CN104606909B - One kind of plant Oleum sesami boiler - Google Patents
One kind of plant Oleum sesami boiler Download PDFInfo
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- CN104606909B CN104606909B CN201510032186.3A CN201510032186A CN104606909B CN 104606909 B CN104606909 B CN 104606909B CN 201510032186 A CN201510032186 A CN 201510032186A CN 104606909 B CN104606909 B CN 104606909B
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- inner bag
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 51
- 238000004821 distillation Methods 0.000 claims abstract description 27
- 238000009833 condensation Methods 0.000 claims abstract description 25
- 230000005494 condensation Effects 0.000 claims abstract description 25
- 238000007599 discharging Methods 0.000 claims abstract description 10
- 238000009413 insulation Methods 0.000 claims abstract description 8
- 239000010865 sewage Substances 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 239000002304 perfume Substances 0.000 claims description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 239000010692 aromatic oil Substances 0.000 claims description 3
- 241000196324 Embryophyta Species 0.000 description 14
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 13
- 239000007789 gas Substances 0.000 description 12
- 239000000463 material Substances 0.000 description 11
- 239000003921 oil Substances 0.000 description 11
- 239000000284 extract Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 8
- 239000002699 waste material Substances 0.000 description 7
- 238000001816 cooling Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000010642 eucalyptus oil Substances 0.000 description 4
- 229940044949 eucalyptus oil Drugs 0.000 description 4
- 244000166124 Eucalyptus globulus Species 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 238000010793 Steam injection (oil industry) Methods 0.000 description 2
- 239000010617 anise oil Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 101100298222 Caenorhabditis elegans pot-1 gene Proteins 0.000 description 1
- STECJAGHUSJQJN-GAUPFVANSA-N Hyoscine Natural products C1([C@H](CO)C(=O)OC2C[C@@H]3N([C@H](C2)[C@@H]2[C@H]3O2)C)=CC=CC=C1 STECJAGHUSJQJN-GAUPFVANSA-N 0.000 description 1
- STECJAGHUSJQJN-UHFFFAOYSA-N N-Methyl-scopolamin Natural products C1C(C2C3O2)N(C)C3CC1OC(=O)C(CO)C1=CC=CC=C1 STECJAGHUSJQJN-UHFFFAOYSA-N 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000010630 cinnamon oil Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000001289 litsea cubeba fruit oil Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- STECJAGHUSJQJN-FWXGHANASA-N scopolamine Chemical compound C1([C@@H](CO)C(=O)O[C@H]2C[C@@H]3N([C@H](C2)[C@@H]2[C@H]3O2)C)=CC=CC=C1 STECJAGHUSJQJN-FWXGHANASA-N 0.000 description 1
- 229960002646 scopolamine Drugs 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Fats And Perfumes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Disclosure one kind of plant Oleum sesami boiler, it includes boiler shell, and boiler enclosure is provided with boiler inner bag, is provided with heat-insulation layer between boiler shell and boiler inner bag;Boiler inner bag top is provided with upper steam vent baffle plate, boiler inner bag top is provided with charge door, boiler inner bag bottom is provided with discharging opening, it is provided with charging plate bottom boiler inner bag, the boiler shell of charging plate bottom is provided with sewage draining exit and steam inlet, upper steam vent baffle plate top is provided with steam and collects baffle plate, upper steam vent baffle plate and steam are collected the space between baffle plate and are formed steam chest, steam chest is provided with leads steam ports, steam is collected baffle plate top and is provided with condensation water tank, condensation water tank bottom is provided with outlet, condensation water tank top is provided with condensed water case lid, condensation water tank is covered with water inlet.The present invention has long service life, easy to operate, distillation efficiency is high, and can make full use of the feature such as heat energy of condensation water tank.
Description
Technical field
The present invention relates to boiler technical field, specifically a kind of steam is as the plant Oleum sesami boiler of thermal source, it is adaptable to distill the distillator of plant perfume, aromatic oil, for instance the branch and leaf of Fructus Anisi Stellati tree are extracted Oleum Anisi Stellati or Colophonium waste residue extracts Colophonium.
