CN104532271A - Preparation method of efficient industrial metal cleaning agent - Google Patents
Preparation method of efficient industrial metal cleaning agent Download PDFInfo
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- CN104532271A CN104532271A CN201410700075.0A CN201410700075A CN104532271A CN 104532271 A CN104532271 A CN 104532271A CN 201410700075 A CN201410700075 A CN 201410700075A CN 104532271 A CN104532271 A CN 104532271A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
- C23G1/04—Cleaning or pickling metallic material with solutions or molten salts with acid solutions using inhibitors
- C23G1/06—Cleaning or pickling metallic material with solutions or molten salts with acid solutions using inhibitors organic inhibitors
- C23G1/063—Cleaning or pickling metallic material with solutions or molten salts with acid solutions using inhibitors organic inhibitors heterocyclic compounds
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
The invention provides a preparation method of an efficient industrial metal cleaning agent. The synergistic effect of components makes the cleaning agent have best cleaning and rust inhibiting effects and form a hydrophobic protection film on the surface of a cleaned metal to main the cleaned metal, so the cleaned metal has a rust inhibition property within a period of time; the cooperation with the rust inhibitor improves the rust inhibition performance of the metal; and the cleaning agent is clean and has no impurities, so the quality of the cleaning agent is improved, and the cleaning agent is safe to use, and effectively guarantees the glossiness of the metal.
Description
Technical field
The present invention relates to clean-out system field, particularly a kind of preparation method of efficient Industrial Metal clean-out system.
Background technology
In the production process of most industrial manufacturing industry, the cleaning of metallic element is the critical process affecting quality product, along with the maturation of industrial automation, the automatization of cleaning requires more and more higher, cleaning efficiency and observable index also require more and more higher, cleaning showers applies more and more extensive, conventional clean-out system in industry cleaning link cannot meet the cleaning requirement of present market metallic element.
Summary of the invention
For the problems referred to above, the present invention proposes a kind of preparation method of efficient Industrial Metal clean-out system.
For solving above technical problem, technical scheme provided by the invention is:
A preparation method for efficient Industrial Metal clean-out system, is characterized in that, described preparation method is as follows:
(1) by weight mark to take starting material as follows:
Metal inhibitor 25-36 parts, washing assistant 15-17 parts, metal antirusting agent 13-15 part, trolamine 8-12 parts, Starso 5-7 parts, Sunmorl N 60S 10-15 parts, alkylphenol polyoxy ether 7-12 parts and hydrochloric acid 3-4 part;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out trolamine, Starso, Sunmorl N 60S and alkylphenol polyoxy ether by weight, and all pour in mixing machine and mix, mixing time is 5-10 minute, obtains compound A;
(4) stir: compound A and metal inhibitor, washing assistant, metal antirusting agent and hydrochloric acid are stirred by stirrer, churning time is 25-30 minute, obtains mixed liquid B;
(5) distill: mixed liquid B is put into vaporizer, revolution distillation 20 minutes, extracts supernatant liquor B;
(6) centrifugal: supernatant liquor B to be put into filtering centrifuge and carries out centrifugal under 1800r/s, the time is 10 minutes, finally obtains scavenging solution.
The preparation method of above-mentioned a kind of efficient Industrial Metal clean-out system, wherein, described metal inhibitor is that ethyl benzotriazole and hexamethylenetetramine mix in the ratio of 1-1.5:1.3-1.6.
The preparation method of above-mentioned a kind of efficient Industrial Metal clean-out system, wherein, described washing assistant is sodium hydroxide.
The preparation method of above-mentioned a kind of efficient Industrial Metal clean-out system, wherein, described hydrochloric acid is technical hydrochloric acid.
The preparation method of above-mentioned a kind of efficient Industrial Metal clean-out system, wherein, described Starso is anhydrous sodium metasilicate.
The preparation method of above-mentioned a kind of efficient Industrial Metal clean-out system, wherein, described metal antirusting agent is tertiary sodium phosphate.
Beneficial effect of the present invention is:
The preparation method of a kind of efficient Industrial Metal clean-out system provided by the invention; by the synergy of each component; cleaning and rust-proof effect is made all to reach best; hydrophobic protective membrane can formed by the metallic surface cleaned simultaneously; the metal of curing quilt cleaning; and make, by metal at one end time of cleaning, be there is rust-proofing character; coordinate funcitonal rust-proof agent; the rust-resisting property of metal can be promoted; the clean inclusion-free of clean-out system; improve the quality of clean-out system, and use safety, and effectively can ensure the glossiness of metal.
