CN104592821A - Water-based industrial anti-corrosion paint and preparation method thereof - Google Patents
Water-based industrial anti-corrosion paint and preparation method thereof Download PDFInfo
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- CN104592821A CN104592821A CN201510050488.3A CN201510050488A CN104592821A CN 104592821 A CN104592821 A CN 104592821A CN 201510050488 A CN201510050488 A CN 201510050488A CN 104592821 A CN104592821 A CN 104592821A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a water-based industrial anti-corrosion paint, which is prepared from the following components in parts by weight: 25-50 parts of a water-based styrene-acrylic emulsion, 1-5 parts of a preservative, 1-5 parts of propylene glycol, 1-5 parts of sodium phosphate dodecahydrate, 1-15 parts of zinc phosphate, 1-15 parts of modified aluminium triphosphate, 1-15 parts of ferrotitanium powder, 1-10 parts of polyaniline, 5-15 parts of talcum powder, 1-10 parts of glass flakes, 0.1-1.0 part of an antifoaming agent, 0.1-1.0 part of a flatting agent and 5-25 parts of deionized water. The invention further discloses a preparation method of the water-based industrial anti-corrosion paint. The water-based industrial anti-corrosion paint disclosed by the invention has the characteristics of good flash-rust resisting property, good chemical resistance, and good storage stability, can be molded by thick coating once, and does not contain poisonous or harmful heavy metals.
Description
Technical field
The present invention relates to a kind of coating, relate to a kind of aqueous industrial protective system and preparation method thereof specifically, mainly use in metallic surface, play a protective role.
Background technology
According to statistics, the whole world is probably 20% of annual production because of the metal of corrosion every year, and China accounts for 4% of GDP because corroding the financial loss that causes every year, and loss has even exceeded the summation of all kinds of natural disaster.Therefore anti-corrosion of metal becomes the most direct way that economizes on resources; and use protective system to be the most effective guard method; all the time; most protective system is all solvent type; and solvent based coating not only inflammable, explosive, toxicity is high; and solvent price is high, after film forming, also environmental pollution can be caused in solvent evaporates to air.Therefore, research uses environment friendly anti-corrosive paint to become current Main way, and the protective system of environmental protection in the market has solvent-free UV coating paint, powder coating and water-borne coatings, and in these environmental protection coating materials, water-borne coatings uses the most extensive, studies the most active.But production and the use of current domestic water-based anticorrosive paint are not also popularized, and restriction water-based anticorrosive paint is produced and the main reason of application is that the performance of water-based anticorrosive paint and the performance of similar solvent-borne type protective system also exist gap.
Summary of the invention
For the deficiencies in the prior art, first object of the present invention is to provide a kind of aqueous industrial protective system, it have anti-ly dodge that rust performance is good, chemical resistance is good, can once thick painting shaping, containing poisonous and hazardous heavy metal and the good feature of storage stability.
Second object of the present invention is the preparation method in order to provide a kind of aqueous industrial protective system.
Realize first object of the present invention to reach by taking following technical scheme:
A kind of aqueous industrial protective system, is characterized in that, be prepared from by following composition by weight:
As preferably, described aqueous industrial protective system, is prepared from by following composition by weight:
As preferably, described waterborne styrene-acrylic emulsion is the model that Nanchang Ward Chemical Co., Ltd. produces is the benzene emulsion of WB-313.
As preferably, described sanitas is HTK-30 fungicidal preservative.
As preferably, described flow agent is the EFKA3034 flow agent of EFKA company.
As preferably, described defoamer is the tegoFoamex1488 defoamer of German Di Gao chemical company.
As preferably, described aluminium triphosphate is the modification aluminium triphosphate that Weihai Tian Chuan Fine Chemical Co., Ltd produces.
A preparation method for aqueous industrial protective system, is characterized in that, comprises the steps:
1) waterborne styrene-acrylic emulsion of formula ratio, sanitas, propylene glycol, ten phosphate dihydrate sodium are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add the zinc phosphate of formula ratio, modification aluminium triphosphate, ferrotitanium powder, polyaniline, talcum powder, glass flake, controlling rotating speed is 1200 turns/min, and jitter time is 10-15min, obtains uniform second solution;
3) flow agent added in the second solution, defoamer, deionized water, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
As preferably, fineness≤70 μm of the second described solution.
