CN104603615A - 测定树脂的粘性温度的方法 - Google Patents
测定树脂的粘性温度的方法 Download PDFInfo
- Publication number
- CN104603615A CN104603615A CN201380046454.6A CN201380046454A CN104603615A CN 104603615 A CN104603615 A CN 104603615A CN 201380046454 A CN201380046454 A CN 201380046454A CN 104603615 A CN104603615 A CN 104603615A
- Authority
- CN
- China
- Prior art keywords
- reactor
- temperature
- ica
- resin
- polymerization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N19/00—Investigating materials by mechanical methods
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/22—Investigating strength properties of solid materials by application of mechanical stress by applying steady torsional forces
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
- G01N33/442—Resins; Plastics
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2430/00—Assays, e.g. immunoassays or enzyme assays, involving synthetic organic compounds as analytes
- G01N2430/60—Synthetic polymers other than synthetic polypeptides as analytes
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Immunology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Adhesives Or Adhesive Processes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810024562.8A CN108106968B (zh) | 2012-09-07 | 2013-09-04 | 控制聚合反应器的系统 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261698286P | 2012-09-07 | 2012-09-07 | |
| US61/698,286 | 2012-09-07 | ||
| PCT/US2013/058002 WO2014039522A1 (en) | 2012-09-07 | 2013-09-04 | A method for determining a stickiness temperature of a resin |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810024562.8A Division CN108106968B (zh) | 2012-09-07 | 2013-09-04 | 控制聚合反应器的系统 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104603615A true CN104603615A (zh) | 2015-05-06 |
Family
ID=49170913
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810024562.8A Active CN108106968B (zh) | 2012-09-07 | 2013-09-04 | 控制聚合反应器的系统 |
| CN201380046454.6A Pending CN104603615A (zh) | 2012-09-07 | 2013-09-04 | 测定树脂的粘性温度的方法 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810024562.8A Active CN108106968B (zh) | 2012-09-07 | 2013-09-04 | 控制聚合反应器的系统 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US10029226B2 (enExample) |
| EP (2) | EP3968020B1 (enExample) |
| CN (2) | CN108106968B (enExample) |
| BR (1) | BR112015004883B1 (enExample) |
| ES (2) | ES2914610T3 (enExample) |
| IN (1) | IN2015DN01316A (enExample) |
| RU (1) | RU2657418C2 (enExample) |
| WO (1) | WO2014039522A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108473626A (zh) * | 2015-12-17 | 2018-08-31 | 道达尔研究技术弗吕公司 | 用于确定烯烃聚合反应器的一个或多个操作条件的方法 |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140202205A1 (en) * | 2013-01-22 | 2014-07-24 | Air Liquide Large Industries U.S. Lp | Reactor liquid cooldown method |
| BR112017010747B1 (pt) | 2014-11-25 | 2021-11-16 | Univation Technologies, Llc | Métodos de controle de índice de fusão de poliolefina |
| BR112017010363B1 (pt) | 2014-11-25 | 2022-05-10 | Univation Technologies, Llc | Método para mudar taxa de produção de poliolefina com a composição de agentes de condensação induzidos |
| CN113677713A (zh) * | 2019-03-21 | 2021-11-19 | 埃克森美孚化学专利公司 | 改进气相聚合的方法 |
| CN113614117B (zh) | 2019-03-21 | 2023-06-20 | 埃克森美孚化学专利公司 | 改进气相聚合中生产的方法 |
| CN112414898B (zh) | 2020-11-10 | 2021-12-21 | 中国农业科学院农产品加工研究所 | 复合粉体混合均匀度的评价方法 |
| CN116413382A (zh) * | 2021-12-29 | 2023-07-11 | 中国石油天然气股份有限公司 | 一种乙烯聚合评价试验装置的评价方法 |
| US20250206859A1 (en) | 2022-03-31 | 2025-06-26 | Exxonmobil Chemical Patents Inc. | Linear low density polyethylenes, polymerizations thereof, and films thereof |
| WO2024044423A1 (en) | 2022-08-22 | 2024-02-29 | Exxonmobil Chemical Patents, Inc. | Polyethylene compositions and films made therefrom |