Embodiment
Embodiment one
A preparation method for efficient Industrial Metal clean-out system, described preparation method is as follows:
(1) by weight mark to take starting material as follows:
Metal inhibitor 30 parts, washing assistant 16 parts, metal antirusting agent 14 parts, trolamine 10 parts, Starso 6 parts, Sunmorl N 60S 10 parts, alkylphenol polyoxy ether 9 parts and hydrochloric acid 4 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out trolamine, Starso, Sunmorl N 60S and alkylphenol polyoxy ether by weight, and all pour in mixing machine and mix, mixing time is 7 minutes, obtains compound A;
(4) stir: compound A and metal inhibitor, washing assistant, metal antirusting agent and hydrochloric acid are stirred by stirrer, churning time is 25 minutes, obtains mixed liquid B;
(5) distill: mixed liquid B is put into vaporizer, revolution distillation 20 minutes, extracts supernatant liquor B;
(6) centrifugal: supernatant liquor B to be put into filtering centrifuge and carries out centrifugal under 1800r/s, the time is 10 minutes, finally obtains scavenging solution.
Wherein, described metal inhibitor is that ethyl benzotriazole and hexamethylenetetramine mix in the ratio of 1:1.6, and described washing assistant is sodium hydroxide, and described hydrochloric acid is technical hydrochloric acid, described Starso is anhydrous sodium metasilicate, and described metal antirusting agent is tertiary sodium phosphate.
Embodiment two
A preparation method for efficient Industrial Metal clean-out system, described preparation method is as follows:
(1) by weight mark to take starting material as follows:
Metal inhibitor 31 parts, washing assistant 17 parts, metal antirusting agent 15 parts, trolamine 8 parts, Starso 7 parts, Sunmorl N 60S 13 parts, alkylphenol polyoxy ether 9 parts and hydrochloric acid 3 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out trolamine, Starso, Sunmorl N 60S and alkylphenol polyoxy ether by weight, and all pour in mixing machine and mix, mixing time is 8 minutes, obtains compound A;
(4) stir: compound A and metal inhibitor, washing assistant, metal antirusting agent and hydrochloric acid are stirred by stirrer, churning time is 28 minutes, obtains mixed liquid B;
(5) distill: mixed liquid B is put into vaporizer, revolution distillation 20 minutes, extracts supernatant liquor B;
(6) centrifugal: supernatant liquor B to be put into filtering centrifuge and carries out centrifugal under 1800r/s, the time is 10 minutes, finally obtains scavenging solution.
Wherein, described metal inhibitor is that ethyl benzotriazole and hexamethylenetetramine mix in the ratio of 1.3:1.5, and described washing assistant is sodium hydroxide, and described hydrochloric acid is technical hydrochloric acid, described Starso is anhydrous sodium metasilicate, and described metal antirusting agent is tertiary sodium phosphate.
Embodiment three
A preparation method for efficient Industrial Metal clean-out system, described preparation method is as follows:
(1) by weight mark to take starting material as follows:
Metal inhibitor 25 parts, washing assistant 17 parts, metal antirusting agent 15 parts, trolamine 12 parts, Starso 7 parts, Sunmorl N 60S 15 parts, alkylphenol polyoxy ether 9 parts and hydrochloric acid 4 parts;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out trolamine, Starso, Sunmorl N 60S and alkylphenol polyoxy ether by weight, and all pour in mixing machine and mix, mixing time is 10 minutes, obtains compound A;
(4) stir: compound A and metal inhibitor, washing assistant, metal antirusting agent and hydrochloric acid are stirred by stirrer, churning time is 26 minutes, obtains mixed liquid B;
(5) distill: mixed liquid B is put into vaporizer, revolution distillation 20 minutes, extracts supernatant liquor B;
(6) centrifugal: supernatant liquor B to be put into filtering centrifuge and carries out centrifugal under 1800r/s, the time is 10 minutes, finally obtains scavenging solution.
Wherein, described metal inhibitor is that ethyl benzotriazole and hexamethylenetetramine mix in the ratio of 1.5:1.6, and described washing assistant is sodium hydroxide, and described hydrochloric acid is technical hydrochloric acid, described Starso is anhydrous sodium metasilicate, and described metal antirusting agent is tertiary sodium phosphate.
A kind of preparation method of efficient Industrial Metal clean-out system; by the synergy of each component, make cleaning and rust-proof effect all reach best, hydrophobic protective membrane can formed by the metallic surface cleaned simultaneously; the metal of curing quilt cleaning; and make, by metal at one end time of cleaning, be there is rust-proofing character, coordinate funcitonal rust-proof agent, the rust-resisting property of metal can be promoted; the clean inclusion-free of clean-out system; improve the quality of clean-out system, and use safety, and effectively can ensure the glossiness of metal.
The above; be only the present invention's preferably embodiment, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.