Beneficial effect of the present invention is:
1, the present invention is by raw material composition and the optimization of consumption, obtains a kind of aqueous industrial protective system, it have anti-ly dodge that rust performance is good, chemical resistance is good, can once thick painting shaping, containing poisonous and hazardous heavy metal and the good advantage of storage stability.The anti-sudden strain of a muscle rust performance good (range estimation 15min not blackening) of product, chemical resistance good (SaltSprayTest), can once thick painting shaping (paint film >=100mm), coating is not containing poisonous and hazardous heavy metal.
2, the synthesis technique of product of the present invention is simple, easy construction.
3, the storage stability of product of the present invention is good, and product is preserved at normal temperature and never degenerated for 12 months.
4, product performance of the present invention are various, by selecting different types of emulsion, powder and auxiliary agent, can obtain the product of different performance.
To sum up, product of the present invention have chemical resistance good, can once thick painting be shaping, easy construction, anti-sudden strain of a muscle rust performance is good, because the material used is not containing objectionable impuritiess such as heavy metals, so coating environmental protection, also has production technique simple in addition, feature easy to use.
Embodiment
Below, in conjunction with embodiment, the present invention is described further:
In an embodiment of the present invention, described waterborne styrene-acrylic emulsion is the model that Nanchang Ward Chemical Co., Ltd. produces is the benzene emulsion of WB-313.The component of benzene emulsion: vinylbenzene, CALCIUM ACRYLATE and function monomer copolymerization anionic emulsion.Its performance and purposes: due to the introducing of organosilicon function monomer, drastically increase the water tolerance (paint film is met water and can not be returned white) of film, weathering resistance and resistance to crocking; Good with base material sticking power, the Calcium ion stability of emulsion is good, and over-all properties is higher than general benzene emulsion.Rational cost performance, especially its distinguishing feature.
Sanitas is HTK-30 fungicidal preservative.
Flow agent is the EFKA3034 flow agent of EFKA company.
Defoamer is tegoFoamex 1488 defoamer of German Di Gao chemical company.
Aluminium triphosphate is the modification aluminium triphosphate that Weihai Tian Chuan Fine Chemical Co., Ltd produces.Product main component: the main antirust group of aluminium triphosphate (ALH2P2O10.2H2O): P3O10-5.Rhombic system crystallization, non-volatile white micro-crystals powder, is insoluble in water, is slightly soluble in alcohol, density 2.0-3.0g/cm3, nontoxic, has no stimulation to skin, and Heat stability is good is more stable to acid.
Propylene glycol is provided by Taizhou Ling Gu Fine Chemical Co., Ltd; Ten phosphate dihydrate sodium are provided by the emerging milky way Chemical Co., Ltd. in Hubei; Zinc phosphate is provided by Weihai Tian Chuan Fine Chemical Co., Ltd; Ferrotitanium powder is provided by Weihai Tian Chuan Fine Chemical Co., Ltd; Polyaniline is provided by Guangzhou turn of speed Chemical Industry Science Co., Ltd; Talcum powder is provided by the rich Chemical Co., Ltd. of Dongguan City three; Glass flake is provided by Langfang, Hebei province Peng Xiang glass flake company limited;
Embodiment 1:
Be equipped with 100Kg aqueous industrial protective system, its preparation method carries out according to the following steps:
1) waterborne styrene-acrylic emulsion 31.8Kg, sanitas 3Kg, propylene glycol 2Kg, ten phosphate dihydrate sodium 3Kg are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add zinc phosphate 4Kg, modification aluminium triphosphate 12Kg, ferrotitanium powder 6Kg, polyaniline 4Kg, talcum powder 12Kg, glass flake 3Kg, controlling rotating speed is 1200 turns/min, and jitter time is 10min, obtains uniform second solution; Control fineness≤70 μm of the second solution;
3) in the second solution, add flow agent 0.7Kg, defoamer 0.5Kg, deionized water 18Kg, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
Detect the aqueous industrial protective system that the present embodiment obtains, concrete detected result is as follows:
Stability in storage: normal temperature is placed 12 months product viscosity and become 28s from 25s, without precipitation, without layering, proves that product shelf life is greater than 12 months.Salt water resistance (5% sodium-chlor), 20 days without considerable change (GB/T9274-88), sticking power 0 grade (hundred lattice methods), salt spray resistance (3% sodium-chlor) 20 days is without considerable change (GB/1771-91), a film >=100mm, range estimation 15min not blackening.
