CN104559463A - Water-based silkscreen printing ink and preparation process thereof - Google Patents
Water-based silkscreen printing ink and preparation process thereof Download PDFInfo
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- CN104559463A CN104559463A CN201310486393.7A CN201310486393A CN104559463A CN 104559463 A CN104559463 A CN 104559463A CN 201310486393 A CN201310486393 A CN 201310486393A CN 104559463 A CN104559463 A CN 104559463A
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- water
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses water-based silkscreen printing ink which comprises components in percentage by weight as follows: 50%-90% of water-based styrene acrylic resin, 0.1%-8% of a leveling agent, 0.1%-4% of a coupling agent, 1%-6% of an emulsifier, 0.2%-4% of an antifoaming agent, 0.1%-3% of a neutralizer and 1%-20% of water, wherein the water-based styrene acrylic resin is a water-based acrylic resin liquid or comprises components in percentage by weight as follows: 40%-60% of acrylic resin emulsion and 10%-30% of water-based styrene acrylic resin liquid. Compared with the prior art, the water-based silkscreen printing ink and a preparation process thereof have the following beneficial and technical effects: the water-based silkscreen printing ink adopts total water-based resin vehicle, is non-toxic, harmless and free from VOC (volatile organic compounds) pollution, and has very good adhesiveness on printing stock for printing cigarette and wine packaging and the like; patterns and texts are clear; after-tack and moistening are avoided; the printing ink is fold-resistant without ink falling, is resistant to a 75 V/V alcoholic solvent, rub-resistant and non-staining under rubbing and the like, and has excellent printing flowability and gloss especially under high-temperature and high-humidity or low-temperature and low-humidity environmental conditions.
Description
Technical field
The present invention relates to printing technology, particularly relate to a kind of water-soluble silk screen ink and manufacturing process thereof.
Background technology
The application of ink for screen printing in the industry such as packages printing and advertising is very general, traditional ink for screen printing with an organic solvent (as: toluene, dimethylbenzene, vinylbenzene, pimelinketone, different fluorine that ketone, acetic acid, ethyl ester, acetic acid, butyl ester, butanols, ethanol, butyl glycol ether, ethylene glycol ethyl ether etc.) conduct dissolves carrier or cleaning equipment, instrument.
This organic solvent not only pollutes the environment, and also can produce poisonous volatilization gas, and harm humans is healthy.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of stable, adaptive, safety, the water-soluble silk screen ink of environmental protection and manufacturing process.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of water-soluble silk screen ink, comprises the component of following weight percent: water-based styrene acrylic resin 50-90%, flow agent 0.1-8%, coupling agent 0.1-4%, emulsifying agent 1-6%, defoamer 0.2-4%, neutralizing agent 0.1-3%, water 1-20%.
Also comprise the component of following weight percent: tinting material 4-15%, weighting agent 1-10%.
Described water-based styrene acrylic resin is water-borne acrylic resin liquid, or is made up of the component of following weight percent: Emulsion acrylic resin 40-60%, water-based styrene acrylic resin liquid 10-30%.
Described water-based styrene acrylic resin liquid be Qingdao beautiful jade can Trade Co., Ltd. produce 507 resins.
Described Emulsion acrylic resin is 6756 products that Shanghai company limited of Jielong Industries Co. produces.
Described flow agent is polyether-modified dimethyl siloxane; Described coupling agent is novel chelating phosphoric acid ester titanate coupling agent; Described emulsifying agent is DOP emulsifying agent; Described defoamer is for containing anchoring based high molecular organosilicon polymer defoamer; Described neutralizing agent is 20-25% ammoniacal liquor; Described water is tap water or seawater.
Described tinting material is light-resistant pigment; Described weighting agent is light calcium carbonate.
