant containing a leaf mustard seed extract. The disinfectant is prepared from the following raw materials in parts by weight: 5-10 parts of leaf mustard seed extract, 5-15 parts of tea tree oil, 10-48 parts of absolute ethyl alcohol, 3-12 parts of polyethylenepyrrolieone ketone, 10-25 parts of triton and 50-200 parts of water. The leaf mustard seed extract is prepared by the following steps: soaking black leaf mustard seeds and yellow leaf mustard seeds in ethanol water at a certain ratio; carrying out ultrasonic treatment on the soaked leaf mustard seeds in a mixed liquid of ethanol water and diethyl ether; and heating and distilling to obtain the leaf mustard seed extract. The disinfectant disclosed by the invention contains a plurality of effective components contained in the leaf mustard seeds, for example, allyl rhodanate, and other micromolecular phenols and esters such as methyl ester and butyl ester, and has a broad-spectrum bactericidal effect; and the preparation method is simple and suitable for sterilization and disinfection of animals.
Description
Technical field
The present invention relates to a kind of thimerosal, specifically a kind of thimerosal containing juncea seeds extract.
Background technology
Leaf mustard is Cruciferae Brassica genus, annual or biennial herb, and (formal name used at school: Brassica juncea) is the special vegetable of Chinese Famous.Leaf mustard contains abundant vitamin A, vitamin B complex, vitamin C and vitamin D, leaf mustard contains a large amount of ascorbic acid, it is active very strong reduction material, participate in the redox process that body is important, oxygen content in brain can be increased, excite brain to the utilization of oxygen, produce refreshing effect to the mind, the effect of relieving fatigue; Secondly also have the merit of removing toxicity for detumescence, the anti-infective and prophylactic generation of energy, the toxicity of anti-bacteria toxin, promotes wound healing, can be used to supplemental treatment infectious diseases; Leaf mustard has a kind of special delicate flavour and fragrance after pickling, can promote stomach, intestinal digestion function, improve a poor appetite, and can be used to appetizing, helps digest; Leaf mustard organize more thick and stiff, containing carotin and a large amount of edible cellulose, therefore have the effect of improving eyesight and wide intestines defaecation, can be used as the dietotherapy good merchantable brand of ophthalmic patient, also can prevent treating constipation, be especially suitable for the elderly and habitual constipation person edible.Leaf mustard can with steaming, to boil or the mode such as stir-fry is cooked; Leaf mustard pickles rear delicious flavour, can improve a poor appetite, and promotes digestive functions; Adding leaf mustard when cooking soup can make dish slightly micro-peppery.
Leaf mustard essential oil is raw material with the juncea seeds of black usually, first seed is macerated in warm water, then adopts steam or hydrodistillation to extract.Although juncea seeds and powder, not containing allyl group isosulfocyanate composition, when manufacturing essential oil, after seed contacts with water, can produce this material under the effect of enzyme.As a kind of essential oil, because leaf mustard essential oil contains the allyl group isosulfocyanate composition of high concentration, therefore can produce skin and musculo-mucosal and stimulate, produce certain toxicity.Therefore, when extracting leaf mustard essential oil, the method adopting seed to contact with water usually can be avoided.
Allyl group isosulfocyanate be a kind of have stimulate the colourless to pale yellow oily liquid body of mustard gas taste, because it has peculiar taste and antibiotic property, recently about research finds that it can suppress the growth of cancer born of the same parents, also can use as soil disinfectant agriculturally substituting Celfume, or antibacterial anticorrosion for food.CN 200910228004.4 discloses a kind of mustard essential oil biofungicide, its composition weight number proportioning: mustard essential oil 2-20 part; Embedding medium 10-30 part; Carrier 5-30 part; Binding agent 5-20 part; Dispersant 5-15 part; Filler 1-20 part.Its feature: application process is simple, is affected by the external environment less; Pollution-free, nuisanceless, have no side effect; In packing container, sheet or powdered bacteriocide is added before storage; be applied to multiple storage fruit and vegetable; protective gas layer is formed in pack environment; effective suppression or kill Main postharvest pathogens; improve fruits and vegetables disease resistance; reduce encountered pathogenic in storage microbial rotten, extend the storage fruit and vegetable time.The extraction of mustard essential oil described in this technology adopts natural extraction process, but its concrete steps undeclared.