Embodiment 2:
Be equipped with 100Kg aqueous industrial protective system, its preparation method carries out according to the following steps:
1) waterborne styrene-acrylic emulsion 38Kg, sanitas 3Kg, propylene glycol 2Kg, ten phosphate dihydrate sodium 3Kg are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add zinc phosphate 6Kg, modification aluminium triphosphate 10Kg, ferrotitanium powder 7Kg, polyaniline 5Kg, talcum powder 10Kg, glass flake 4Kg, controlling rotating speed is 1200 turns/min, and jitter time is 12min, obtains uniform second solution; Control fineness≤70 μm of the second solution;
3) in the second solution, add flow agent 0.7Kg, defoamer 0.5Kg, deionized water 10.8Kg, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
Detect the aqueous industrial protective system that the present embodiment obtains, concrete detected result is as follows:
Stability in storage: normal temperature is placed 12 months product viscosity and become 35s from 30s, without precipitation, without layering, proves that product shelf life is greater than 12 months.Salt water resistance (5% sodium-chlor), 20 days without considerable change (GB/T9274-88), sticking power 0 grade (hundred lattice methods), salt spray resistance (3% sodium-chlor) 20 days is without considerable change (GB/1771-91), a film >=100mm, range estimation 15min not blackening.
Embodiment 3:
Be equipped with 100Kg aqueous industrial protective system, its preparation method carries out according to the following steps:
1) waterborne styrene-acrylic emulsion 32Kg, sanitas 3Kg, propylene glycol 2Kg, ten phosphate dihydrate sodium 3Kg are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add zinc phosphate 8Kg, modification aluminium triphosphate 8Kg, ferrotitanium powder 8Kg, polyaniline 7Kg, talcum powder 8Kg, glass flake 5Kg, controlling rotating speed is 1200 turns/min, and jitter time is 15min, obtains uniform second solution; Control fineness≤70 μm of the second solution;
3) the flow agent 0.7Kg added in the second solution, defoamer 0.5Kg, deionized water 14.8Kg, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
Detect the aqueous industrial protective system that the present embodiment obtains, concrete detected result is as follows:
Stability in storage: normal temperature is placed 12 months product viscosity and become 37s from 26s, without precipitation, without layering, proves that product shelf life is greater than 12 months.Salt water resistance (5% sodium-chlor), 20 days without considerable change (GB/T9274-88), sticking power 0 grade (hundred lattice methods), salt spray resistance (3% sodium-chlor) 20 days is without considerable change (GB/1771-91), a film >=100mm, range estimation 15min not blackening.
Embodiment 4:
Be equipped with 100Kg aqueous industrial protective system, its preparation method carries out according to the following steps:
1) waterborne styrene-acrylic emulsion 34Kg, sanitas 3Kg, propylene glycol 2Kg, ten phosphate dihydrate sodium 3Kg are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add zinc phosphate 10Kg, modification aluminium triphosphate 6Kg, ferrotitanium powder 9Kg, polyaniline 7Kg, talcum powder 6Kg, glass flake 6Kg, controlling rotating speed is 1200 turns/min, and jitter time is 15min, obtains uniform second solution; Control fineness≤70 μm of the second solution;
3) the flow agent 0.7Kg added in the second solution, defoamer 0.5Kg, deionized water 12.8Kg, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
Detect the aqueous industrial protective system that the present embodiment obtains, concrete detected result is as follows:
Stability in storage: normal temperature is placed 12 months product viscosity and become 35s from 28s, without precipitation, without layering, proves that product shelf life is greater than 12 months.Salt water resistance (5% sodium-chlor), 20 days without considerable change (GB/T9274-88), sticking power 0 grade (hundred lattice methods), salt spray resistance (3% sodium-chlor) 20 days is without considerable change (GB/1771-91), a film >=100mm, range estimation 15min not blackening.