| EP4584306A1 (en) | 2022-09-07 | 2025-07-16 | ExxonMobil Chemical Patents Inc. | Polyethylenes and articles thereof |
| WO2025250307A1 (en) | 2024-05-30 | 2025-12-04 | ExxonMobil Technology and Engineering Company | Methods for improving gas phase polymerization |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1582305A (zh) * | 2001-12-20 | 2005-02-16 | 联合碳化化学及塑料技术公司 | 湍流条件下在流化床中的高冷凝模式聚烯烃生产方法 |
| CN2852109Y (zh) * | 2005-12-29 | 2006-12-27 | 华东理工大学 | 高温高压旋转粘度计 |
| US20070265400A1 (en) * | 2006-05-12 | 2007-11-15 | Fischbuch D B | Low molecular weight induced condensing agents |
| CN101511877A (zh) * | 2006-09-07 | 2009-08-19 | 尤尼威蒂恩技术有限责任公司 | 由聚合反应监测产生的数据确定指示树脂粘附的温度值的方法 |
| CN101511882A (zh) * | 2006-09-07 | 2009-08-19 | 尤尼威蒂恩技术有限责任公司 | 使用降低熔融起始温度的模型在线测定树脂粘着性程度的方法 |
| CN101720334A (zh) * | 2007-02-16 | 2010-06-02 | 尤尼威蒂恩技术有限责任公司 | 在线监测和控制聚合方法和反应器以防止中断事故的方法 |
| CN102015090A (zh) * | 2008-04-22 | 2011-04-13 | 尤尼威蒂恩技术有限公司 | 反应器系统和使用该反应器系统的方法 |
| CN102050985A (zh) * | 2010-12-30 | 2011-05-11 | 浙江工业大学 | 一种提高超高分子量聚乙烯树脂加工流变性的方法 |
| CN102346123A (zh) * | 2011-07-18 | 2012-02-08 | 上海化工研究院 | 一种分析超高分子量聚乙烯树脂溶胀性能的方法 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4543399A (en) | 1982-03-24 | 1985-09-24 | Union Carbide Corporation | Fluidized bed reaction systems |
| US4588790A (en) | 1982-03-24 | 1986-05-13 | Union Carbide Corporation | Method for fluidized bed polymerization |
| NZ235032A (en) | 1989-08-31 | 1993-04-28 | Dow Chemical Co | Constrained geometry complexes of titanium, zirconium or hafnium comprising a substituted cyclopentadiene ligand; use as olefin polymerisation catalyst component |
| US5026798A (en) | 1989-09-13 | 1991-06-25 | Exxon Chemical Patents Inc. | Process for producing crystalline poly-α-olefins with a monocyclopentadienyl transition metal catalyst system |
| US5352749A (en) | 1992-03-19 | 1994-10-04 | Exxon Chemical Patents, Inc. | Process for polymerizing monomers in fluidized beds |
| US5436304A (en) | 1992-03-19 | 1995-07-25 | Exxon Chemical Patents Inc. | Process for polymerizing monomers in fluidized beds |
| AU682821B2 (en) | 1993-04-26 | 1997-10-23 | Exxon Chemical Patents Inc. | Process for polymerizing monomers in fluidized beds |
| US5342907A (en) * | 1993-06-28 | 1994-08-30 | Union Carbide Chemicals & Plastics Technology Corporation | Ethylene/propylene copolymer rubbers |
| US5747406A (en) | 1997-01-10 | 1998-05-05 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for the production of olefin polymers |
| US6242545B1 (en) | 1997-12-08 | 2001-06-05 | Univation Technologies | Polymerization catalyst systems comprising substituted hafinocenes |
| US6069213A (en) | 1997-12-16 | 2000-05-30 | Union Carbide Chemicals & Plastics Technology Corporation | Mixed catalyst system |
| US6894131B2 (en) | 1998-08-21 | 2005-05-17 | Univation Technologies, Llc | Polymerization process using a metallocene catalyst system |
| JP2001255251A (ja) * | 2000-03-13 | 2001-09-21 | Sumitomo Bakelite Co Ltd | フェノール樹脂成形材料の流動性評価方法 |
| US7226789B2 (en) | 2001-12-17 | 2007-06-05 | Unication Technolofies, Llc | Method of applying non-linear dynamics to control a gas-phase polyethylene reactor operability |
| US6846884B2 (en) | 2002-09-27 | 2005-01-25 | Union Carbide Chemicals & Plastics Technology Corporation | Control of resin properties |
| WO2005049663A2 (en) | 2002-10-15 | 2005-06-02 | Exxonmobil Chemical Patents Inc. | On-line measurement and control of polymer properties by raman spectroscopy |
| US7244795B2 (en) | 2003-12-08 | 2007-07-17 | Univation Technologies, Llc | Polymerization process using metallocene catalyst systems |
| US7410926B2 (en) | 2003-12-30 | 2008-08-12 | Univation Technologies, Llc | Polymerization process using a supported, treated catalyst system |