Summary of the invention
The object of the invention is for the deficiencies in the prior art, provides a kind of thimerosal containing juncea seeds extract and preparation method thereof.
The present invention contains the thimerosal of juncea seeds extract, by juncea seeds extract 5 ~ 10 parts, tea oil 5 ~ 15 parts, absolute ethyl alcohol 10 ~ 48 parts, polyvinyl pyrrolidone 3 ~ 12 parts, Qu Latong 10 ~ 25 parts, 50 ~ 200 parts, water prepares, the preparation method of described juncea seeds extract is as follows: black juncea seeds and yellow juncea seeds be soaked in be preheated to according to quality proportioning 1:1 ~ 3 and be incubated at 30 ~ 50 DEG C, in the ethanol water of mass fraction 30 ~ 60% 18 ~ 24 hours, then by juncea seeds and juncea seeds quality 3 ~ 5 times and mass fraction is the ethanol water of 70 ~ 90%, the ether of juncea seeds quality 10 ~ 20% is blended in airtight container, carry out ultrasonic process 10-30 min, after ultrasonic end, mixed liquor is added thermal distillation 30 ~ 60min, removing solid content, to obtain final product.
Described ultrasonic process adopts frequency to be 30-60 kHz, and voltage is 50 ~ 80V.
Preferably, described thimerosal is prepared by following raw material: juncea seeds extract 6 parts, tea oil 12 parts, absolute ethyl alcohol 32 parts, polyvinyl pyrrolidone 8 parts, Qu Latong 20 parts, 130 parts, water.
Preferably, the preparation method of described juncea seeds extract is as follows: black juncea seeds and yellow juncea seeds be soaked according to quality proportioning 1:1 ~ 3 and be preheated in ethanol water that be incubated at 40 DEG C, mass fraction 50% 20 hours, then in soak, juncea seeds quality 3 ~ 5 times is added and mass fraction is the ethanol water of 80%, the ether of juncea seeds quality 15%, in airtight container, carry out ultrasonic process 20 min; After ultrasonic end, mixed liquor is added thermal distillation 45min, to obtain final product.
Preferred further, described black juncea seeds and yellow juncea seeds quality proportioning are 1:2.
The object of the invention is also the preparation method providing above-mentioned a kind of thimerosal, comprises the steps:
(1) preparation method of above-mentioned juncea seeds extract is adopted to obtain juncea seeds extract;
(2) by tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 5 ~ 10min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 40 ~ 50 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 5 ~ 10min, add remaining juncea seeds extract and Qu Latong, continue stirring 5 ~ 10min, then water is slowly added and be stirred to evenly.
The thimerosal of phase of the present invention is avoided adopting pure water directly to contact seed in the process that shepherd's purse seed extracts, and causes the precipitation of active ingredient as allyl isothiocyanate etc. too fast and the content of active ingredient is reduced; Simultaneously, in conjunction with the ultrasonic process under temperate condition, make through immersion soft after its structure of seed loose further, expose more structure, by vibration by while further for active ingredient stripping, make other micromolecular phenols, ester class, as methyl esters, butyl ester etc. are also deviate from thereupon, making is not single in the active ingredient of final extract, but containing plurality of active ingredients, the thimerosal making the present invention adopt this extract to prepare has bactericidal effect widely, and its preparation method is simple, is applicable to the sterilizing of animal.
Embodiment
Be described in further details the present invention below by embodiment, these embodiments are only used for the present invention is described, do not limit the scope of the invention.