Background technology
Plant perfume, Oleum sesami distillator be the visual plant of spice processing, containing abundant Oleum Anisi Stellati in spice producing region, the branch and leaf of Fructus Anisi Stellati tree, Oleum Anisi Stellati can hyoscine, annual branch and leaf do not utilize tangible unfortunate!Extracting Oleum Anisi Stellati in the branch and leaf of Fructus Anisi Stellati tree, optimal method is the way of distillation;In addition pine gum processing industry is also adopted by way of distillation separation Oleum Terebinthinae and Colophonium.
Adopt the way of distillation, just can't do without the use of boiler.Open source literature also reports some boilers, for instance:
1, Chinese patent, title: a kind of boiler, application number: 201320279416.2, the applying date: 2013.05.22, patentee: Anhui Heng Jin agricultural development company limited, address: 236600 Tai Bo roads, area just outside a city gate town, Fuyang City Taihe County, Anhui Province, inventor: Fan Hengjin, Zhang Mengmeng, Liu Xian, model circle in the air, summary: this utility model belongs to food processing and arranges field, in particular, relates to the boiler used in a kind of food processing.A kind of boiler, including cylindrical boiler body, boiler body oral area arranges and has stated flange one, and boiler body bottom portion is provided with flange two, and boiler body exterior is provided with suspension hook on side.A kind of boiler adopting this utility model technical scheme separates with retort, this boiler can be transported to original collection place of distillation as required in the process used, being gathered on distillating material limit is concurrently placed in boiler, eliminate after distillating material collection is returned in the step being placed in boiler distillation, save time and operation, improve production efficiency.
2, Chinese patent, title: a kind of boiler for distilling Colophonium waste residue, application number: 201220688480.1, the applying date: 2012.12.13, patentee: Yunnan Flos Camelliae Japonicae Lin Hua company limited, address: 675700 Nan Jian towns, Dali Bai Autonomous prefecture, Yunnan Nan Jian county, inventor: Duan Bo, summary: this utility model proposes a kind of boiler for distilling Colophonium waste residue, relates to the processing technique field of Colophonium.It includes pot, pot offers slag inlet, slag notch and oil steam pipe, is provided with sieve plate and is positioned at the jet chimney below this sieve plate in pot;Sieve plate is removably connected by bracing frame and pot;Jet chimney is connected with pot, and the opening of this jet chimney stretches out outside pot, and offers several apertures on this jet chimney.The advantage of this utility model is, after adopting above-mentioned boiler, fully the effective volatile ingredient in Colophonium waste residue to be extracted, thus avoiding the wasting of resources, moreover it is possible to alleviate the degree of danger of waste residue and the degree of contaminated environment.
3, Chinese patent, title: a kind of boiler for extracting Oleum Anisi Stellati, the applying date: 2009.4.30, application number, 200920151108.5, patentee: Xu Pinger, address: 311400 No. 83 mailbox of Fuyang City of Zhejiang Province Chinese lute pier, inventor: Xu Pinger, summary: this utility model belongs to boiler technical field, relates to a kind of boiler for extracting Oleum Anisi Stellati.It includes water inlet pipe, pot and stove and chimney in boiler, top cover and pipe guide, bitubular cooling oil conservator, cooling bucket, pot, boiler is upper lower semi-circular middle cylinder shape, semicircle top, top sets conduit and becomes top cover and pipe guide, lower semicircular shape bottom sets water inlet pipe in the pot with control valve, bitubular cooling oil conservator is accessed in top cover and pipe guide lower end, bitubular cooling oil conservator is seated in cooling bucket, boiler is seated on brick pot and stove, pot and stove upwardly extends chimney, thus forming the boiler for extracting Oleum Anisi Stellati.This utility model has the advantage that distillation speed is fast, oil yield is high.
