CN104560416A - Rap oil candle and preparation method thereof - Google Patents
Rap oil candle and preparation method thereof Download PDFInfo
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- CN104560416A CN104560416A CN201510044335.8A CN201510044335A CN104560416A CN 104560416 A CN104560416 A CN 104560416A CN 201510044335 A CN201510044335 A CN 201510044335A CN 104560416 A CN104560416 A CN 104560416A
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- Prior art keywords
- wax
- rapeseed oil
- candle
- wax liquid
- massfraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/02—Apparatus for preparation thereof
- C11C5/026—Apparatus for preparation thereof by a continuous process, e.g. by extrusion by conveying a melt together with the wick through a solidification zone
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- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a rap oil candle which is prepared from the following components in percentage by mass: 10-100% of rap oil wax and 90-0% of wax, wherein the wax is one of paraffin, stearic acid, palm stearin and vegetable oil grease; the rap oil wax comprises rap oil wax I with the melting point of 45-52 DEG C and rap oil wax II with the melting point of 53-58 DEG C; the rap oil wax I accounts for 10-50% of the rap oil wax in percentage by mass; the rap oil wax II accounts for 50-90% of the rap oil wax in percentage by mass. The invention further discloses a method for preparing the rap oil candle. The raw material, that is, the rap oil, is easy to obtain and relatively low in price, and the raw materials of the rap oil can be regenerated and circulate and are green and environment-friendly; the rap can be planted only in spare time in winter, so that the farmland for field crops is not occupied; the situation that candles can be manufactured depending on raw materials such as imported soybean wax and palm wax is avoided, the raw material initiative is held, and the use amount of the raw material paraffin can be reduced.
Description
Technical field
The present invention relates to a kind of rapeseed oil candle and preparation method thereof.
Background technology
At present, the paraffin that the manufacture raw material of candle mainly extract from oil, also has small part from plant, to refine the palm wax processed, the vegetable matters such as soya wax.The subject matter existed is: oil is non-renewable, nondegradable rare fossil energy, makees raw material making candle unreasonable to energy utilization with paraffin; Palm wax almost all needs import, needs to cut down large stretch of natural forests, destroys physical environment; Soya wax also needs a large amount of import, takies large stretch of farmland and ploughs.
Rapeseed oil from Semen Brassicae campestris, this kind of plant in China Yangtze valley or southwest, the Northwest extensively plants, can utilize plant winter slack, do not strive ground with field crop, China's output occupies first place in the world, and also has a large amount of plantation in European Union.Rapeseed oil, through point carrying or become after hydrogenation processing the rapeseed oil wax of solidification, uses that rapeseed oil is waxed makes candle, can ensure that candle raw material initiative rests in our hand, green, and environmental protection is renewable, capable of circulation, and candle raw material also can be made abundanter.Therefore, the waxed candle tool of doing of rapeseed oil is used to be of great significance.
Summary of the invention
Need to consume a large amount of paraffin, palm wax or soya wax according to the existing candlemaking of above-mentioned proposition, cause environmental pollution and take the technical problem of ploughing in large stretch of farmland, and a kind of rapeseed oil candle and preparation method thereof is provided.
The technique means that the present invention adopts is as follows:
A kind of rapeseed oil candle is the rapeseed oil wax of 10%-100% and massfraction containing massfraction is the wax of 90%-0%, and described wax is paraffin, stearic acid, the one in palm stearin and hydrogenated vegetable fat;
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C-52 DEG C and fusing point the be rapeseed oil wax two of 53 DEG C-58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%-50%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%-50%, described rapeseed oil wax one is obtained by hydrogenation technique or fractionation technology obtains, and described rapeseed oil wax two is obtained by hydrogenation technique or fractionation technology obtains.