Because coating rate of drying of the present invention is fast, chemical resistance good, can once thick painting be shaping, easy construction, anti-sudden strain of a muscle rust performance is good, be particularly suitable for the application of outdoor large hardware, because the material used is not containing objectionable impuritiess such as heavy metals, so coating environmental protection, also have production technique simple in addition, feature easy to use.
For a person skilled in the art, according to technical scheme described above and design, other various corresponding change and distortion can be made, and all these change and distortion all should belong within the protection domain of the claims in the present invention.
Claims (9)
1. an aqueous industrial protective system, is characterized in that, is prepared from by following composition by weight:
2. aqueous industrial protective system according to claim 1, is characterized in that, is prepared from by following composition by weight:
3. aqueous industrial protective system according to claim 1, is characterized in that: described waterborne styrene-acrylic emulsion is the model that Nanchang Ward Chemical Co., Ltd. produces is the benzene emulsion of WB-313.
4. aqueous industrial protective system according to claim 1, is characterized in that: described sanitas is HTK-30 fungicidal preservative.
5. aqueous industrial protective system according to claim 1, is characterized in that: described flow agent is the EFKA3034 flow agent of EFKA company.
6. aqueous industrial protective system according to claim 1, is characterized in that: described defoamer is tegoFoamex 1488 defoamer of German Di Gao chemical company.
7. aqueous industrial protective system according to claim 1, is characterized in that: described aluminium triphosphate is the modification aluminium triphosphate that Weihai Tian Chuan Fine Chemical Co., Ltd produces.
8. a preparation method for aqueous industrial protective system according to claim 1, is characterized in that, comprise the steps:
1) waterborne styrene-acrylic emulsion of formula ratio, sanitas, propylene glycol, ten phosphate dihydrate sodium are put into dispersion cylinder, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform first solution;
2) in the first solution, add the zinc phosphate of formula ratio, modification aluminium triphosphate, ferrotitanium powder, polyaniline, talcum powder, glass flake, controlling rotating speed is 1200 turns/min, and jitter time is 10-15min, obtains uniform second solution;
3) flow agent added in the second solution, defoamer, deionized water, controlling rotating speed is 600 turns/min, and jitter time is 5min, obtains uniform 3rd solution;
4) the 3rd solution is filtered, packs, put in storage, namely obtain aqueous industrial protective system.
9. the preparation method of aqueous industrial protective system according to claim 8, is characterized in that: fineness≤70 μm of the second described solution.
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| CN201510050488.3A CN104592821B (en) | 2015-01-31 | 2015-01-31 | A kind of aqueous industrial anticorrosive paint and preparation method thereof |
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| CN201510050488.3A CN104592821B (en) | 2015-01-31 | 2015-01-31 | A kind of aqueous industrial anticorrosive paint and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107880662A (en) * | 2017-11-20 | 2018-04-06 | 广东华兹卜新材料科技有限公司 | A kind of water soluble acrylic acid anticorrosive paint and preparation method thereof |
| CN108587340A (en) * | 2018-06-05 | 2018-09-28 | 上海鸣昂机械科技有限公司 | Special-purpose aqueous anticorrosive paint of container and preparation method thereof |
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Address after: 528400 Zhongshan Torch Development Zone, Guangdong, West Road, No. 12 Patentee after: Guangdong Huazibuxin Mstar Technology Ltd Address before: 528400 Zhongshan Torch Development Zone, Guangdong, West Road, No. 12 Patentee before: Guangdong Valspar Chemical Industry Co., Ltd. |
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Effective date of registration: 20190529 Address after: 528437 Room 202, 2nd floor, No. 12 Deneng West Road Office Building, Zhongshan Torch Development Zone, Guangdong Province (Residence Declaration) Patentee after: Zhongshan Magic Painting New Material Technology Co., Ltd. Address before: 528400 No. 12 Deneng West Road, Torch Development Zone, Zhongshan City, Guangdong Province Patentee before: Guangdong Huazibuxin Mstar Technology Ltd |