CN104607344A - Graphene film doping equipment - Google Patents
Graphene film doping equipment Download PDFInfo
- Publication number
- CN104607344A CN104607344A CN201510036776.3A CN201510036776A CN104607344A CN 104607344 A CN104607344 A CN 104607344A CN 201510036776 A CN201510036776 A CN 201510036776A CN 104607344 A CN104607344 A CN 104607344A
- Authority
- CN
- China
- Prior art keywords
- graphene film
- spray assembly
- conveyer belt
- implantation equipment
- mist spray
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B13/00—Machines or plants for applying liquids or other fluent materials to surfaces of objects or other work by spraying, not covered by groups B05B1/00 - B05B11/00
- B05B13/02—Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work
- B05B13/04—Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work the spray heads being moved during spraying operation
- B05B13/0405—Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work the spray heads being moved during spraying operation with reciprocating or oscillating spray heads
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B12/00—Arrangements for controlling delivery; Arrangements for controlling the spray area
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B14/00—Arrangements for collecting, re-using or eliminating excess spraying material
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- Nozzles (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention relates to graphene film doping equipment. The graphene film doping equipment comprises a sealed tank, a conveyer belt rotationally installed in the sealed tank, a conveying motor used for driving the conveyer belt to rotate, a swing assembly installed in the sealed tank and located above the conveyer belt, two rows of mist spray assemblies installed on the swing assembly in a staggered mode, addition boxes communicated with the mist spray assemblies respectively and used for adding doping agents into the mist spray assemblies, and air inlet pipelines communicated with the mist spray assemblies respectively and used for guiding compressed gas into the mist spray assemblies, wherein the two rows of mist spray assemblies are arranged in parallel. On one hand, the conveyer belt is arranged in the sealed tank and used for forwards conveying graphene films to be doped; on the other hand, the two rows of mist spray assemblies are installed on the swing assembly and are arranged in the staggered mode, so that the uniformity degree of spraying of the doping agents is improved, and then it is ensured that the graphene films are evenly doped.
Description
Technical field
The present invention relates to a kind of film doping equipment, be specifically related to a kind of graphene film implantation equipment.
Background technology
Graphene is by a kind of carbonaceous material of the directly tightly packed bi-dimensional cellular shape lattice structure of carbon atom.The preparation method of current graphene film mainly contains micromechanics glass method, liquid chemical method, silicon carbide epitaxy graphene film valve, chemical vapour deposition technique etc., not only area is little wherein to obtain Graphene by micromechanics stripping method, and output is few, does not there is industrial application and be worth; And the sheet resistance of graphene thin film obtained by liquid chemical method, silicon carbide epitaxy graphene film method, chemical vapour deposition technique is comparatively large, the sheet resistance of graphene thin film that liquid chemical method obtains is 5 × 10
3about Ω, silicon carbide epitaxy sheet resistance of graphene thin film is 1.05 × 10
5about Ω, the single-layer graphene film sheet resistance obtained by chemical vapour deposition technique is 1 × 10
3about Ω.After the graphene film superposition multilayer that chemical vapour deposition technique obtains, effectively can reduce the sheet resistance of graphene film; But the light transmission of graphene film is also in reduction while superposition multilayer, because which limit the application of graphene film at Display Technique field and other industrial circles.
In prior art, usually the method that nitric acid adulterates or gold chloride adulterates is adopted in order to overcome the large defect of sheet resistance of graphene thin film, and nitric acid doping or gold chloride doping are mainly through hand spray, first adulterant is put into watering can, taken out of by compressed air and form atomization, hand-held nozzle just adulterates to graphene film.Hand spray efficiency is low, doping difficult quality guarantee.
Summary of the invention
The present invention seeks to provide a kind of graphene film implantation equipment to overcome the deficiencies in the prior art.
For achieving the above object, the technical solution adopted in the present invention is: a kind of graphene film implantation equipment, it comprises seal case, be installed in rotation on the conveyer belt in described seal case, the conveying motor rotated for driving described conveyer belt, to be arranged in described seal case and the wobble component be positioned at above described conveyer belt, to be arranged on described wobble component and the two row's spray assemblies arranged that stagger, be connected for adding the interpolation box of adulterant wherein and being connected respectively the air inlet pipeline for importing Compressed Gas wherein with described spray assembly respectively with described spray assembly, the described spray assembly of two rows parallels setting, the atomized particle size of described spray assembly is 0.2 ~ 5 micron.
Optimally, be provided with blower fan bottom described conveyer belt, described blower fan is connected with waste gas recovery assembly.
Further, described wobble component comprising swing frame, being arranged on bottom described swing frame and symmetrically arranged multiple roller and being connected with described swing frame for driving it to carry out the oscillating motor swung.
Further, it also comprises the Feed lines be connected respectively with described spray assembly, and described Feed lines is provided with main valve and the independence be arranged between described spray assembly and described Feed lines controls hand-operated valve.