The invention also discloses a kind of rapeseed oil candle, comprise the material of following weight part:
Rapeseed oil wax: 70-100 part,
Wax: 0-30 part,
Described wax is paraffin, stearic acid, the one in palm stearin and hydrogenated vegetable fat;
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C-47 DEG C and fusing point the be rapeseed oil wax two of 56 DEG C-58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%-50%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%-50%
Described rapeseed oil candle also comprises the auxiliary material prepared needed for candle, and described auxiliary material comprises dyestuff and spices.The quality of described dyestuff accounts for the 0%-0.2% of rapeseed oil wax and wax amount sum; The quality of described spices accounts for the 0-3% of rapeseed oil wax and wax amount sum;
In technique scheme, described rapeseed oil wax is preferably 70 parts, and described wax is preferably 30 parts, and the massfraction that preferred described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, and the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%.
Described rapeseed oil wax one is obtained by hydrogenation technique or fractionation technology obtains, and described rapeseed oil wax two is obtained by hydrogenation technique or fractionation technology obtains.
Described hydrogenation technique, i.e. the direct selectivity of rapeseed oil or extremely hydrogenation, undersaturated grease is become the semi-saturation of different melting points or fat oil Zhi rapeseed oil wax; Described fractionation technology, namely different according to the fusing point of the heterogeneity in rapeseed oil, extracted respectively by the grease of dystectic grease and low melting point, the dystectic grease obtained is exactly rapeseed oil wax.
Described paraffin is a kind of in semi-refined 54#, 56#, 58#, 60# paraffin or is the one in 54#, 56#, 58#, 60# paraffin of full refining.
Described stearic acid to be fusing point the be stearic acid of 56 DEG C-63 DEG C, described stearic molecular formula C
18h
36o
2or CH
3(CH
2)
16cOOH, described stearic molecular weight 284.48, described stearic acid has powder or the crystallisate of soapy feeling in white or off-white color.
Described palm stearin is fusing point is 44 DEG C of-50 DEG C of palm stearins, and described palm stearin is the saturated vegetable oil glyceride of unhydrogenation, in semi-solid state or solid-state, and white or off-white color mixture.
Described hydrogenated vegetable fat is fusing point is 52 DEG C of-60 DEG C of hydrogenated vegetable fats, and described hydrogenated vegetable fat is the saturated vegetable oil glyceride through over hydrogenation, in solid-state, and white or off-white powder or granular mixture.
The invention discloses a kind of method making rapeseed oil candle, there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, the recirculated cooling water that temperature is 13 DEG C-16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, the described cylindric solidification wax obtained in step S4 is positioned on base plate, described location refers to fixes described cylindric solidification wax or is placed on a certain pour point on described base plate by three locating points, described cylindric solidification wax overcoat has a cylindrical die, described mould is positioned on described base plate by three locating points, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm-10mm, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm-8mm;
Candle is made after S7, cooling.
Before step S6, described mould carried out preheating or do not carry out preheating, if described mould is carried out preheating, the temperature of described preheating is 50 DEG C-60 DEG C.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
The invention discloses the method that another makes rapeseed oil candle, there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
Candle is made after S3, cooling.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
The invention also discloses a kind of method making rapeseed oil candle, there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, is connected with the recirculated cooling water that temperature is 13 DEG C-16 DEG C in described steel round tube type rotary drum;
S3, described particulate matter are pressed into candle.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
The invention discloses a kind of method making rapeseed oil candle, there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: above-mentioned wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, the recirculated cooling water that temperature is 13 DEG C-16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, the described cylindric solidification wax obtained in step S4 is positioned on base plate, described location refers to fixes described cylindric solidification wax or is placed on a certain pour point on described base plate by three locating points, described cylindric solidification wax overcoat has a cylindrical die, described mould is positioned on described base plate by three locating points, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm-10mm, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm-8mm;
Candle is made after S7, cooling.
Before step S6, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality; Described mould carried out preheating or do not carry out preheating, if described mould is carried out preheating, the temperature of described preheating is 50 DEG C-60 DEG C.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
The invention discloses a kind of method making rapeseed oil candle, there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
Candle is made after S3, cooling.
Before step S2, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
The invention discloses a kind of method making rapeseed oil candle, there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, is connected with the recirculated cooling water that temperature is 13 DEG C-16 DEG C in described steel round tube type rotary drum;
S3, described particulate matter are pressed into candle.