Claims (6)
1. a preparation method for efficient Industrial Metal clean-out system, is characterized in that, described preparation method is as follows:
(1) by weight mark to take starting material as follows:
Metal inhibitor 25-36 parts, washing assistant 15-17 parts, metal antirusting agent 13-15 part, trolamine 8-12 parts, Starso 5-7 parts, Sunmorl N 60S 10-15 parts, alkylphenol polyoxy ether 7-12 parts and hydrochloric acid 3-4 part;
(2) screen: respectively each solid material is screened by vibratory screening apparatus;
(3) mix: take out trolamine, Starso, Sunmorl N 60S and alkylphenol polyoxy ether by weight, and all pour in mixing machine and mix, mixing time is 5-10 minute, obtains compound A;
(4) stir: compound A and metal inhibitor, washing assistant, metal antirusting agent and hydrochloric acid are stirred by stirrer, churning time is 25-30 minute, obtains mixed liquid B;
(5) distill: mixed liquid B is put into vaporizer, revolution distillation 20 minutes, extracts supernatant liquor B;
(6) centrifugal: supernatant liquor B to be put into filtering centrifuge and carries out centrifugal under 1800r/s, the time is 10 minutes, finally obtains scavenging solution.
2. the preparation method of a kind of efficient Industrial Metal clean-out system as claimed in claim 1, is characterized in that, described metal inhibitor is that ethyl benzotriazole and hexamethylenetetramine mix in the ratio of 1-1.5:1.3-1.6.
3. the preparation method of a kind of efficient Industrial Metal clean-out system as claimed in claim 1, it is characterized in that, described washing assistant is sodium hydroxide.
4. the preparation method of a kind of efficient Industrial Metal clean-out system as claimed in claim 1, it is characterized in that, described hydrochloric acid is technical hydrochloric acid.
5. the preparation method of a kind of efficient Industrial Metal clean-out system as claimed in claim 1, it is characterized in that, described Starso is anhydrous sodium metasilicate.
6. the preparation method of a kind of efficient Industrial Metal clean-out system as claimed in claim 1, it is characterized in that, described metal antirusting agent is tertiary sodium phosphate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410700075.0A CN104532271A (en) | 2014-11-28 | 2014-11-28 | Preparation method of efficient industrial metal cleaning agent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410700075.0A CN104532271A (en) | 2014-11-28 | 2014-11-28 | Preparation method of efficient industrial metal cleaning agent |
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| CN104532271A true CN104532271A (en) | 2015-04-22 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104929293A (en) * | 2015-06-03 | 2015-09-23 | 安徽鸿路钢结构(集团)股份有限公司 | Treatment method of galvanized bottom plate of floor support plate of steel bar truss |
| CN106868515A (en) * | 2017-01-23 | 2017-06-20 | 麻城天安化工股份有限公司 | A kind of metal surface activation agent and preparation method thereof |
| CN107460488A (en) * | 2017-07-12 | 2017-12-12 | 宁波科星材料科技有限公司 | A kind of SmCo magnetic material cleaning fluid and cleaning method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5902415A (en) * | 1996-04-02 | 1999-05-11 | Church & Dwight Co., Inc. | Aqueous sodium salt metal cleaner and method of using same |
| CN102242369A (en) * | 2011-07-05 | 2011-11-16 | 白马轴承技术(洛阳)有限公司 | Metal bearing water-based cleaning agent and preparation method and application thereof |
| CN103290421A (en) * | 2013-06-19 | 2013-09-11 | 武汉钢铁(集团)公司 | Cleaning agent for treating steel plate after annealing and before tin plating |
| CN103757651A (en) * | 2013-12-20 | 2014-04-30 | 栾晓健 | Preparation method of industrial steel plate cleaning agent |
-
2014
- 2014-11-28 CN CN201410700075.0A patent/CN104532271A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5902415A (en) * | 1996-04-02 | 1999-05-11 | Church & Dwight Co., Inc. | Aqueous sodium salt metal cleaner and method of using same |
| CN102242369A (en) * | 2011-07-05 | 2011-11-16 | 白马轴承技术(洛阳)有限公司 | Metal bearing water-based cleaning agent and preparation method and application thereof |
| CN103290421A (en) * | 2013-06-19 | 2013-09-11 | 武汉钢铁(集团)公司 | Cleaning agent for treating steel plate after annealing and before tin plating |
| CN103757651A (en) * | 2013-12-20 | 2014-04-30 | 栾晓健 | Preparation method of industrial steel plate cleaning agent |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104929293A (en) * | 2015-06-03 | 2015-09-23 | 安徽鸿路钢结构(集团)股份有限公司 | Treatment method of galvanized bottom plate of floor support plate of steel bar truss |
| CN106868515A (en) * | 2017-01-23 | 2017-06-20 | 麻城天安化工股份有限公司 | A kind of metal surface activation agent and preparation method thereof |
| CN107460488A (en) * | 2017-07-12 | 2017-12-12 | 宁波科星材料科技有限公司 | A kind of SmCo magnetic material cleaning fluid and cleaning method |
| CN107460488B (en) * | 2017-07-12 | 2019-03-01 | 宁波科星材料科技有限公司 | A kind of SmCo magnetic material cleaning solution and cleaning method |
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Application publication date: 20150422 |
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