Present invention also offers the technique manufacturing above-mentioned water-soluble silk screen ink:
A manufacturing process for water-soluble silk screen ink, comprises the steps:
A1: add neutralizing agent debugging pH value in water-based styrene acrylic resin liquid, control ph is 6.8-8.3;
B1: by low-melting ink vehicle obtained for steps A 1 and other remaining components sand mill sand milling one time or ball mill ball milling 30 hours, sampling and testing is carried out again after three-roller grinds 1 time, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
A manufacturing process for water-soluble silk screen ink, comprises the steps:
A1: add neutralizing agent debugging pH value in water-based styrene acrylic resin liquid, control ph is 6.8-8.3;
B1: by other components except Emulsion acrylic resin and the obtained low-melting ink vehicle of steps A 1 through pre-dispersed evenly after on three-roller, grind 3-5 time, make it to required fineness requirement, obtain aqueous color paste;
C1: drop into Emulsion acrylic resin in the aqueous color paste that step B1 is obtained, continue to grind on three-roller 1-2 all over after carry out sampling and testing, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
Compared with prior art, water-soluble silk screen ink of the present invention and manufacturing process thereof have following Advantageous Effects: water-soluble silk screen ink of the present invention adopts full water-base resin low-melting ink vehicle, nontoxic, harmless, VOC free pollutes, stock such as printing cigarette, Wine packaging etc. has good tack, picture and text are clear, do not after-tack, do not get damp, fold resistant does not fall ink, resistance to 75 degree of alcoholic solvents, scouring are not dyeed, especially, under high temperature, high humidity or low temperature, low moisture environments condition, excellent printing mobility and glossiness is had.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Water-soluble silk screen ink of the present invention, comprises the component of following weight percent: water-based styrene acrylic resin 50-90%, flow agent 0.1-8%, coupling agent 0.1-4%, emulsifying agent 1-6%, defoamer 0.2-4%, neutralizing agent 0.1-3%, water 1-20%.
The tinting material that water-soluble silk screen ink of the present invention can also comprise weight percent 4-15% is painted to carry out.
Water-soluble silk screen ink of the present invention can also comprise weight percent 1-10% weighting agent accelerating drying, reduce costs, Film with Preventing Adhesion.
Described water-based styrene acrylic resin is water-based styrene acrylic resin liquid, or weight percent 40-60% Emulsion acrylic resin and weight percent 10-30% water-based styrene acrylic resin liquid.
6756 products that described Emulsion acrylic resin can select Shanghai company limited of Jielong Industries Co. to produce; Described water-based styrene acrylic resin liquid can select Qingdao beautiful jade can Trade Co., Ltd. produce 507 resins; Described flow agent is polyether-modified dimethyl siloxane; Described coupling agent is novel chelating phosphoric acid ester titanate coupling agent; Described emulsifying agent is DOP emulsifying agent; Described defoamer is for containing anchoring based high molecular organosilicon polymer defoamer; Described neutralizing agent is 20-25% ammoniacal liquor; Described water is tap water or seawater; Described tinting material is light-resistant pigment; Described weighting agent is light calcium carbonate.
Embodiment one:
The water-soluble silk screen ink of the present embodiment is made up of the component of following weight percent: Emulsion acrylic resin 50%, water-based styrene acrylic resin liquid 20%, flow agent 2%, coupling agent 2%, emulsifying agent 2%, defoamer 2%, neutralizing agent 1%, water 10%, tinting material 7%, weighting agent 4%.
The manufacturing process of the water-soluble silk screen ink of the present embodiment comprises the steps:
A1: add neutralizing agent debugging pH value in water-based styrene acrylic resin liquid, control ph is 6.8-8.3;
B1: by low-melting ink vehicle obtained for steps A 1 and flow agent, coupling agent, emulsifying agent, defoamer, neutralizing agent, water, tinting material, weighting agent through pre-dispersed evenly after on three-roller, grind 3-5 time, make it arrive required fineness requirement, obtain aqueous color paste;
C1: drop into Emulsion acrylic resin in the aqueous color paste that step B1 is obtained, continue to grind on three-roller 1-2 all over after carry out sampling and testing, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
Embodiment two:
The water-soluble silk screen ink of the present embodiment is made up of the component of following weight percent: Emulsion acrylic resin 25%, water-based styrene acrylic resin liquid 45%, flow agent 1.5%, coupling agent 2.5%, emulsifying agent 3%, defoamer 1%, neutralizing agent 1%, water 11%, tinting material 9%, weighting agent 1%.
The manufacturing process of the water-soluble silk screen ink of the present embodiment is identical with embodiment one.