Before step S2, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
Compared with prior art the present invention has the following advantages:
Rapeseed oil raw material is easy to get, and price is lower, and China is global first output big country, and the raw material of rapeseed oil is renewable, capable of circulation, environmental protection, and rapeseed oil is produced, and only in plantation in season in winter slack, will not strive ground by field crop; Avoid dependence on import soya wax, palm wax makes candle as raw material, have the initiative of raw material, and paraffin raw material usage quantity can be reduced.
The present invention extensively can promote in fields such as candles and preparation method thereof for the foregoing reasons.
Embodiment
Embodiment 1
Make a method for rapeseed oil candle, there are following steps:
S1, batching: be the rapeseed oil wax of 15% by massfraction, massfraction is that the 58# paraffin of the full refining of 85% is mixed and made into wax liquid, the temperature of described wax liquid is 65 DEG C, described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C and fusing point the be rapeseed oil wax two of 58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%, and the 58# melting point of paraffin wax of described full refining is 58 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-70 μm, the rotating speed of described steel round tube type rotary drum is 3 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, and the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum;
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, the described cylindric solidification wax obtained in step S4 is fixed on base plate by three locating points, outer wall and described three locating points of described cylindric solidification wax are tangent, described cylindric solidification wax overcoat has a cylindrical die, inwall and described three locating points of described cylindrical die are tangent, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 5mm, the material of described mould is cast iron, and described mould is carried out preheating, and the temperature of described preheating is 50 DEG C;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 8mm;
After S7, cooling, diameter is made in the demoulding is 70mm, and height is the cylindrical candle of 150mm.
The envrionment temperature making above-mentioned rapeseed oil candle is 20 DEG C.
Embodiment 2
Make a method for rapeseed oil candle, there are following steps:
S1, batching: 70 parts of rapeseed oil waxes and 30 parts of stearic acid are mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C, described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 47 DEG C and fusing point the be rapeseed oil wax two of 56 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 20%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 80%, and described stearic fusing point is 61 DEG C;
S2, powder process: above-mentioned wax liquid is made the particulate matter that diameter is 70-100 μm, a shower nozzle is delivered to by the described wax liquid pump of part, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 70-100 μm, the rotating speed of described steel round tube type rotary drum is 3 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, a certain pour point described cylindric solidification wax obtained in step S4 is placed on described base plate, described cylindric solidification wax overcoat has a cylindrical die, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 10mm, the material of described mould is glass, described mould is carried out preheating, and the temperature of described preheating is 60 DEG C;
S6, 70 parts of rapeseed oil waxes and 30 parts of stearic acid are mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C, and add milk yellow dyestuff and stir, the quality of described milk yellow dyestuff is 0.01% of the quality of described wax liquid, described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 47 DEG C and fusing point the be rapeseed oil wax two of 56 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 20%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 80%, described stearic fusing point is 61 DEG C, be injected between the inwall of described mould and the outer wall of described cylindric solidification wax afterwards, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 7mm,
Making diameter after S7, cooling is 85mm, and height is the glass cylinder container candle of 90mm.
The envrionment temperature making above-mentioned rapeseed oil candle is 25 DEG C.
Embodiment 3
Make a method for rapeseed oil candle, there are following steps:
S1, batching: be the rapeseed oil wax of 85% by massfraction, massfraction be 15% palm stearin be mixed and made into wax liquid, the temperature of described wax liquid is 65 DEG C, described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 52 DEG C and fusing point the be rapeseed oil wax two of 57 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 30%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 70%, and the fusing point of described palm stearin is 48 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 70-100 μm, the rotating speed of described steel round tube type rotary drum is 3 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter are 22mm by being crushed to diameter, and height is the bar wax of 180mm.
The envrionment temperature making described rapeseed oil candle is 20 DEG C.