4, Chinese patent, title: Colophonium boiler, the applying date: 2003.10.30, application number: 200310103745.2, applicant: Lu Rangxian, address: enrich people No. 3 of three tunnels 69 in 543002 Wuzhous, Guangxi Zhuang Autonomous Region, inventor: Lu Rangxian, summary: a kind of Colophonium boiler is provided, it is by the top pot 1 with venthole, the bottom of a pan 2, steam heating coil group 3, steam injection ring pipe group 4, charging liquid level visor 5, visor 6 is observed in distillation, thermometer 8, put fragrant mouth 7 and put fragrant valve 9, grease inlet and ester inlet valve 10, distillation vapour conduit 11 and cooler 12, steam pipeline 13 grade is constituted, it is characterized in that the fragrant mouth 7 of putting of boiler is arranged on the downside of pot, near lowest point, the bottom of a pan, the bottom of a pan is one piece and puts the garden type flat board that fragrant mouth 7 tilts towards boiler, steam injection ring pipe group 3 is placed at the bottom of flat pot above 2, and with flat pot at the bottom of keep balance, both are at a distance of 20-60mm.The Colophonium boiler of this invention, reduce the setting height(from bottom) of boiler, save investment cost, it is to avoid fat liquid is half-cooked, crystallization and cause rosin quality to decline, improve Colophonium product quality.
And the present inventor studies discovery, boiler disclosed above, some unreasonable structure, cost is high, and service life is not long, inconvenient operation, the condensed water that fully can not recycle condensation having.
Summary of the invention
It is an object of the invention to provide a kind of simple in construction, easy to operate, distillation efficiency is high, can recycle the condensed water for condensing and using steam as the plant Oleum sesami boiler of thermal source, it is adaptable to distill the distillation of plant perfume, aromatic oil.
To achieve these goals, the technical solution used in the present invention is:
One kind of plant Oleum sesami boiler, it includes boiler shell, and boiler enclosure is provided with boiler inner bag, is provided with heat-insulation layer between boiler shell and boiler inner bag;Boiler inner bag top is provided with upper steam vent baffle plate, boiler inner bag top is provided with charge door, boiler inner bag bottom is provided with discharging opening, it is provided with charging plate bottom boiler inner bag, the boiler shell of charging plate bottom is provided with sewage draining exit and the steam inlet of logical vapours, upper steam vent baffle plate top is provided with steam and collects baffle plate, upper steam vent baffle plate and steam are collected the space between baffle plate and are formed steam chest, steam chest is provided with leads steam ports, steam is collected baffle plate top and is provided with condensation water tank, condensation water tank bottom is provided with outlet, condensation water tank top is provided with condensed water case lid, condensation water tank is covered with water inlet.
It is inverted " v " that described steam collects baffle plate, and its " V " shape angle is 60~130 degree, the distillating liquid of condensation is played guide functions, facilitates retort gas and the collection of Oleum sesami liquid;Steam collects the distillating liquid that can better collect water conservancy diversion condensation that arranges of baffle angle, and the liquid of minimizing distillation drips back in boiler, improves distillation extraction rate.
Described charge door and discharging opening are designed with sealing lid, it is prevented that steam is run out of.
Described heat-insulation layer inwall is provided with aluminum film heat-reflecting layer, and fully reflection utilizes the heat of steam.
Described upper steam vent baffle plate is inverted " v ", and is provided with upper steam vent, facilitates boil-off gas to pass through, and upper steam vent baffle plate is the recovery that inverted " v " is beneficial to boil-off gas.
Described charging plate is provided with steam hole, is that material can be distilled by vapours smoothly by charging plate.
Described plant Oleum sesami boiler can be used for distilling that the branch and leaf of Fructus Anisi Stellati tree extract Oleum Anisi Stellati, distillation Fructus Cinnamomi Cassiae Immaturi extracts cinnamon oil, distillation eucalyptus leaves extracts eucalyptus oil, distillation Fructus Litseae extracts litsea cubeba oil or Colophonium waste residue extracts Colophonium;Can also be used for distilling other and be with volatile plant Oleum sesami, it extracts Oleum sesami oil yield can improve more than 20%.
