CN104568858A - Fluorescence detector - Google Patents

Fluorescence detector Download PDF

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Publication number
CN104568858A
CN104568858A CN201310474901.XA CN201310474901A CN104568858A CN 104568858 A CN104568858 A CN 104568858A CN 201310474901 A CN201310474901 A CN 201310474901A CN 104568858 A CN104568858 A CN 104568858A
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CN
China
Prior art keywords
fluorescence
interference filter
light path
signal processing
processing system
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310474901.XA
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Chinese (zh)
Inventor
陈国平
夏方方
杜成铭
陈丽庆
王霞
张梁
吴涛英
荆吉仁
夏新开
王海大
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DANYANG HENG'AN CHEMICAL TECHNOLOGY INSTITUTE Co Ltd
Original Assignee
DANYANG HENG'AN CHEMICAL TECHNOLOGY INSTITUTE Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DANYANG HENG'AN CHEMICAL TECHNOLOGY INSTITUTE Co Ltd filed Critical DANYANG HENG'AN CHEMICAL TECHNOLOGY INSTITUTE Co Ltd
Priority to CN201310474901.XA priority Critical patent/CN104568858A/en
Publication of CN104568858A publication Critical patent/CN104568858A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a fluorescence detector and relates to the optical-mechanical field. The fluorescence detector comprises a housing and internal components. The internal components contain a fluorescence excitation light-path, a fluorescence receiving light-path and a signal processing system. The housing is provided with a power switch and a receive switch. The housing is equipped with a photoscope which brings convenience for eye detection during instrument detection. The side of the photoscope, close to the internal components, is provided with a silver iodide coating which changes colors when encountering ultraviolet light so as to resist ultraviolet light and protect eyes. The fluorescence excitation light-path contains an excitation light source, an interference filter and a sample cell. The interference filter is detachable. When the interference filter is mounted, ultraviolet transition can happen, and fluorescent light is produced by excitation. When the interference filter is dismounted, the fluorescence excitation light-path can be used as an ultraviolet-visible detector. The receive switch can independently control the signal processing system. When fluorescent light cannot be seen by naked eye, there is no need to rerun the signal processing system. Thus, system operation load is reduced, and service life is prolonged.