Embodiment three:
The water-soluble silk screen ink of the present embodiment is made up of the component of following weight percent: water-based styrene acrylic resin liquid 66%, flow agent 3%, coupling agent 4%, emulsifying agent 3.5%, defoamer 0.5%, neutralizing agent 0.5%, water 17.7%, tinting material 4.5%, weighting agent 0.3%.
The manufacturing process of the water-soluble silk screen ink of the present embodiment comprises the steps:
A1: add neutralizing agent debugging pH value in water-based styrene acrylic resin liquid, control ph is 6.8-8.3;
B1: the low-melting ink vehicle obtained by steps A 1 and flow agent, coupling agent, emulsifying agent, defoamer, neutralizing agent, water, tinting material, weighting agent are sand mill sand milling one time or ball mill ball milling 30 hours, sampling and testing is carried out again after three-roller grinds 1 time, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
According to contents such as China national examination criteria GB/T14624.1, the test event of water-soluble silk screen ink of the present invention please see the following form:
Above-described embodiment is the preferred embodiment for the present invention, and its principles all are identical with the present embodiment or approximate with basic structure, all within scope.
Claims (10)
1. a water-soluble silk screen ink, is characterized in that, comprises the component of following weight percent: water-based styrene acrylic resin 50-90%, flow agent 0.1-8%, coupling agent 0.1-4%, emulsifying agent 1-6%, defoamer 0.2-4%, neutralizing agent 0.1-3%, water 1-20%.
2. water-soluble silk screen ink according to claim 1, is characterized in that, also comprises the component of following weight percent: tinting material 4-15%, weighting agent 1-10%.
3. water-soluble silk screen ink according to claim 1, is characterized in that: described water-based styrene acrylic resin is water-based styrene acrylic resin liquid.
4. water-soluble silk screen ink according to claim 1, is characterized in that: described water-borne acrylic resin is made up of the component of following weight percent: Emulsion acrylic resin 40-60%, water-based styrene acrylic resin liquid 10-30%.
5. the water-soluble silk screen ink according to claim 3 or 4, is characterized in that: described water-borne acrylic resin liquid be Qingdao beautiful jade can Trade Co., Ltd. produce 507 resins.
6. water-soluble silk screen ink according to claim 4, is characterized in that: described Emulsion acrylic resin is 6756 products that Shanghai company limited of Jielong Industries Co. produces.
7. water-soluble silk screen ink according to claim 1, is characterized in that: described flow agent is polyether-modified dimethyl siloxane; Described coupling agent is novel chelating phosphoric acid ester titanate coupling agent; Described emulsifying agent is DOP emulsifying agent; Described defoamer is for containing anchoring based high molecular organosilicon polymer defoamer; Described neutralizing agent is 20-25% ammoniacal liquor; Described water is tap water or seawater.
8. water-soluble silk screen ink according to claim 2, is characterized in that: described tinting material is light-resistant pigment; Described weighting agent is light calcium carbonate.
