CN104607344B - A kind of graphene film implantation equipment - Google Patents

A kind of graphene film implantation equipment Download PDF

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Publication number
CN104607344B
CN104607344B CN201510036776.3A CN201510036776A CN104607344B CN 104607344 B CN104607344 B CN 104607344B CN 201510036776 A CN201510036776 A CN 201510036776A CN 104607344 B CN104607344 B CN 104607344B
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CN
China
Prior art keywords
spray assembly
graphene film
conveyer belt
implantation equipment
seal case
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Application number
CN201510036776.3A
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Chinese (zh)
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CN104607344A (en
Inventor
施利君
徐鸽
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Suzhou Kzone Equipment Technology Co Ltd
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Suzhou Kzone Equipment Technology Co Ltd
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Priority to CN201510036776.3A priority Critical patent/CN104607344B/en
Publication of CN104607344A publication Critical patent/CN104607344A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B13/00Machines or plants for applying liquids or other fluent materials to surfaces of objects or other work by spraying, not covered by groups B05B1/00 - B05B11/00
    • B05B13/02Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work
    • B05B13/04Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work the spray heads being moved during spraying operation
    • B05B13/0405Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work the spray heads being moved during spraying operation with reciprocating or oscillating spray heads
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B12/00Arrangements for controlling delivery; Arrangements for controlling the spray area
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B14/00Arrangements for collecting, re-using or eliminating excess spraying material

Landscapes

  • Nozzles (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The present invention relates to a kind of graphene film implantation equipment, it includes seal case, it is installed in rotation on the conveyer belt in described seal case, for the conveying motor driving described conveyer belt to rotate, it is arranged in described seal case and is positioned at the wobble component above described conveyer belt, be arranged on described wobble component and stagger the two row's spray assemblies arranged, it is respectively connected with being common to being added thereto to adding box and being respectively connected with, with described spray assembly, the air inlet pipeline that is common to import compressed gas wherein of adulterant with described spray assembly, the parallel setting of spray assembly described in two rows.Graphene film implantation equipment of the present invention, on the one hand arranges conveyer belt in seal case, for being fed forward by graphene film to be adulterated;On the other hand two row's spray assemblies are installed on wobble component, and spray assembly staggers settings, so can improve the uniformity coefficient of adulterant sprinkling, and then guarantee the uniform doping of graphene film.