| US7683140B2 (en) | 2004-05-20 | 2010-03-23 | Univation Technologies, Llc | Method for determining temperature value indicative of resin stickiness from data generated by polymerization reaction monitoring |
| KR100895168B1 (ko) | 2004-05-20 | 2009-05-04 | 유니베이션 테크놀로지즈, 엘엘씨 | 가스 올레핀 중합 방법 |
| WO2006009980A2 (en) | 2004-06-21 | 2006-01-26 | Exxonmobil Chemical Patents Inc. | Olefin polymerisation process |
| US20060058427A1 (en) * | 2004-09-15 | 2006-03-16 | O'neill Julia C | Power-controlled bonding of resin or (co)polymer powder and flake materials |
| WO2008076386A1 (en) * | 2006-12-18 | 2008-06-26 | Univation Technologies, Llc | Method for reducing and/or preventing production of excessively low density polymer product during polymerization transitions |
| KR101518695B1 (ko) * | 2006-12-29 | 2015-05-08 | 바셀 폴리올레핀 이탈리아 에스.알.엘 | 폴리올레핀 마감손질을 위한 공정 |
-
2013
- 2013-09-04 IN IN1316DEN2015 patent/IN2015DN01316A/en unknown
- 2013-09-04 RU RU2015112331A patent/RU2657418C2/ru active
- 2013-09-04 US US14/424,797 patent/US10029226B2/en active Active
- 2013-09-04 EP EP21206074.3A patent/EP3968020B1/en active Active
- 2013-09-04 ES ES13762675T patent/ES2914610T3/es active Active
- 2013-09-04 EP EP13762675.0A patent/EP2893342B1/en active Active
- 2013-09-04 CN CN201810024562.8A patent/CN108106968B/zh active Active
- 2013-09-04 BR BR112015004883-8A patent/BR112015004883B1/pt active IP Right Grant
- 2013-09-04 ES ES21206074T patent/ES2987855T3/es active Active
- 2013-09-04 WO PCT/US2013/058002 patent/WO2014039522A1/en not_active Ceased
- 2013-09-04 CN CN201380046454.6A patent/CN104603615A/zh active Pending
-
2018
- 2018-07-12 US US16/033,893 patent/US20180326386A1/en not_active Abandoned
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1582305A (zh) * | 2001-12-20 | 2005-02-16 | 联合碳化化学及塑料技术公司 | 湍流条件下在流化床中的高冷凝模式聚烯烃生产方法 |
| CN2852109Y (zh) * | 2005-12-29 | 2006-12-27 | 华东理工大学 | 高温高压旋转粘度计 |
| US20070265400A1 (en) * | 2006-05-12 | 2007-11-15 | Fischbuch D B | Low molecular weight induced condensing agents |
| CN101511877A (zh) * | 2006-09-07 | 2009-08-19 | 尤尼威蒂恩技术有限责任公司 | 由聚合反应监测产生的数据确定指示树脂粘附的温度值的方法 |
| CN101511882A (zh) * | 2006-09-07 | 2009-08-19 | 尤尼威蒂恩技术有限责任公司 | 使用降低熔融起始温度的模型在线测定树脂粘着性程度的方法 |
| CN101720334A (zh) * | 2007-02-16 | 2010-06-02 | 尤尼威蒂恩技术有限责任公司 | 在线监测和控制聚合方法和反应器以防止中断事故的方法 |
| CN102015090A (zh) * | 2008-04-22 | 2011-04-13 | 尤尼威蒂恩技术有限公司 | 反应器系统和使用该反应器系统的方法 |
| CN102050985A (zh) * | 2010-12-30 | 2011-05-11 | 浙江工业大学 | 一种提高超高分子量聚乙烯树脂加工流变性的方法 |
| CN102346123A (zh) * | 2011-07-18 | 2012-02-08 | 上海化工研究院 | 一种分析超高分子量聚乙烯树脂溶胀性能的方法 |
Non-Patent Citations (1)
| Title |
|---|
| L.L.BLYLER,JR: "An analysis of brabender torque rheometer date", 《POLYMER ENGINEERING AND SCIERNCE》, 1 July 1964 (1964-07-01), pages 1 - 4 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108473626A (zh) * | 2015-12-17 | 2018-08-31 | 道达尔研究技术弗吕公司 | 用于确定烯烃聚合反应器的一个或多个操作条件的方法 |
| CN108473626B (zh) * | 2015-12-17 | 2021-08-17 | 道达尔研究技术弗吕公司 | 用于确定烯烃聚合反应器的一个或多个操作条件的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP3968020B1 (en) | 2024-07-24 |
| CN108106968A (zh) | 2018-06-01 |
| ES2914610T3 (es) | 2022-06-14 |
| RU2657418C2 (ru) | 2018-06-13 |
| WO2014039522A1 (en) | 2014-03-13 |
| BR112015004883B1 (pt) | 2021-11-09 |
| US10029226B2 (en) | 2018-07-24 |
| IN2015DN01316A (enExample) | 2015-07-03 |
| EP2893342A1 (en) | 2015-07-15 |
| US20150209751A1 (en) | 2015-07-30 |
| RU2015112331A (ru) | 2016-10-27 |
| BR112015004883A2 (pt) | 2017-07-04 |
| CN108106968B (zh) | 2020-09-25 |
| ES2987855T3 (es) | 2024-11-18 |
| EP3968020A1 (en) | 2022-03-16 |
| US20180326386A1 (en) | 2018-11-15 |
| EP2893342B1 (en) | 2022-04-27 |
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Application publication date: 20150506 |