CN209138001U - A kind of alcohol distillation column rapid condensation device - Google Patents

A kind of alcohol distillation column rapid condensation device Download PDF

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Publication number
CN209138001U
CN209138001U CN201821787287.7U CN201821787287U CN209138001U CN 209138001 U CN209138001 U CN 209138001U CN 201821787287 U CN201821787287 U CN 201821787287U CN 209138001 U CN209138001 U CN 209138001U
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China
Prior art keywords
condensing unit
pipeline
alcohol
tower body
distillation column
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CN201821787287.7U
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Chinese (zh)
Inventor
秦承雪
秦银基
秦文基
刘振勋
任燕茹
张晓�
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SHANDONG HANFANG PHARMACEUTICAL CO Ltd
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SHANDONG HANFANG PHARMACEUTICAL CO Ltd
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A kind of alcohol distillation column rapid condensation device, including alcohol distillation column, the alcohol distillation column includes tower body, gas sensor is equipped in tower body, tower reactor is connected in the lower part of tower body, steam heater is connected with by pipeline in the bottom end of tower reactor, the first condensing unit is connected with by pipeline at the top of tower body, the other end of first condensing unit is connected with the second condensing unit by pipeline, the other end of second condensing unit is connected with alcohol recycle tank by pipeline, second distillation device is additionally provided between the first condensing unit and the second condensing unit, the first solenoid valve is equipped in pipeline between the first condensing unit and the second condensing unit, liquid valve door is equipped in pipeline between the second condensing unit and alcohol recycle tank;Different condensation process can be selected according to the component of raw material in tower reactor, simplified the preparation flow of alcoholic solution, improved the purity of alcoholic solution.