Description

A kind of graphene film implantation equipment
Technical field
The present invention relates to a kind of film doping equipment, be specifically related to a kind of graphene film implantation equipment.
Background technology
Graphene is a kind of carbonaceous material of the bi-dimensional cellular shape lattice structure the most tightly packed by carbon atom.The preparation method of graphene film mainly has micromechanics glass method, liquid chemical method, silicon carbide epitaxy graphene film valve, chemical vapour deposition technique etc. at present, wherein obtain Graphene not only area by micromechanics stripping method little, and yield is few, not there is industrial application and be worth;And the sheet resistance of graphene thin film obtained by liquid chemical method, silicon carbide epitaxy graphene film method, chemical vapour deposition technique is relatively big, the sheet resistance of graphene thin film that liquid chemical method obtains is 5 × 103About Ω, silicon carbide epitaxy sheet resistance of graphene thin film is 1.05 × 105About Ω, the single-layer graphene film sheet resistance obtained by chemical vapour deposition technique is 1 × 103About Ω.After the graphene film superposition multilamellar that chemical vapour deposition technique obtains, can effectively reduce the sheet resistance of graphene film;But while superposition multilamellar, the light transmission of graphene film is also reducing, and therefore limits graphene film in Display Technique field and the application of other industrial circles.
In prior art, in order to overcome the defect that sheet resistance of graphene thin film is big generally to use nitric acid doping or the method for gold chloride doping, and hand spray is mainly passed through in nitric acid doping or gold chloride doping, first adulterant is put into watering can, being taken out of by compressed air and form atomization, graphene film is just doped by hand-held nozzle.Hand spray efficiency is low, difficult quality guarantee of adulterating.
Summary of the invention
The invention aims to overcome the deficiencies in the prior art to provide a kind of graphene film implantation equipment.
For reaching above-mentioned purpose, the technical solution adopted in the present invention is: a kind of graphene film implantation equipment, it includes seal case, it is installed in rotation on the conveyer belt in described seal case, for the conveying motor driving described conveyer belt to rotate, it is arranged in described seal case and is positioned at the wobble component above described conveyer belt, be arranged on described wobble component and stagger the two row's spray assemblies arranged, it is respectively connected with being common to being added thereto to adding box and being respectively connected with, with described spray assembly, the air inlet pipeline that is common to import compressed gas wherein of adulterant with described spray assembly, the parallel setting of spray assembly described in two rows, the atomized particle size of described spray assembly is 0.2 ~ 5 micron.
Optimally, being provided with blower fan bottom described conveyer belt, described blower fan connects waste gas recovery assembly.
Further, described wobble component includes swing frame, is arranged on bottom described swing frame and symmetrically arranged multiple roller and being connected with described swing frame for driving it to carry out the oscillating motor swung.
Further, it also includes being respectively connected with, with described spray assembly, the Feed lines that leads to, and described Feed lines is provided with main valve and the independence that is arranged between described spray assembly and described Feed lines controls hand-operated valve.
Optimally, described air inlet pipeline is provided with air inlet air relief valve.
Optimally, described spray assembly being removably provided with shower nozzle, described shower nozzle is made up of PVC plastic.
Owing to technique scheme is used, the present invention compared with prior art has the advantage that graphene film implantation equipment of the present invention, on the one hand arranges conveyer belt in seal case, for being fed forward by graphene film to be adulterated;On the other hand two row's spray assemblies are installed on wobble component, and spray assembly staggers settings, so can improve the uniformity coefficient of adulterant sprinkling, and then guarantee the uniform doping of graphene film.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of graphene film implantation equipment of the present invention;
Accompanying drawing 2 is the part-structure schematic diagram of accompanying drawing 1;
Wherein, 1, seal case;2, conveyer belt;3, conveying motor;4, wobble component;41, swing frame;42, roller;43, oscillating motor;5, box is added;6, main valve;7, independent control hand-operated valve;8, spray assembly;81, shower nozzle;9, Feed lines;10, air inlet pipeline;11, air inlet air relief valve;12, blower fan;13, waste gas recovery assembly.
Detailed description of the invention
Below in conjunction with accompanying drawing, the preferred embodiment of the invention is described in detail.
Graphene film implantation equipment as depicted in figs. 1 and 2, it includes seal case 1, conveyer belt 2, conveying motor 3, wobble component 4, adds box 5, spray assembly 8 and air inlet pipeline 10.
Wherein, seal case 1 is installed on the ground, and its bottom is provided with multiple spikes, owing to adulterant is the corrosive chemical such as nitric acid or gold chloride, therefore seal case 1 needs seal and use resistant material, it is to avoid the pollution to environment of the above-mentioned chemical substance.Conveyer belt 2 is installed in rotation in seal case 1, for being constantly fed forward graphene film.Conveying motor 3 is connected with conveyer belt 2, is used for driving conveyer belt 2 to rotate.Wobble component 4 is arranged in seal case 1, and is positioned at the top of conveyer belt 2, and it swings back and forth above conveyer belt 2.Spray assembly 8 has multiple, they are uniformly distributed and are formed two neat rows, in this parallel setting of two rows spray assembly 8 and this two rows spray assembly 8, corresponding needs stagger setting, so can improve the uniformity coefficient that adulterant sprays, and then guarantee the uniform doping of graphene film;Spray assembly 8 can form ultra micro mist, and the atomized particle size of ultra micro mist is 0.2 ~ 5 micron.Add box 5 to be respectively connected with leading to spray assembly 8, be used for being added thereto to adulterant;Air inlet pipeline 10 is respectively connected with leading to spray assembly 8, and for importing compressed gas wherein, such adulterant can spray after being atomized in spray assembly 8 via compressed gas.This spray assembly 8 is used in combination creates beyond thought effect with interpolation box 5, air inlet pipeline 10: the ultra micro mist of formation does not has impulsive force when spraying from spray assembly 8, therefore, it is possible to obtain the most uniform dopant deposit effect, its effect is similar to diaphragm and is positioned in mist, slowly deposition is formed by fog and film contact, deposit thickness easily controls, and stability is high;It addition, the liquid medicine consumption of ejection is only the 0.5% ~ 1% of traditional consumption from spray assembly 8, owing to the cost of liquid medicine is much more expensive, the cost of doping so can be greatly reduced.
In the present embodiment, being provided with blower fan 12 bottom conveyer belt 2, blower fan 12 connects waste gas recovery assembly 13, so can remaining chemical substance be collected in waste gas recovery assembly 13, plays protection environment, the effect of maintenance shopwork condition.Wobble component 4 includes swing frame 41, be arranged on bottom swing frame 41 and symmetrically arranged multiple roller 42 and being connected with swing frame 41 for driving it to carry out the oscillating motor 43 swung.Spray assembly 8 is connected with two Feed lines 9 the most respectively, and Feed lines 9 forms main road and branch road, and main road is provided with main valve 6;Every branch road is connected with each spray assembly 8 respectively, and it is installed above has and independent control hand-operated valve 7, utilizes main valve 6 and the independent cooperation controlling hand-operated valve 7 to be capable of adding the accurate control of adulterant in spray assembly 8;Air inlet air relief valve 11 is additionally installed on air inlet pipeline 10, so can regulate compressed-air actuated carrying capacity, such that it is able to cooperate with main valve 6, the independent hand-operated valve 7 that controls, it is achieved the accurate control to spray assembly 8 spouting liquid.Being provided with shower nozzle 81 on spray assembly 8, shower nozzle 81 is removably mounted on spray assembly 8, and it uses transparent PVC plastic to make.
Above-described embodiment only for technology design and the feature of the present invention are described, its object is to allow person skilled in the art will appreciate that present disclosure and to implement according to this, can not limit the scope of the invention with this.All equivalence changes made according to spirit of the invention or modification, all should contain within protection scope of the present invention.