The thimerosal that embodiment 1 the present invention contains juncea seeds extract adopts following steps preparation:
(1) black juncea seeds and yellow juncea seeds are soaked according to quality proportioning 1:2 are preheated in ethanol water that be incubated at 40 DEG C, mass fraction 50% 20 hours, then by juncea seeds and juncea seeds quality 4 times and mass fraction be the ethanol water of 80%, the ether of juncea seeds quality 15% is blended in airtight container, carrying out employing frequency is 50 kHz, and voltage is the ultrasonic echography process 20min of 50V; After ultrasonic end, mixed liquor is added thermal distillation 45min, removing solid content, obtained juncea seeds extract;
(2) thimerosal preparation: get juncea seeds extract 6 parts, tea oil 12 parts, absolute ethyl alcohol 32 parts, polyvinyl pyrrolidone 8 parts, Qu Latong 20 parts, 130 parts, water; By tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 10min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 45 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 8min, add remaining juncea seeds extract and Qu Latong, continue to stir 10min, then water is slowly added and be stirred to evenly.
The thimerosal that embodiment 2 the present invention contains juncea seeds extract adopts following steps preparation:
(1) preparation of juncea seeds extract: black juncea seeds and yellow juncea seeds are soaked according to quality proportioning 1:1 and are preheated in ethanol water that be incubated at 45 DEG C, mass fraction 55% 18 hours, then by juncea seeds and juncea seeds quality 3 times and mass fraction be the ethanol water of 75%, the ether of juncea seeds quality 10% is blended in airtight container, carrying out employing frequency is 60 kHz, and voltage is the ultrasonic echography process 10min of 80V; After ultrasonic end, mixed liquor is added thermal distillation 60min, removing solid content, to obtain final product;
(2) thimerosal preparation: get juncea seeds extract 5 parts, tea oil 5 parts, absolute ethyl alcohol 10 parts, polyvinyl pyrrolidone 10 parts, Qu Latong 10 parts, 170 parts, water; By tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 10min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 50 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 5min, add remaining juncea seeds extract and Qu Latong, continue to stir 10min, then water is slowly added and be stirred to evenly.
The thimerosal that embodiment 3 the present invention contains juncea seeds extract adopts following steps preparation:
(1) preparation of juncea seeds extract: black juncea seeds and yellow juncea seeds are soaked according to quality proportioning 1:3 and are preheated in ethanol water that be incubated at 30 DEG C, mass fraction 60% 24 hours, then by juncea seeds and juncea seeds quality 5 times and mass fraction be the ethanol water of 70%, the ether of juncea seeds quality 20% is blended in airtight container, carrying out employing frequency is 40 kHz, and voltage is ultrasonic echography process 25 min of 50V; After ultrasonic end, mixed liquor is added thermal distillation 50min, removing solid content, to obtain final product;
(2) thimerosal preparation: get juncea seeds extract 10 parts, tea oil 8 parts, absolute ethyl alcohol 48 parts, polyvinyl pyrrolidone 12 parts, Qu Latong 25 parts, 90 parts, water; By tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 5min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 40 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 10min, add remaining juncea seeds extract and Qu Latong, continue to stir 5min, then water is slowly added and be stirred to evenly.
The thimerosal that embodiment 4 the present invention contains juncea seeds extract adopts following steps preparation:
(1) preparation of juncea seeds extract: black juncea seeds and yellow juncea seeds are soaked according to quality proportioning 1:2 and are preheated in ethanol water that be incubated at 50 DEG C, mass fraction 30% 24 hours, then by juncea seeds and juncea seeds quality 5 times and mass fraction be the ethanol water of 90%, the ether of juncea seeds quality 12% is blended in airtight container, carrying out employing frequency is 30 kHz, and voltage is ultrasonic echography process 30 min of 70V; After ultrasonic end, mixed liquor is added thermal distillation 30min, removing solid content, to obtain final product;
(2) thimerosal preparation: get juncea seeds extract 10 parts, tea oil 15 parts, absolute ethyl alcohol 40 parts, polyvinyl pyrrolidone 3 parts, Qu Latong 10 parts, 100 parts, water; By tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 10min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 50 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 10min, add remaining juncea seeds extract and Qu Latong, continue to stir 10min, then water is slowly added and be stirred to evenly.