Embodiment 4
Make a method for rapeseed oil candle, there are following steps:
S1, batching: be the rapeseed oil wax of 70% by massfraction, massfraction be 30% semi-refined 60# paraffin be mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C,
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C and fusing point the be rapeseed oil wax two of 58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, and the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%,
Described semi-refined 60# melting point of paraffin wax is 60 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 70-100 μm, the rotating speed of described steel round tube type rotary drum is 5 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, a certain pour point described cylindric solidification wax obtained in step S4 is placed on described base plate, described cylindric solidification wax overcoat has a cylindrical die, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm, and the material of described mould is plastics;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm;
Making diameter after S7, cooling is 37.5mm, and height is the tealight of 17mm.
The envrionment temperature making above-mentioned rapeseed oil candle is 20 DEG C.
The feature performance benefit of above-mentioned tealight is as follows:
1, residual low: residual quantity significantly reduces about 30%;
2, not fuel-displaced, do not ftracture: formula homogeneity, mutual solubility is better, and high temperature test is not fuel-displaced; High/low temperature switch test does not ftracture;
3, Color whiteness is good: the colour Lovibond R1.5 of rapeseed oil, and the palmitic colour Lovibond R3.5 of reference sample; Improve quality product, reducing costs (because without the need to adding dyestuff to brighten) simultaneously;
4, flame height, reaches like product level combustion time.
Embodiment 5
Make a method for rapeseed oil candle, there are following steps:
S1, batching: be the rapeseed oil wax of 50% by massfraction, massfraction be 50% stearic acid be mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C,
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 48 DEG C and fusing point the be rapeseed oil wax two of 53 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 20%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 80%, and described stearic fusing point is 58 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is white steel;
After S3, cooling, diameter is made in the demoulding is 70mm, and height is the cylindrical candle of 150mm.
The envrionment temperature making described rapeseed oil candle is 32 DEG C.
Embodiment 6
Make a method for rapeseed oil candle, there are following steps:
S1, batching: be the rapeseed oil wax of 30% by massfraction, massfraction be 70% hydrogenated vegetable fat be mixed and made into wax liquid, the temperature of described wax liquid is 70 DEG C,
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 52 DEG C and fusing point the be rapeseed oil wax two of 57 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 30%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 70%, and the fusing point of described hydrogenated vegetable fat is 58 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is white steel;
After S3, cooling, bottom surface one-tenth pentagram is made in the demoulding, and height is the candle of 150mm, and the outside surface of described candle is coated with multi color pattern.
The envrionment temperature making described rapeseed oil candle is 25 DEG C.
Embodiment 7
Make a method for rapeseed oil candle, there are following steps:
S1, batching: 70 parts of rapeseed oil waxes and 30 parts of semi-refined 60# paraffin are mixed and made into wax liquid, and the temperature of described wax liquid is 75 DEG C,
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C and fusing point the be rapeseed oil wax two of 58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, and the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%,
Described semi-refined 60# melting point of paraffin wax is 60 DEG C;
S2, powder process: above-mentioned wax liquid is made the particulate matter that diameter is 70-100 μm, a shower nozzle is delivered to by the described wax liquid pump of part, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 70-100 μm, the rotating speed of described steel round tube type rotary drum is 5 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, a certain pour point described cylindric solidification wax obtained in step S4 is placed on described base plate, described cylindric solidification wax overcoat has a cylindrical die, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm, and the material of described mould is plastics;
S6,70 parts of rapeseed oil waxes and 30 parts of semi-refined 60# paraffin are mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C, and adds milk yellow dyestuff and stir, and the quality of described milk yellow dyestuff is 0.01% of the quality of described wax liquid,
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C and fusing point the be rapeseed oil wax two of 58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, and the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%,
Described semi-refined 60# melting point of paraffin wax is 60 DEG C;
Be injected into afterwards between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm;
Making diameter after S7, cooling is 37.5mm, and height is the tealight of 17mm.
The envrionment temperature making above-mentioned rapeseed oil candle is 20 DEG C.
The feature performance benefit of above-mentioned tealight is as follows:
1, residual low: residual quantity significantly reduces about 30%;
2, not fuel-displaced, do not ftracture: formula homogeneity, mutual solubility is better, and high temperature test is not fuel-displaced; High/low temperature switch test does not ftracture;
3, flame height, reaches like product level combustion time.