The beneficial effect of plant Oleum sesami boiler of the present invention:
1, plant Oleum sesami boiler simple in construction, distilling material is placed and taken out all very convenient.
2, using hydro-thermal steam as thermal source, distillation efficiency is high, and the collection and confinement of gases of distillation is convenient.
3, steam collects baffle plate is inverted " v ", it is easy to shaping and the collection of Oleum sesami gas liquid oil in condensation process, it is greatly improved the distillation rate of each kind of plant Oleum sesami, also the structure making distillation equipment is greatly simplified, the Oleum sesami of the boiler that the past adopts is only to connect condenser by the outlet of equipment top, distilling relatively low Oleum sesami and return again in the water in pot but without arriving condenser, oil yield is relatively low, adopts this structure can be greatly improved oil yield.
4, collect baffle plate top at inverted " v " steam and be provided directly with condensation water tank, retort gas is big with the condensed water temperature difference, be conducive to the conversion to liquid of the spice gas, after retort gas is condensed, discharge as heat (temperature) water, water is not contaminated, can recycle, and condensation efficiency is higher than the boiler that top outlet connects condenser.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Title and sequence number in figure be:
Sewage draining exit 1, seal lid 2, discharging opening 3, charging plate 4, steam hole 5, boiler inner chamber 6, boiler shell 7, heat-insulation layer 8, boiler inner bag 9, lead steam ports 10, upper steam vent 11, upper steam vent baffle plate 12, steam chest 13, steam collect baffle plate 14, condensed water 15, condensed water case lid 16, water inlet 17, condensation water tank 18, outlet 19, charge door 20, steam inlet 21.
Detailed description of the invention
Introducing the present invention in order to more detailed, below in conjunction with accompanying drawing, the present invention will be further described.
As it can be seen, plant Oleum sesami boiler, including boiler shell 7, boiler shell 7 is internally provided with boiler inner bag 9, is provided with heat-insulation layer 8 between boiler shell 7 and boiler inner bag 9, and heat-insulation layer 8 inwall is provided with aluminum film heat-reflecting layer;Boiler inner bag 9 top is provided with upper steam vent baffle plate 12, upper steam vent baffle plate 12 is provided with upper steam vent 11, boiler inner bag 9 top is provided with charge door 20, boiler inner bag 9 bottom is provided with discharging opening 3, charge door 20 and discharging opening 3 are designed with sealing lid 2, charging plate 4 it is provided with bottom boiler inner bag 9, charging plate 4 is provided with steam hole 5, the boiler shell 7 of charging plate 4 bottom is provided with the steam inlet 21 of sewage draining exit 1 and logical vapours, upper steam vent baffle plate 12 top is provided with the steam in inverted " v " and collects baffle plate 14, upper steam vent baffle plate 12 and steam are collected the space between baffle plate 14 and are formed steam chest 13, steam chest 13 is provided with leads steam ports 10, steam is collected baffle plate 14 top and is provided with condensation water tank 18, condensation water tank 18 bottom is provided with outlet 19, condensation water tank 18 top is provided with condensed water case lid 16, condensed water case lid 16 is provided with the water inlet 17 injecting condensed water 15.
The operation principle of the present invention is: be first shut off the sealing lid 2 of discharging opening 3, the material of distillation will be needed again, the boiler inner chamber 6 of boiler inner bag 9 is put into from charge door 20, after adding the material of distillation, close the sealing lid 2 of charge door 20, condensed water 15 is injected condensation water tank 18 from water inlet 17, vapours is passed into from steam inlet 21, material is heated distilling by vapours by the steam hole 5 of charging plate 4, the boil-off gas that material produces, the boil-off gas upper steam vent 11 by upper steam vent baffle plate 12, enter in vaporium 13, after boil-off gas runs into steam collection baffle plate 14, under the effect of condensed water, condensation is in watery, collect the inflow of baffle plate 14 wall from steam and lead steam ports 10, part boil-off gas is also discharged from leading steam ports 10;When need to change the condensed water in condensation water tank 18, original condensed water is drained into from outlet 19 place of needs, newer condensed water is injected from filler 17;The waste water, the waste residue that produce in still-process are discharged from sewage draining exit 1;After material distillation, open the sealing lid 2 of discharging opening 3, material is taken out, complete material distillation.