Description

A kind of alcohol distillation column rapid condensation device
Technical field:
The utility model relates to a kind of alcohol distillation column rapid condensation devices.
Background technique:
Alcohol distillation column is common a kind of equipment in the industries such as pharmacy, food, light industry, chemical industry, its working principle is that It is lower than the characteristic of other solution boiling points, with the temperature of a little higher than alcohol boiling point, the alcoholic solution that will need to be recycled using alcohol boiling point Heating volatilization is carried out, after alcohol recycle column distillation, alcohol gas is precipitated, improves the concentration of alcoholic solution, reaches recovered alcohol Purpose.
Existing alcohol distillation column only simply distills raw material, after obtaining retort gas, condenses through condenser Solution is obtained, is recycled;This technique is suitable for the single situation of raw material components, when raw material components are complex, uses This technique, impurity content is more in finally obtained alcoholic solution, and needing to carry out other techniques could remove in alcoholic solution Impurity, obtain the higher alcohol of purity, it is time-consuming and laborious, it is cumbersome.
Utility model content:
The utility model in order to make up for the deficiencies of the prior art, provides a kind of alcohol distillation column rapid condensation device, knot Structure design rationally, can select different condensation process according to the component of raw material in tower reactor, simplify the preparation stream of alcoholic solution Journey improves the purity of alcoholic solution, solves problems of the prior art.
Used technical solution is the utility model to solve above-mentioned technical problem:
A kind of alcohol distillation column rapid condensation device, including alcohol distillation column, the alcohol distillation column includes tower body, in tower The lower part of body is connected with tower reactor, is connected with steam heater by pipeline in the bottom end of tower reactor, passes through pipe at the top of tower body Road is connected with the first condensing unit, and the other end of first condensing unit is connected with the second condensing unit by pipeline, described The other end of second condensing unit is connected with alcohol recycle tank by pipeline, between the first condensing unit and the second condensing unit It is additionally provided with second distillation device, the first solenoid valve is equipped in the pipeline between the first condensing unit and the second condensing unit, Liquid valve door is equipped in pipeline between second condensing unit and alcohol recycle tank, the vapo(u)rizing temperature of the tower reactor is higher than alcohol Boiling point, the temperature of the second distillation device are lower than the boiling point of alcohol.
The steam heater includes vapor interface, is connected with steam storage tank by pipeline on vapor interface, Air intake valve is equipped in pipeline between vapor interface and steam storage tank, the steam storage tank passes through pipeline and tower reactor phase Even.
The barometer popped one's head in and protruded into inside steam storage tank is equipped on steam storage tank.
First condensing unit includes shell, the trapezoidal condenser pipe that is connected is equipped in shell, on trapezoidal condenser pipe Equipped with the first condensed water water inlet line and the first condensed water outlet conduit.
Second condensing unit includes shell, and the circular ring shape condenser pipe being connected is equipped in shell, cold in circular ring shape Solidifying pipe is equipped with the second condensed water water inlet line and the second condensed water outlet conduit.
The second distillation device includes two alembics, is respectively equipped with electric heating wire, the alembic in each alembic It is connected respectively by pipeline with the first condensing unit, the alembic is connected by Y-shaped pipeline with the second condensing unit.
Filter screen is respectively equipped in pipeline between alembic and the first condensing unit.
Second solenoid valve is equipped in Y-shaped pipeline.
It is equipped with active carbon disinfection network between tower body and the first condensing unit, densitometer is equipped in alcohol recycle tank.
Gas sensor is equipped in tower body;
The gas sensor is for detecting raw material components and transmitting information;
The information opens second solenoid valve for prompting the user whether.
The utility model using the above structure, the component of retort gas is judged by the gas sensor in tower reactor, from And select different preparation flows;It is removed in retort gas by the active carbon disinfection network between tower body and the first condensing unit Organic substance;The concentration of alcoholic solution is detected by the densitometer in alcohol recycle tank, easy to operate, time saving and energy saving, energy It is enough quickly to prepare the higher alcoholic solution of purity.Have the advantages that efficient convenience, structure novel.
Detailed description of the invention:
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the structural schematic diagram of first condensing unit of the utility model.
Fig. 3 is the structural schematic diagram of second condensing unit of the utility model.
In figure, 1, tower body, 2, gas sensor, 3, tower reactor, 4, alcohol recycle tank, the 5, first solenoid valve, 6, liquid valve door, 7, vapor interface, 8, steam storage tank, 9, air intake valve, 10, barometer, 11, trapezoidal condenser pipe, the water inlet of the 12, first condensed water Pipeline, the 13, first condensed water outlet conduit, 14, circular ring shape condenser pipe, the 15, second condensed water water inlet line, the 16, second condensation Water outlet conduit, 17, alembic, 18, electric heating wire, 19, Y-shaped pipeline, 20, filter screen, 21, second solenoid valve, 22, active carbon Disinfection network, 23, densitometer.
Specific embodiment:
In order to clarify the technical characteristics of the invention, below by specific embodiment, and its attached drawing is combined, to this reality It is described in detail with novel.
As illustrated in fig. 1-3, a kind of alcohol distillation column rapid condensation device, including alcohol distillation column, the alcohol recycle Tower includes tower body 1, is connected with tower reactor 3 in the lower part of tower body 1, is connected with steam heater by pipeline in the bottom end of tower reactor 3, First condensing unit is connected with by pipeline at the top of tower body 1, the other end of first condensing unit is connected by pipeline There is the second condensing unit, the other end of second condensing unit is connected with alcohol recycle tank 4 by pipeline, in the first condensation dress It sets and is additionally provided with second distillation device between the second condensing unit, the pipeline between the first condensing unit and the second condensing unit It is inside equipped with the first solenoid valve 5, liquid valve door 6, the tower are equipped in the pipeline between the second condensing unit and alcohol recycle tank 4 The vapo(u)rizing temperature of kettle 3 is higher than the boiling point of alcohol, and the temperature of the second distillation device is lower than the boiling point of alcohol.
The steam heater includes vapor interface 7, is connected with steam storage tank 8 by pipeline on vapor interface 7, Air intake valve 9 is equipped in pipeline between vapor interface 7 and steam storage tank 8, the steam storage tank 8 passes through pipeline and tower Kettle 3 is connected.
The barometer 10 popped one's head in and protruded into inside steam storage tank 8 is equipped on steam storage tank 8.
First condensing unit includes shell, the trapezoidal condenser pipe 11 that is connected is equipped in shell, in trapezoidal condenser pipe 11 are equipped with the first condensed water water inlet line 12 and the first condensed water outlet conduit 13.
Second condensing unit includes shell, the circular ring shape condenser pipe 14 being connected is equipped in shell, in circular ring shape Condenser pipe 14 is equipped with the second condensed water water inlet line 15 and the second condensed water outlet conduit 16.
The second distillation device includes two alembics 17, is respectively equipped with electric heating wire 18 in each alembic 17, described Alembic 17 is connected by pipeline with the first condensing unit respectively, and the alembic passes through Y-shaped pipeline 19 and the second condensing unit It is connected.
Filter screen 20 is respectively equipped in pipeline between alembic 17 and the first condensing unit.
Second solenoid valve 21 is equipped in Y-shaped pipeline 19.
It is equipped with active carbon disinfection network 22 between tower body 1 and the first condensing unit, densitometer is equipped in alcohol recycle tank 4 23。
Gas sensor 2 is equipped in tower body 1;
The gas sensor 2 is for detecting raw material components and transmitting information;
The information opens second solenoid valve 21 for prompting the user whether.
In use, being placed with raw material in tower reactor 3, vapor interface 7 accesses external steam unit, opens air intake valve 9, Steam is stored in steam storage tank 8, the barometer 10 on steam storage tank 8 detects steam content in steam storage tank 8, guarantees dress Steam in setting is sufficient, promotes distillation quality;Raw material is distilled in tower reactor 3, retort gas is obtained and is stored in tower body 1 And the component of retort gas is examined by gas sensor 2, and when component is single in retort gas, only alcohol gas or a small amount of miscellaneous When matter, the first solenoid valve 5 is opened, the circular ring shape on the trapezoidal condenser pipe 11 and the second condensing unit on the first condensing unit is passed through Condenser pipe 14 carries out condensation process, obtains alcoholic solution, opens liquid valve door 6, is collected in alcohol recycle tank 4, trapezoidal Condenser pipe 11 and circular ring shape condenser pipe 14 can be improved the efficiency of condensation;When the component of retort gas is complex, the is closed One solenoid valve 5 opens second solenoid valve 21, second distillation is carried out in alembic 17, removes extra gas component, filter screen 20 can filter out the impurity liquid generated in the condensation of the first condensing unit, obtain the higher ethanol gas of purity by second distillation Body passes through the second condensing unit again and is handled, and obtains alcoholic solution;Densitometer 23 in alcohol recycle tank 4 can detecte alcohol Purity, guarantee alcohol quality;Active carbon disinfection network 22 can be reduced in retort gas with organic gas in adsorptive distillation gas Impurity improves alcohol purity.
Above-mentioned specific embodiment cannot function as the limitation to scope of protection of the utility model, for the skill of the art For art personnel, any alternate modification or transformation made to the utility model embodiment all fall within the guarantor of the utility model It protects in range.
Place is not described in detail for the utility model, is the well-known technique of those skilled in the art of the present technique.