Claims (6)
1. the thimerosal containing juncea seeds extract, it is characterized in that: be by juncea seeds extract 5 ~ 10 parts, tea oil 5 ~ 15 parts, absolute ethyl alcohol 10 ~ 48 parts, polyvinyl pyrrolidone 3 ~ 12 parts, Qu Latong 10 ~ 25 parts, 50 ~ 200 parts, water prepares, the preparation method of described juncea seeds extract is as follows: black juncea seeds and yellow juncea seeds be soaked in be preheated to according to quality proportioning 1:1 ~ 3 and be incubated at 30 ~ 50 DEG C, in the ethanol water of mass fraction 30 ~ 60% 18 ~ 24 hours, then by juncea seeds and juncea seeds quality 3 ~ 5 times and mass fraction is the ethanol water of 70 ~ 90%, the ether of juncea seeds quality 10 ~ 20% is blended in airtight container, carry out ultrasonic process 10-30min, after ultrasonic end, mixed liquor is added thermal distillation 30 ~ 60min, removing solid content, to obtain final product.
2. thimerosal according to claim 1, is characterized in that: described ultrasonic process adopts frequency to be 30-60kHz, and voltage is 50 ~ 80V.
3. thimerosal according to claim 1, is characterized in that: described thimerosal is prepared by following raw material: juncea seeds extract 6 parts, tea oil 12 parts, absolute ethyl alcohol 32 parts, polyvinyl pyrrolidone 8 parts, Qu Latong 20 parts, 130 parts, water.
4. thimerosal according to claim 1, it is characterized in that: the preparation method of described juncea seeds extract is as follows: black juncea seeds and yellow juncea seeds are soaked according to quality proportioning 1:1 ~ 3 and are preheated in ethanol water that be incubated at 40 DEG C, mass fraction 50% 20 hours, then in soak, juncea seeds quality 3 ~ 5 times is added and mass fraction is the ethanol water of 80%, the ether of juncea seeds quality 15%, in airtight container, carry out ultrasonic process 20min; After ultrasonic end, mixed liquor is added thermal distillation 45min, to obtain final product.
5. thimerosal according to claim 1, is characterized in that: described black juncea seeds and yellow juncea seeds quality proportioning are 1:2.
6. a preparation method for sterilization according to claim 1, is characterized in that: adopt following steps:
(1) preparation method of juncea seeds extract described in claim 1 is adopted to obtain juncea seeds extract;
(2) by tea oil, absolute ethyl alcohol, polyvinyl pyrrolidone mix and blend 5 ~ 10min, then add by 1/2nd of the juncea seeds extract taken of filling a prescription, after being heated to 40 ~ 50 DEG C while stirring, add 1/2nd of the Qu Latong taken in formula, after stirring 5 ~ 10min, add remaining juncea seeds extract and Qu Latong, continue stirring 5 ~ 10min, then water is slowly added and be stirred to evenly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410699974.3A CN104621189A (en) | 2014-11-28 | 2014-11-28 | Disinfectant containing leaf mustard seed extract |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410699974.3A CN104621189A (en) | 2014-11-28 | 2014-11-28 | Disinfectant containing leaf mustard seed extract |
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| CN104621189A true CN104621189A (en) | 2015-05-20 |
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| CN201410699974.3A Pending CN104621189A (en) | 2014-11-28 | 2014-11-28 | Disinfectant containing leaf mustard seed extract |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112941145A (en) * | 2021-02-02 | 2021-06-11 | 郑州安图生物工程股份有限公司 | Inactivating reagent for enveloped viruses and pathogenic bacteria and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112941145A (en) * | 2021-02-02 | 2021-06-11 | 郑州安图生物工程股份有限公司 | Inactivating reagent for enveloped viruses and pathogenic bacteria and application thereof |
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