Application Example
1, forest farm, Guangxi adopts in the past and exports, with water cooler and equipment top, the boiler connecing condenser, carry out the anistree anistree anise-oil of leaf distillation, device structure is complicated, anistree anise-oil yield is low, the boiler of rear employing the above embodiment of the present invention, same anistree leaf raw material, same weight, it extracts Oleum sesami oil yield and improves 20% than former boiler.
2, forest farm, Guangxi adopts in the past and exports, with water cooler and equipment top, the boiler connecing condenser, carry out eucalyptus leaves distillation extraction eucalyptus oil, device structure is complicated, eucalyptus oil yield is low, the boiler of rear employing the above embodiment of the present invention, same eucalyptus leaves raw material, same weight, it extracts eucalyptus oil oil yield and improves 22% than former boiler.
Claims (3)
1. a kind of plant Oleum sesami boiler, it is characterised in that: including boiler shell (7), boiler shell (7) is internally provided with boiler inner bag (9), is provided with heat-insulation layer (8) between boiler shell (7) and boiler inner bag (9);Boiler inner bag (9) top is provided with upper steam vent baffle plate (12), boiler inner bag (9) top is provided with charge door (20), boiler inner bag (9) bottom is provided with discharging opening (3), boiler inner bag (9) bottom is provided with charging plate (4), the boiler shell (7) of charging plate (4) bottom is provided with the steam inlet (21) of sewage draining exit (1) and logical vapours, upper steam vent baffle plate (12) top is provided with steam and collects baffle plate (14), upper steam vent baffle plate (12) and steam are collected the space between baffle plate (14) and are formed steam chest (13), steam chest (13) is provided with leads steam ports (10), steam is collected baffle plate (14) top and is provided with condensation water tank (18), condensation water tank (18) bottom is provided with outlet (19), condensation water tank (18) top is provided with condensed water case lid (16), condensed water case lid (16) is provided with the water inlet (17) injecting condensed water (15);
Described steam collects baffle plate (14) in inverted " v ", and its " V " shape angle is 60~130 degree;Described heat-insulation layer (8) inwall is provided with aluminum film heat-reflecting layer;
Described upper steam vent baffle plate (12) is in inverted " v ", and is provided with upper steam vent (11);
Described charging plate (4) is provided with steam hole (5).
2. plant Oleum sesami boiler according to claim 1, it is characterised in that: described charge door (20) and discharging opening (3) are designed with sealing lid (2).
3. the application in distillation plant perfume and aromatic oil of the plant Oleum sesami boiler described in claim 1.
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CN111821720A (en) * | 2020-09-05 | 2020-10-27 | 广州鑫泽化工科技有限公司 | Preparation and processing technology of natural plant essence extract |
CN114797168A (en) * | 2022-06-28 | 2022-07-29 | 潍坊新普食品科技有限公司 | Plant extraction of essential oil device |
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JP4234692B2 (en) * | 2005-04-08 | 2009-03-04 | 株式会社エヌシーシー | Method for extracting essential oil from citrus fruits and vacuum distilled essential oil extraction device |
CN201643760U (en) * | 2010-04-20 | 2010-11-24 | 湖北俊辉药业有限公司 | Vapour extractor |
TWI423837B (en) * | 2011-10-12 | 2014-01-21 | Tzung Hui Chi | Aromatic distilled water and essential oil distilling device |
CN103740468B (en) * | 2014-02-07 | 2015-04-08 | 郭永来 | Steam distillation aromatic essential oil equipment |
CN204502440U (en) * | 2015-01-22 | 2015-07-29 | 李而宏 | One Plants sesame oil boiler |
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