9. a manufacturing process for water-soluble silk screen ink as claimed in claim 3, is characterized in that, comprises the steps:
A1: add neutralizing agent debugging pH value in water-borne acrylic resin liquid, control ph is 6.8-8.3;
B1: by low-melting ink vehicle obtained for steps A 1 and other remaining components sand mill sand milling one time or ball mill ball milling 30 hours, sampling and testing is carried out again after three-roller grinds 1 time, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
10. a manufacturing process for water-soluble silk screen ink as claimed in claim 4, is characterized in that, comprises the steps:
A1: add neutralizing agent debugging pH value in water-borne acrylic resin liquid, control ph is 6.8-8.3;
B1: by other components except Emulsion acrylic resin and the obtained low-melting ink vehicle of steps A 1 through pre-dispersed evenly after on three-roller, grind 3-5 time, make it to required fineness requirement, obtain aqueous color paste;
C1: drop into Emulsion acrylic resin in the aqueous color paste that step B1 is obtained, continue to grind on three-roller 1-2 all over after carry out sampling and testing, when test result all reaches existing solvent-borne type ink for screen printing standard, get final product discharging, filtration, packaging obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310486393.7A CN104559463A (en) | 2013-10-16 | 2013-10-16 | Water-based silkscreen printing ink and preparation process thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310486393.7A CN104559463A (en) | 2013-10-16 | 2013-10-16 | Water-based silkscreen printing ink and preparation process thereof |
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| CN104559463A true CN104559463A (en) | 2015-04-29 |
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| CN201310486393.7A Pending CN104559463A (en) | 2013-10-16 | 2013-10-16 | Water-based silkscreen printing ink and preparation process thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106752359A (en) * | 2017-01-09 | 2017-05-31 | 新丰也乐化学工业制造有限公司 | A kind of silk-screen environmental protection watercolor ink and preparation method thereof |
| CN109401431A (en) * | 2018-10-30 | 2019-03-01 | 惠州市嘉淇涂料有限公司 | A kind of aluminum-pinch silk-screen water-based ink |
| CN114806271A (en) * | 2022-05-20 | 2022-07-29 | 朗升柯式印刷(深圳)有限公司 | Environment-friendly printing ink and preparation method thereof |
| CN114806286A (en) * | 2022-05-27 | 2022-07-29 | 深圳市安力环保科技有限公司 | High-performance super-dispersion resin liquid and preparation method thereof |
| CN115521659A (en) * | 2022-10-26 | 2022-12-27 | 贵州省仁怀市申仁包装印务有限责任公司 | Environment-friendly highlight printing inking process of carton printing equipment |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| EP1108756A2 (en) * | 1999-12-14 | 2001-06-20 | Seiko Epson Corporation | Ink for ink jet recording |
| WO2007137292A2 (en) * | 2006-05-23 | 2007-11-29 | Evident Technologies, Inc. | Quantum dot fluorescent inks |
| CN101125976A (en) * | 2006-08-15 | 2008-02-20 | 东莞市英科水墨有限公司 | Water silk screen painting ink and preparing method thereof |
| CN101134864A (en) * | 2007-10-15 | 2008-03-05 | 山西精华科工贸有限公司 | Cigarette label high-speed intaglio printing water-based ink |
| CN102352151A (en) * | 2011-08-24 | 2012-02-15 | 哈尔滨大东方卷烟材料科技开发有限责任公司 | Water-based ink for plastic printing and preparation method thereof |
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2013
- 2013-10-16 CN CN201310486393.7A patent/CN104559463A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1108756A2 (en) * | 1999-12-14 | 2001-06-20 | Seiko Epson Corporation | Ink for ink jet recording |
| WO2007137292A2 (en) * | 2006-05-23 | 2007-11-29 | Evident Technologies, Inc. | Quantum dot fluorescent inks |
| CN101125976A (en) * | 2006-08-15 | 2008-02-20 | 东莞市英科水墨有限公司 | Water silk screen painting ink and preparing method thereof |
| CN101134864A (en) * | 2007-10-15 | 2008-03-05 | 山西精华科工贸有限公司 | Cigarette label high-speed intaglio printing water-based ink |
| CN102352151A (en) * | 2011-08-24 | 2012-02-15 | 哈尔滨大东方卷烟材料科技开发有限责任公司 | Water-based ink for plastic printing and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106752359A (en) * | 2017-01-09 | 2017-05-31 | 新丰也乐化学工业制造有限公司 | A kind of silk-screen environmental protection watercolor ink and preparation method thereof |
| CN109401431A (en) * | 2018-10-30 | 2019-03-01 | 惠州市嘉淇涂料有限公司 | A kind of aluminum-pinch silk-screen water-based ink |
| CN114806271A (en) * | 2022-05-20 | 2022-07-29 | 朗升柯式印刷(深圳)有限公司 | Environment-friendly printing ink and preparation method thereof |
| CN114806286A (en) * | 2022-05-27 | 2022-07-29 | 深圳市安力环保科技有限公司 | High-performance super-dispersion resin liquid and preparation method thereof |
| CN115521659A (en) * | 2022-10-26 | 2022-12-27 | 贵州省仁怀市申仁包装印务有限责任公司 | Environment-friendly highlight printing inking process of carton printing equipment |
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Application publication date: 20150429 |
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