Description

A kind of fluorescence detector
Technical field
The present invention relates to optomechanical arts, be specifically related to a kind of fluorescence detector.
Background technology
Compound is by after ultraviolet excitation, launch the light longer than excitation wavelength, be called fluorescence, fluorescence detector is a kind of detecting device that high pressure liquid chromatograph is conventional, use Ultraviolet radiation chromatographic fraction, when sample fraction has fluorescence property, can detect, fluorescence detector selectivity is high, only has response to fluorescent material, sensitivity is also high, minimum detectability can reach 10-12ug/ml, be suitable for the trace analysis of palycyclic aromatic and various fluorescent material, also can be used for detecting and not fluoresce but can fluorescigenic material after chemical reaction, in analyzing at phenols, most phenols does not fluoresce, elder generation is treated for this reason makes it become fluorescent material, then analyze, the patent No. is 201220408285.9 relate to a kind of novel fluorescence detecting instrument, comprise interpretation of result treating apparatus, image received device, Amici prism, condenser lens, mercury light source, stabilized voltage supply, object lens, determinand platform, described interpretation of result treating apparatus is connected with image received device, image received device is connected with Amici prism, also object lens are provided with below Amici prism, object lens are arranged at the top of determinand platform, Amici prism one end is also provided with condenser lens, one end of condenser lens is provided with mercury light source, mercury light source is connected with stabilized voltage supply, by the Curve guide impeller of whole device, luminoscope can be convenient for carrying out using, the utilization rate of luminoscope improves, there is extraordinary effect, by adding image received device and the design of interpretation of result treating apparatus, data image directly can receive and pass through process, avoid manual observation and occur too much error, can not intuitive judgment but fluorescence detector fluorescent effect can not be solved, data analysis task amount is large, can not the problem of multi-functional use.
Summary of the invention
The object of the present invention is to provide a kind of fluorescence detector, to solve the above-mentioned multinomial defect caused in prior art.
A kind of fluorescence detector, comprise shell and internals, described internals comprises fluorescence excitation light path, fluorescence reception light path is provided with before described fluorescence excitation light path, signal processing system is provided with before described fluorescence reception light path, described shell is provided with power switch and receiving key, described shell is provided with photoscope, described photoscope close to the inner portion member side is provided with silver iodide coating, the thickness of described silver iodide coating is 0.5-2mm, containing copper particle in described silver iodide coating, described fluorescence excitation light path comprises excitation source, interference filter and sample cell, described interference filter is detachable, interference filter is provided with before described excitation source, sample cell is provided with before described interference filter, described fluorescence reception light path and signal processing system are electrically connected with receiving key.
Preferably, described excitation source is halogen tungsten lamp and deuterium lamp.
Preferably, in described excitation source, the wavelength of exciting light is 200-760nm.
Preferably, described shell is provided with wavelength display.
Preferably, described wavelength display is other is provided with knob.
Preferably, described sample cell length and width are 1cm.
The invention has the advantages that: rational in infrastructure, easy to use, described shell is provided with photoscope, can while the detection of instrument, also convenient eyes detect, described photoscope close to the inner portion member side is provided with silver iodide coating, containing copper particle in described silver iodide coating, silver iodide coating meets ultraviolet light, there is variable color, ultraviolet can be resisted, protection eyes, copper particle can as sensitizer, increase silver iodide to ultraviolet susceptibility, described interference filter is detachable, load onto and can carry out generation ultraviolet transition, excite generation fluorescence, unload and can use as UV, visible light detector, described fluorescence reception light path and signal processing system are electrically connected with receiving key, receiving key can individual control signal disposal system, when fluorescence is can't see in visual inspection, without the need to signal processing system of reruning, reduce system cloud gray model burden, increase the service life, described excitation source is halogen tungsten lamp and deuterium lamp, can determined wavelength be 200-760nm, light source conversion is carried out at 330nm place, extend usable range, described shell is provided with wavelength display and knob, after conveniently regulating, carry out Single wavelength scanning detection.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of fluorescence detector of the present invention.
Fig. 2 is the structural representation of photoscope of the present invention.
Wherein: 1-shell, 2-internals, 3-fluorescence excitation light path, 4-fluorescence reception light path, 5-signal processing system, 6-power switch, 7-receiving key, 8-photoscope, 9-silver iodide coating, 10-copper particle, 11-excitation source, 12-interference filter, 13-sample cell, 14-halogen tungsten lamp, 15-deuterium lamp, 16-wavelength display, 17-knob.
Embodiment
The technological means realized for making the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with embodiment, setting forth the present invention further.
As depicted in figs. 1 and 2, a kind of fluorescence detector, comprise shell 1 and internals 2, described internals 2 comprises fluorescence excitation light path 3, fluorescence reception light path 4 is provided with before described fluorescence excitation light path 3, signal processing system 5 is provided with before described fluorescence reception light path 4, described shell 1 is provided with power switch 6 and receiving key 7, described shell 1 is provided with photoscope 8, can while the detection of instrument, also convenient eyes detect, described photoscope 8 close to the inner portion member side is provided with silver iodide coating 9, silver iodide coating meets ultraviolet light, there is variable color, ultraviolet can be resisted, protection eyes, the thickness of described silver iodide coating 9 is 0.5-2mm, containing copper particle 10 in described silver iodide coating 9, copper particle can as sensitizer, increase silver iodide to ultraviolet susceptibility, described fluorescence excitation light path 3 comprises excitation source 11, interference filter 12 and sample cell 13, described interference filter 12 is detachable, load onto and can carry out generation ultraviolet transition, excite generation fluorescence, unload and can use as UV, visible light detector, interference filter 12 is provided with before described excitation source 11, sample cell 13 is provided with before described interference filter 12, described fluorescence reception light path 4 and signal processing system 5 are electrically connected with receiving key 7, receiving key can individual control signal disposal system, when fluorescence is can't see in visual inspection, without the need to signal processing system of reruning, reduce system cloud gray model burden, increase the service life.
It should be noted that described excitation source 11 is halogen tungsten lamp 14 and deuterium lamp 15, carry out light source conversion at 330nm place, extend usable range, in described excitation source 11, the wavelength of exciting light is 200-760nm, includes ultraviolet-visible district, can carry out the detection of ultraviolet-visible.
And described shell 1 is provided with wavelength display 16, described wavelength display 16 is other is provided with knob 17.After conveniently regulating, carry out Single wavelength scanning detection, described sample cell 13 length and width are 1cm.
Based on above-mentioned, this fluorescence detector is rational in infrastructure, easy to use, described shell is provided with photoscope, can while the detection of instrument, also convenient eyes detect, described photoscope close to the inner portion member side is provided with silver iodide coating, containing copper particle in described silver iodide coating, silver iodide coating meets ultraviolet light, there is variable color, ultraviolet can be resisted, protection eyes, copper particle can as sensitizer, increase silver iodide to ultraviolet susceptibility, described interference filter is detachable, load onto and can carry out generation ultraviolet transition, excite generation fluorescence, unload and can use as UV, visible light detector, described fluorescence reception light path and signal processing system are electrically connected with receiving key, receiving key can individual control signal disposal system, when fluorescence is can't see in visual inspection, without the need to signal processing system of reruning, reduce system cloud gray model burden, increase the service life, described excitation source is halogen tungsten lamp and deuterium lamp, can determined wavelength be 200-760nm, light source conversion is carried out at 330nm place, extend usable range, described shell is provided with wavelength display and knob, after conveniently regulating, carry out Single wavelength scanning detection.
As known by the technical knowledge, the present invention can be realized by other the embodiment not departing from its Spirit Essence or essential feature.Therefore, above-mentioned disclosed embodiment, with regard to each side, all just illustrates, is not only.Within the scope of the present invention all or be all included in the invention being equal to the change in scope of the present invention.