Claims (10)

1. a kind of alcohol distillation column rapid condensation device, it is characterised in that: including alcohol distillation column, the alcohol distillation column includes Tower body, is connected with tower reactor in the lower part of tower body, steam heater is connected with by pipeline in the bottom end of tower reactor, on the top of tower body Portion is connected with the first condensing unit by pipeline, and the other end of first condensing unit is connected with the second condensation dress by pipeline It sets, the other end of second condensing unit is connected with alcohol recycle tank by pipeline, condenses in the first condensing unit and second It is additionally provided with second distillation device between device, the first electricity is equipped in the pipeline between the first condensing unit and the second condensing unit Magnet valve, liquid valve door is equipped in the pipeline between the second condensing unit and alcohol recycle tank, and the vapo(u)rizing temperature of the tower reactor is high In the boiling point of alcohol, the temperature of the second distillation device is lower than the boiling point of alcohol.
2. the apparatus according to claim 1, it is characterised in that: the steam heater includes vapor interface, in steam Steam storage tank is connected with by pipeline on interface, intake valve is equipped in the pipeline between vapor interface and steam storage tank Door, the steam storage tank are connected by pipeline with tower reactor.
3. the apparatus of claim 2, it is characterised in that: be equipped with probe on steam storage tank and protrude into steam storage tank Internal barometer.
4. the apparatus according to claim 1, it is characterised in that: first condensing unit includes shell, is set in shell There is the trapezoidal condenser pipe that is connected, the first condensed water water inlet line and the first condensed water outlet conduit are equipped on trapezoidal condenser pipe.
5. the apparatus according to claim 1, it is characterised in that: second condensing unit includes shell, is set in shell There is the circular ring shape condenser pipe being connected, the second condensed water water inlet line is equipped on circular ring shape condenser pipe and the second condensed water is discharged Pipeline.
6. the apparatus according to claim 1, it is characterised in that: the second distillation device includes two alembics, Mei Gezheng It evaporates and is respectively equipped with electric heating wire in tank, the alembic passes through pipeline respectively and is connected with the first condensing unit, and the alembic is logical Y-shaped pipeline is crossed to be connected with the second condensing unit.
7. device according to claim 6, it is characterised in that: divide in the pipeline between alembic and the first condensing unit It She You not filter screen.
8. device according to claim 6, it is characterised in that: be equipped with second solenoid valve in Y-shaped pipeline.
9. the apparatus according to claim 1, it is characterised in that: disappear between tower body and the first condensing unit equipped with active carbon Malicious net is equipped with densitometer in alcohol recycle tank.
10. the apparatus according to claim 1, it is characterised in that: be equipped with gas sensor in tower body;
The gas sensor is for detecting raw material components and transmitting information;
The information opens second solenoid valve for prompting the user whether.
CN201821787287.7U 2018-10-31 2018-10-31 A kind of alcohol distillation column rapid condensation device Active CN209138001U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821787287.7U CN209138001U (en) 2018-10-31 2018-10-31 A kind of alcohol distillation column rapid condensation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821787287.7U CN209138001U (en) 2018-10-31 2018-10-31 A kind of alcohol distillation column rapid condensation device

Publications (1)

Publication Number Publication Date
CN209138001U true CN209138001U (en) 2019-07-23

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Application Number Title Priority Date Filing Date
CN201821787287.7U Active CN209138001U (en) 2018-10-31 2018-10-31 A kind of alcohol distillation column rapid condensation device

Country Status (1)

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CN (1) CN209138001U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111454800A (en) * 2020-05-13 2020-07-28 仲崇涛 Integrated intelligent fermentation wine making equipment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111454800A (en) * 2020-05-13 2020-07-28 仲崇涛 Integrated intelligent fermentation wine making equipment
CN111454800B (en) * 2020-05-13 2024-01-30 仲崇涛 Integrated intelligent wine fermenting equipment

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