Optimally, described air inlet pipeline is provided with air inlet pressure-reducing valve.
Optimally, described spray assembly is removably provided with shower nozzle, described shower nozzle is made up of PVC plastic.
Because technique scheme is used, the present invention compared with prior art has following advantages: graphene film implantation equipment of the present invention, arranges conveyer belt, for being fed forward by graphene film to be adulterated on the one hand in seal case; On wobble component, install two row's spray assemblies on the other hand, the setting and spray assembly staggers, can improve the uniformity coefficient that adulterant sprays like this, and then guarantee the uniform doping of graphene film.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of graphene film implantation equipment of the present invention;
Accompanying drawing 2 is part-structure schematic diagrames of accompanying drawing 1;
Wherein, 1, seal case; 2, conveyer belt; 3, motor is carried; 4, wobble component; 41, swing frame; 42, roller; 43, oscillating motor; 5, box is added; 6, main valve; 7, independently hand-operated valve is controlled; 8, spray assembly; 81, shower nozzle; 9, Feed lines; 10, air inlet pipeline; 11, air inlet pressure-reducing valve; 12, blower fan; 13, waste gas recovery assembly.
Detailed description of the invention
Below in conjunction with accompanying drawing, the preferred embodiment of the invention is described in detail.
Graphene film implantation equipment as depicted in figs. 1 and 2, it comprises seal case 1, conveyer belt 2, conveying motor 3, wobble component 4, adds box 5, spray assembly 8 and air inlet pipeline 10.
Wherein, seal case 1 is installed on the ground, and its bottom is provided with multiple feet, because adulterant is the corrosive chemical such as nitric acid or gold chloride, therefore seal case 1 needs sealing and uses resistant material, avoids above-mentioned chemical substance to the pollution of environment.Conveyer belt 2 is installed in rotation in seal case 1, for being constantly fed forward graphene film.Conveying motor 3 is connected with conveyer belt 2, rotates for driving conveyer belt 2.Wobble component 4 is arranged in seal case 1, and is positioned at the top of conveyer belt 2, and it swings back and forth above conveyer belt 2.Spray assembly 8 has multiple, they are uniformly distributed and form two neat rows, this two rows spray assembly 8 parallels setting and in this two rows spray assembly 8, corresponding needs stagger settings, can improve the uniformity coefficient of adulterant sprinkling like this, and then guarantee the uniform doping of graphene film; Spray assembly 8 can form ultra micro mist, and the atomized particle size of ultra micro mist is 0.2 ~ 5 micron.Add box 5 to be connected respectively with spray assembly 8, for adding adulterant wherein; Air inlet pipeline 10 is connected respectively with spray assembly 8, for importing Compressed Gas wherein, and ejection after such adulterant can be atomized in spray assembly 8 via Compressed Gas.This spray assembly 8 and interpolation box 5, air inlet pipeline 10 conbined usage are created beyond thought effect: when the ultra micro mist of formation sprays from spray assembly 8, there is no impulsive force, therefore, it is possible to obtain extremely uniform dopant deposit effect, the similar diaphragm of its effect is positioned in mist, slow deposition is formed by fog and film contact, deposit thickness very easily controls, and stability is high; In addition, from spray assembly 8, the liquid medicine consumption of ejection is only 0.5% ~ 1% of traditional consumption, because the cost of liquid medicine is very expensive, greatly can reduce the cost of doping like this.
In the present embodiment, be provided with blower fan 12 bottom conveyer belt 2, blower fan 12 is connected with waste gas recovery assembly 13, remaining chemical substance can be collected in waste gas recovery assembly 13 like this, plays protection of the environment, maintains the effect of shopwork condition.Wobble component 4 comprises swing frame 41, to be arranged on bottom swing frame 41 and symmetrically arranged multiple roller 42 and being connected with swing frame 41 for driving it to carry out the oscillating motor 43 swung.Spray assembly 8 is also connected with two Feed lines 9 respectively, and Feed lines 9 forms main road and branch road, main road is provided with main valve 6; Every root branch road is connected with each spray assembly 8 respectively, is provided with independent control hand-operated valve 7 above it, utilizes main valve 6 can realize the accurate control to adding adulterant in spray assembly 8 with the independent cooperation controlling hand-operated valve 7; In addition air inlet pipeline 10 is provided with air inlet pressure-reducing valve 11, compressed-air actuated carrying capacity can be regulated like this, thus hand-operated valve 7 can be controlled and cooperatively interact with main valve 6, independence, realize the accurate control to spray assembly 8 spouting liquid.Spray assembly 8 is provided with shower nozzle 81, shower nozzle 81 is removably mounted on spray assembly 8, and it uses transparent PVC plastic to make.
Above-described embodiment, only for technical conceive of the present invention and feature are described, its object is to person skilled in the art can be understood content of the present invention and implement according to this, can not limit the scope of the invention with this.All equivalences done according to Spirit Essence of the present invention change or modify, and all should be encompassed within protection scope of the present invention.