Claims (6)

1. a fluorescence detector, comprise shell and internals, described internals comprises fluorescence excitation light path, fluorescence reception light path is provided with before described fluorescence excitation light path, signal processing system is provided with before described fluorescence reception light path, it is characterized in that: described shell is provided with power switch and receiving key, described shell is provided with photoscope, described photoscope close to the inner portion member side is provided with silver iodide coating, the thickness of described silver iodide coating is 0.5-2mm, containing copper particle in described silver iodide coating, described fluorescence excitation light path comprises excitation source, interference filter and sample cell, described interference filter is detachable, interference filter is provided with before described excitation source, sample cell is provided with before described interference filter, described fluorescence reception light path and signal processing system are electrically connected with receiving key.
2. a kind of fluorescence detector according to claim 1, is characterized in that: described excitation source is halogen tungsten lamp and deuterium lamp.
3. a kind of fluorescence detector according to claim 1, is characterized in that: in described excitation source, the wavelength of exciting light is 200-760nm.
4. a kind of fluorescence detector according to claim 1, is characterized in that: described shell is provided with wavelength display.
5. a kind of fluorescence detector according to claim 4, is characterized in that: described wavelength display is other is provided with knob.
6. a kind of fluorescence detector according to claim 1, is characterized in that: described sample cell length and width are 1cm.
CN201310474901.XA 2013-10-12 2013-10-12 Fluorescence detector Pending CN104568858A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310474901.XA CN104568858A (en) 2013-10-12 2013-10-12 Fluorescence detector

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310474901.XA CN104568858A (en) 2013-10-12 2013-10-12 Fluorescence detector

Publications (1)

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CN104568858A true CN104568858A (en) 2015-04-29

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017206942A1 (en) * 2016-06-02 2017-12-07 Henkel (China) Investment Co., Ltd. Portable ultraviolet excited fluorescence intensity detector
CN109870523A (en) * 2019-04-08 2019-06-11 山东悟空仪器有限公司 Light source assembly, fluorescence detector and liquid chromatographic system

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1349784A (en) * 2000-10-25 2002-05-22 李秀知 Electric welding mask
CN1566910A (en) * 2003-07-10 2005-01-19 上海复生生物工程研究所有限公司 Fluorescence detecting instrument
CN203176742U (en) * 2012-12-20 2013-09-04 上海显恒光电科技股份有限公司 Authenticating and perspective system by using electronic gun for exciting ultraviolet fluorescence light source
CN103278484A (en) * 2013-05-11 2013-09-04 徐培实 Portable fluorescent brightener detector
JP2013190211A (en) * 2012-03-12 2013-09-26 Dkk Toa Corp Fluorometric analysis apparatus
CN203587501U (en) * 2013-10-12 2014-05-07 丹阳恒安化学科技研究所有限公司 Fluorescence detector

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1349784A (en) * 2000-10-25 2002-05-22 李秀知 Electric welding mask
CN1566910A (en) * 2003-07-10 2005-01-19 上海复生生物工程研究所有限公司 Fluorescence detecting instrument
JP2013190211A (en) * 2012-03-12 2013-09-26 Dkk Toa Corp Fluorometric analysis apparatus
CN203176742U (en) * 2012-12-20 2013-09-04 上海显恒光电科技股份有限公司 Authenticating and perspective system by using electronic gun for exciting ultraviolet fluorescence light source
CN103278484A (en) * 2013-05-11 2013-09-04 徐培实 Portable fluorescent brightener detector
CN203587501U (en) * 2013-10-12 2014-05-07 丹阳恒安化学科技研究所有限公司 Fluorescence detector

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017206942A1 (en) * 2016-06-02 2017-12-07 Henkel (China) Investment Co., Ltd. Portable ultraviolet excited fluorescence intensity detector
US10718714B2 (en) 2016-06-02 2020-07-21 Henkel (China) Investment Co. Ltd. Portable ultraviolet excited fluorescence intensity detector
RU2737228C2 (en) * 2016-06-02 2020-11-26 ХЕНКЕЛЬ АГУНД Ко. КГаА Portable fluorescence intensity detector excited by ultraviolet radiation
CN109870523A (en) * 2019-04-08 2019-06-11 山东悟空仪器有限公司 Light source assembly, fluorescence detector and liquid chromatographic system

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