Embodiment 8
Make a method for rapeseed oil candle, there are following steps:
S1, batching: 85 parts of rapeseed oil waxes and 15 parts of palm stearins are mixed and made into wax liquid, the temperature of described wax liquid is 65 DEG C, and add milk yellow dyestuff and stir, the quality of described milk yellow dyestuff is 0.01% of the quality of described wax liquid, described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 47 DEG C and fusing point the be rapeseed oil wax two of 57 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 30%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 70%, and the fusing point of described palm stearin is 48 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 70-100 μm, the rotating speed of described steel round tube type rotary drum is 3 revs/min, the recirculated cooling water that temperature is 16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter are 22mm by being crushed to diameter, and height is the bar wax of 180mm.
The envrionment temperature making described rapeseed oil candle is 20 DEG C.
Embodiment 9
Make a method for rapeseed oil candle, there are following steps:
S1, batching: 75 parts of rapeseed oil waxes and 25 parts of stearic acid are mixed and made into wax liquid, the temperature of described wax liquid is 75 DEG C, and add pink colour dyestuff and rose compound stirs, the quality of described pink colour dyestuff is 0.012% of the quality of described wax liquid, the quality of described rose is 3% of described wax liquid quality
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 47 DEG C and fusing point the be rapeseed oil wax two of 56 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 20%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 80%, and described stearic fusing point is 58 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is white steel;
After S3, cooling, diameter is made in the demoulding is 70mm, and height is the cylindrical candle of 150mm.
The envrionment temperature making described rapeseed oil candle is 32 DEG C.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (9)
1. a rapeseed oil candle is the rapeseed oil wax of 10%-100% and massfraction containing massfraction is the wax of 90%-0%, and described wax is paraffin, stearic acid, the one in palm stearin and hydrogenated vegetable fat;
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C-52 DEG C and fusing point the be rapeseed oil wax two of 53 DEG C-58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%-50%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%-50%, described rapeseed oil wax one is obtained by hydrogenation technique or fractionation technology obtains, and described rapeseed oil wax two is obtained by hydrogenation technique or fractionation technology obtains.
2. a rapeseed oil candle, comprises the material of following weight part:
Rapeseed oil wax: 70-100 part,
Wax: 0-30 part,
Described wax is paraffin, stearic acid, the one in palm stearin and hydrogenated vegetable fat;
Described rapeseed oil wax comprises fusing point to be the rapeseed oil wax one of 45 DEG C-47 DEG C and fusing point the be rapeseed oil wax two of 56 DEG C-58 DEG C, the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%-50%, the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%-50%
Described rapeseed oil candle also comprises the auxiliary material prepared needed for candle.
3. rapeseed oil candle according to claim 2, it is characterized in that: described rapeseed oil wax is 70 parts, described wax is 30 parts, and the massfraction that described rapeseed oil wax one accounts for described rapeseed oil wax is 10%, and the massfraction that described rapeseed oil wax two accounts for described rapeseed oil wax is 90%.
4. make a method for rapeseed oil candle according to claim 1, it is characterized in that there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, is connected with the recirculated cooling water that temperature is 13 DEG C-16 DEG C in described steel round tube type rotary drum;
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, be positioned on base plate by the described cylindric solidification wax obtained in step S4, described cylindric solidification wax overcoat has a cylindrical die, and the spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm-10mm;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm-8mm;
Candle is made after S7, cooling.
5. make a method for rapeseed oil candle according to claim 1, it is characterized in that there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould;
Candle is made after S3, cooling.
6. make a method for rapeseed oil candle according to claim 1, it is characterized in that there are following steps:
S1, batching: the wax of to be the rapeseed oil wax of 10%-100% and described massfraction by described massfraction be 90%-0% is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, is connected with the recirculated cooling water that temperature is 13 DEG C-16 DEG C in described steel round tube type rotary drum;
S3, described particulate matter are pressed into candle.