Claims (6)
1. a graphene film implantation equipment, it is characterized in that: it comprises seal case (1), be installed in rotation on the conveyer belt (2) in described seal case (1), the conveying motor (3) rotated for driving described conveyer belt (2), to be arranged in described seal case (1) and to be positioned at the wobble component (4) of described conveyer belt (2) top, be arranged on described wobble component (4) to go up and two rows' spray assembly (8) arranged that stagger, be connected for adding the interpolation box (5) of adulterant wherein and being connected for the air inlet pipeline (10) importing Compressed Gas wherein respectively with described spray assembly (8) respectively with described spray assembly (8), the two described spray assembly of rows (8) parallel setting, the atomized particle size of described spray assembly (8) is 0.2 ~ 5 micron.
2. graphene film implantation equipment according to claim 1, is characterized in that: described conveyer belt (2) bottom is provided with blower fan (12), and described blower fan (12) is connected with waste gas recovery assembly (13).
3. graphene film implantation equipment according to claim 1 and 2, is characterized in that: described wobble component (4) comprises swing frame (41), be arranged on described swing frame (41) bottom and symmetrically arranged multiple roller (42) and being connected for the oscillating motor (43) driving it to carry out swinging with described swing frame (41).
4. graphene film implantation equipment according to claim 1 and 2, it is characterized in that: it also comprises the Feed lines (9) be connected respectively with described spray assembly (8), described Feed lines (9) is provided with main valve (6) and the independence be arranged between described spray assembly (8) and described Feed lines (9) controls hand-operated valve (7).
5. graphene film implantation equipment according to claim 1, is characterized in that: described air inlet pipeline (10) is provided with air inlet pressure-reducing valve (11).
6. graphene film implantation equipment according to claim 1, is characterized in that: described spray assembly (8) is removably provided with shower nozzle (81), and described shower nozzle (81) is made up of PVC plastic.
Priority Applications (1)
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CN201510036776.3A CN104607344B (en) | 2015-01-26 | 2015-01-26 | A kind of graphene film implantation equipment |
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CN201510036776.3A CN104607344B (en) | 2015-01-26 | 2015-01-26 | A kind of graphene film implantation equipment |
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CN104607344A true CN104607344A (en) | 2015-05-13 |
CN104607344B CN104607344B (en) | 2016-09-21 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105562275A (en) * | 2016-03-04 | 2016-05-11 | 东华大学 | Spraying device for preparing perovskite solar cell |
CN109453927A (en) * | 2018-12-15 | 2019-03-12 | 饶玉明 | A kind of graphene anti-corrosion spray mechanism |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1259405A (en) * | 1999-08-30 | 2000-07-12 | 上海交通大学 | Transparent conductive film and reflection reduction film spray coating equipment and method |
US20100021630A1 (en) * | 2007-04-13 | 2010-01-28 | Jakov Makover | Method and System for Applying Hot Melt Adhesive Powder onto a Non-Metallic Object Surface |
CN201655826U (en) * | 2009-12-29 | 2010-11-24 | 中国电子科技集团公司第十八研究所 | Buffer layer preparation device for CIGS solar battery |
EP1757372B1 (en) * | 2005-08-24 | 2012-04-11 | Brother Kogyo Kabushiki Kaisha | Film forming apparatus and method of film formation |
CN103909692A (en) * | 2013-01-05 | 2014-07-09 | 神华集团有限责任公司 | Laminated transparent conductive oxide film, and making method and application thereof |
-
2015
- 2015-01-26 CN CN201510036776.3A patent/CN104607344B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1259405A (en) * | 1999-08-30 | 2000-07-12 | 上海交通大学 | Transparent conductive film and reflection reduction film spray coating equipment and method |
EP1757372B1 (en) * | 2005-08-24 | 2012-04-11 | Brother Kogyo Kabushiki Kaisha | Film forming apparatus and method of film formation |
US20100021630A1 (en) * | 2007-04-13 | 2010-01-28 | Jakov Makover | Method and System for Applying Hot Melt Adhesive Powder onto a Non-Metallic Object Surface |
CN201655826U (en) * | 2009-12-29 | 2010-11-24 | 中国电子科技集团公司第十八研究所 | Buffer layer preparation device for CIGS solar battery |
CN103909692A (en) * | 2013-01-05 | 2014-07-09 | 神华集团有限责任公司 | Laminated transparent conductive oxide film, and making method and application thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105562275A (en) * | 2016-03-04 | 2016-05-11 | 东华大学 | Spraying device for preparing perovskite solar cell |
CN109453927A (en) * | 2018-12-15 | 2019-03-12 | 饶玉明 | A kind of graphene anti-corrosion spray mechanism |
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CN104607344B (en) | 2016-09-21 |
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