Claims (5)

1. a graphene film implantation equipment, it is characterized in that: it includes seal case (1), the conveyer belt (2) being installed in rotation in described seal case (1), for the conveying motor (3) driving described conveyer belt (2) to rotate, it is arranged in described seal case (1) and is positioned at the wobble component (4) of described conveyer belt (2) top, be arranged on described wobble component (4) and stagger the two row's spray assemblies (8) arranged, it is respectively connected with being common to be added thereto to the interpolation box (5) of adulterant with described spray assembly (8) and is respectively connected with, with described spray assembly (8), the air inlet pipeline (10) that is common to import compressed gas wherein, spray assembly (8) parallel setting described in two rows, the atomized particle size of described spray assembly (8) is 0.2 ~ 5 micron;Described wobble component (4) includes swing frame (41), is arranged on described swing frame (41) bottom and symmetrically arranged multiple roller (42) and is connected for the oscillating motor (43) driving it to carry out swinging with described swing frame (41).
Graphene film implantation equipment the most according to claim 1, it is characterised in that: described conveyer belt (2) bottom is provided with blower fan (12), and described blower fan (12) connects waste gas recovery assembly (13).
Graphene film implantation equipment the most according to claim 1 and 2, it is characterized in that: it also includes being respectively connected with, with described spray assembly (8), the Feed lines (9) that leads to, described Feed lines (9) is provided with main valve (6) and the independence that is arranged between described spray assembly (8) and described Feed lines (9) controls hand-operated valve (7).
Graphene film implantation equipment the most according to claim 1, it is characterised in that: air inlet air relief valve (11) is installed on described air inlet pipeline (10).
Graphene film implantation equipment the most according to claim 1, it is characterised in that: being removably provided with shower nozzle (81) on described spray assembly (8), described shower nozzle (81) is made up of PVC plastic.
CN201510036776.3A 2015-01-26 2015-01-26 A kind of graphene film implantation equipment Active CN104607344B (en)

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CN104607344B true CN104607344B (en) 2016-09-21

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105562275A (en) * 2016-03-04 2016-05-11 东华大学 Spraying device for preparing perovskite solar cell
CN109453927B (en) * 2018-12-15 2021-06-22 饶玉明 Anticorrosive spraying mechanism of graphite alkene

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1259405A (en) * 1999-08-30 2000-07-12 上海交通大学 Transparent conductive film and reflection reduction film spray coating equipment and method
CN201655826U (en) * 2009-12-29 2010-11-24 中国电子科技集团公司第十八研究所 Buffer layer preparation device for CIGS solar battery
EP1757372B1 (en) * 2005-08-24 2012-04-11 Brother Kogyo Kabushiki Kaisha Film forming apparatus and method of film formation
CN103909692A (en) * 2013-01-05 2014-07-09 神华集团有限责任公司 Laminated transparent conductive oxide film, and making method and application thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101284265B (en) * 2007-04-13 2010-09-08 欧利速精密工业股份有限公司 Processing method and apparatus for hot melting adhesive glue powder using in nonmetal object surface

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1259405A (en) * 1999-08-30 2000-07-12 上海交通大学 Transparent conductive film and reflection reduction film spray coating equipment and method
EP1757372B1 (en) * 2005-08-24 2012-04-11 Brother Kogyo Kabushiki Kaisha Film forming apparatus and method of film formation
CN201655826U (en) * 2009-12-29 2010-11-24 中国电子科技集团公司第十八研究所 Buffer layer preparation device for CIGS solar battery
CN103909692A (en) * 2013-01-05 2014-07-09 神华集团有限责任公司 Laminated transparent conductive oxide film, and making method and application thereof

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