7. make a method for the rapeseed oil candle described in Claims 2 or 3, it is characterized in that there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: above-mentioned wax liquid pump is delivered to a shower nozzle, described shower nozzle comprises multiple spray orifice, the diameter of described spray orifice is 40 μm, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, the recirculated cooling water that temperature is 13 DEG C-16 DEG C is connected with in described steel round tube type rotary drum, described shower nozzle is shaft-like, described multiple spray orifice is along the axis direction word order of described shower nozzle, the axis of described shower nozzle is parallel with the turning axle of described steel round tube type rotary drum,
S3, described particulate matter make cylindric solidification wax by punching press;
S4, wax core is penetrated in described cylindric solidification wax;
S5, the described cylindric solidification wax obtained in step S4 is positioned on base plate, described location refers to fixes described cylindric solidification wax or is placed on a certain pour point on described base plate by three locating points, described cylindric solidification wax overcoat has a cylindrical die, described mould is positioned on described base plate by three locating points, spacing between the inwall of described mould and the outer wall of described cylindric solidification wax is 0.5mm-10mm, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
S6, the other part of described wax liquid obtained by S1 are injected between the inwall of described mould and the outer wall of described cylindric solidification wax, until cover on the top of described cylindric solidification wax the wax liquid layer that a thickness is 1mm-8mm;
Candle is made after S7, cooling.
Before step S6, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality; Described mould carried out preheating or do not carry out preheating, if described mould is carried out preheating, the temperature of described preheating is 50 DEG C-60 DEG C.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
8. make a method for a kind of rapeseed oil candle described in Claims 2 or 3, it is characterized in that there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, the described wax liquid obtained by S1 are injected in mould, and the material of described mould is the one in white steel, cast iron, aluminium, plastics, glass, pottery;
Candle is made after S3, cooling.
Before step S2, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
9. make a method for a kind of rapeseed oil candle described in Claims 2 or 3, it is characterized in that there are following steps:
S1, batching: each component of agreement weight proportion is mixed and made into wax liquid, and the temperature of described wax liquid is 65 DEG C-75 DEG C;
S2, powder process: described for part wax liquid pump is delivered to a shower nozzle, described wax liquid drops on the outer wall of a steel round tube type rotary drum from the spray orifice ejection of described shower nozzle, form the particulate matter that diameter is 50-100 μm, the rotating speed of described steel round tube type rotary drum is 3-5 rev/min, is connected with the recirculated cooling water that temperature is 13 DEG C-16 DEG C in described steel round tube type rotary drum;
S3, described particulate matter are pressed into candle.
Before step S2, dyestuff and spices being joined in described wax liquid and to stir, the quality of described dyestuff is the 0%-0.2% of the quality of described wax liquid; The quality of described spices is the 0-3% of described wax liquid quality.
The envrionment temperature making described rapeseed oil candle is 15 DEG C-32 DEG C.
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Cited By (3)
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| CN106867683A (en) * | 2017-03-01 | 2017-06-20 | 青岛金王应用化学股份有限公司 | A kind of cottonseed oil candle and preparation method thereof |
| CN112725095A (en) * | 2020-12-07 | 2021-04-30 | 大连达伦特工艺品有限公司 | Shea butter candle and manufacturing method thereof |
| CN115216368A (en) * | 2022-07-22 | 2022-10-21 | 大连达伦特香氛科技有限公司 | Un-peeling glass container wax based on shea butter wax and method thereof |
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| CN104774696A (en) * | 2015-03-30 | 2015-07-15 | 浙江弘茂家居有限公司 | Light transmission craft candle and manufacturing method thereof |
| CN106916632A (en) * | 2017-02-21 | 2017-07-04 | 大连达伦特工艺品有限公司 | A kind of rice bran candle and preparation method thereof |
| CN107674766A (en) * | 2017-09-28 | 2018-02-09 | 山东巧妻食品科技有限公司 | It is a kind of using cottonseed oil as edible birthday candle of primary raw material and preparation method thereof |
| US20230027101A1 (en) * | 2019-12-09 | 2023-01-26 | Aak Ab (Publ) | Wax compositions for use in candles and methods of preparing wax compositions |
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