CN104525016A - Stirring device for gas-liquid mixing reactor - Google Patents

Stirring device for gas-liquid mixing reactor Download PDF

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Publication number
CN104525016A
CN104525016A CN201410816085.0A CN201410816085A CN104525016A CN 104525016 A CN104525016 A CN 104525016A CN 201410816085 A CN201410816085 A CN 201410816085A CN 104525016 A CN104525016 A CN 104525016A
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China
Prior art keywords
gas
hollow shaft
liquid mixed
stirring
agitating device
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CN201410816085.0A
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Chinese (zh)
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CN104525016B (en
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易苗
尹新
杨江宇
义贤富
武长安
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Zhejiang Jitai New Material Co., Ltd
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ZHEJIANG LINJIANG CHEMICAL Co Ltd
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Abstract

The invention discloses a stirring device for a gas-liquid mixing reactor. The stirring device for the gas-liquid mixing reactor comprises a support seat, wherein stirring paddles and a motor for driving the stirring paddles are installed on the support seat, each stirring paddle comprises a hollow shaft rotatably installed on the support seat, and a plurality of air vents are formed in the hollow shaft; the stirring device further comprises a belt wheel fixed at the top of the hollow shaft and linked with a motor, a pipeline rotary joint installed at the top end of the hollow shaft and communicated with the interior of the hollow shaft, and a plurality of stirring fins fixed on the outer wall of the hollow shaft. According to the stirring device for the gas-liquid mixing reactor disclosed by the invention, during stirring, the stirring paddles release air and generate air bubbles, large air bubbles are crushed into small air bubbles under the beating of the stirring fins, the small air bubbles easily stay in a liquid for further gas-liquid mixing, and the small air bubbles can easily diffuse to various parts under the action of the stirring fins.

Description

A kind of agitating device for gas-liquid mixed reactor
Technical field
The present invention relates to field of chemical equipment, particularly relate to a kind of agitating device for gas-liquid mixed reactor.
Background technology
When chemical field carries out material reaction, often relate to mixing of materials, usually by stirring, material is fully mixed, the uniform mixture of height of formation.
In the prior art, for the solution polymerization process preparing rare-earth isoprene rubber, conventional raw material pre-compounding process many employings static mixer carries out.But because static mixer exists fluid stagnation district usually in exit, therefore the velocity flow profile of material is uneven, and disturbance effect is poor, causes mixed effect not ideal enough.
At present, usually also adopt the stirring autoclave blender of structure relative complex as raw material premixed device.Wherein, under the effect of paddle, the turbulent extent of material strengthens, and causes mixed effect to be strengthened.But the characteristic due to paddle causes the Flow Field Distribution in still uneven, and easily there is the larger mixing dead band of volume, cause final mixed effect also not ideal enough.In addition, the structural design of stirred tank is the key factor affecting premixing effect.In pre-compounding process, both required catalyst high uniformity dispersion in material system, required again that the upper and lower mixing in whole stirred tank was even as much as possible.Traditional stirred tank often can not reach this requirement.
Also having is together in series static mixer and stirred tank carries out the premixing process of raw material premix.Publication number is that the Chinese patent literature of CN201415984Y discloses a kind of premixing device for rare-earth isoprene rubber production, comprising the pipeline super mixer be in series and premix still.Before entering polymeric kettle, polymerisation material carries out premix in this pre-mixing apparatus, the microcosmic Homogeneous phase mixing of height can be reached, thus improve the catalytic efficiency of catalyst, decrease the degree of branching of product, make the distribution of molecular weight more even, finally improve the product quality of isoprene rubber.But the shortcoming of this pre-mixing apparatus is, the mean residence time of material in premix still is longer, and then after the polymerization reaction kettle reaction of multiple stage series connection, final conversion ratio can only reach 85-90wt%.
Existing gas-liquid mixed arranges air inlet at reactor bottom usually, and carries out constantly stirring to accelerate gas-liquid mixed to reactant with agitator, but bubble is also unmixed in a large number has just risen to liquid surface, and mixed effect is poor.
Summary of the invention
The invention provides a kind of agitating device for gas-liquid mixed reactor, gas-liquid mixed evenly.
Technical scheme of the present invention is: a kind of agitating device for gas-liquid mixed reactor, comprises bearing, and this bearing is provided with paddle and drives the motor of described paddle, described paddle comprises:
Be rotatably installed in the hollow shaft on bearing, this hollow shaft is provided with some ventholes;
Be fixed on hollow shaft top and with the belt pulley of motor linkage;
Be arranged on hollow shaft top and the pipeline swivel joint be communicated with hollow shaft inside;
Be fixed on the multiple agitating fins on hollow shaft outer wall.
Agitating device for gas-liquid mixed reactor of the present invention, can gas-liquid mixed be made evenly.Described paddle is provided with venthole and agitating fins simultaneously, gas forms bubble in a liquid after venthole is discharged, and be namely stirred fin when bubble has just started to rise to smash and become minute bubbles, minute bubbles easily stay and are absorbed in a liquid, and under the effect of centrifugal force and liquid flow, minute bubbles are also easy to edge-diffusion.
As preferably, described hollow shaft comprises:
Through bearing and the house steward be rotatably assorted with bearing, described belt pulley and pipeline swivel joint are installed on this house steward;
Access house steward in parallel, and to be parallel to each other at least two axial arms arranged with house steward, described venthole is positioned on axial arm;
Be fixedly connected on the stiffener of all axial arm bottoms.
Axial arm is fixed on supervisor bottom, and under High Rotation Speed, loosening easily appears in the connecting portion of axial arm and supervisor, and affect the service life of agitator further, all axial arms are fixed together by described stiffener, make whole paddle more stable.
Preferably axially the quantity of arm is 4 ~ 6 further.
As preferably, the axis of described agitating fins arm is vertically uniformly distributed.
Described agitating fins is for agitated liquid on the one hand, is smash bubble on the other hand, gas is mixed with liquid evenly.The described agitating fins vertically axis of arm is uniformly distributed and can ensures that the liquid at each position around axial arm all obtains uniform stirring.
As preferably, described agitating fins is projected as ellipse along its thickness direction.
Described venthole matches with agitating fins.
As preferably, the axis of described venthole arm is vertically uniformly distributed.
Described venthole vertically arm axial distribution is more conducive to gas-liquid mixed.
As preferably, described venthole quantity and each venthole corresponding with agitating fins is positioned at below corresponding agitating fins.
As preferably, the radially projecting of described venthole arm is vertically triangle, and this leg-of-mutton summit is towards stiffener.
As preferably, described rest base is fixed with beam.
During machine operation, vibration is comparatively large, and agitator also can produce larger vibration when rotating in addition.Described beam is for reducing the noise produced by vibration.
Agitating device for gas-liquid mixed reactor of the present invention, while stirring, paddle can be vented outward and produce bubble in liquid around, and under the beating of agitating fins, air pocket is ground into minute bubbles, and minute bubbles more easily stop and are mixed into a step for gas-liquid in a liquid and react.
Accompanying drawing explanation
Fig. 1 is the side schematic view of the agitating device for gas-liquid mixed reactor of the present invention.
Fig. 2 is the top view of the agitating device for gas-liquid mixed reactor of the present invention.
Detailed description of the invention
Illustrate according to the specific embodiment of the present invention below in conjunction with accompanying drawing.
Set forth a lot of detail in the following description so that fully understand the present invention, but the present invention can also adopt other to be different from other modes described here and implement, and therefore, the present invention is not limited to the restriction of following public specific embodiment.
As depicted in figs. 1 and 2, a kind of agitating device for gas-liquid mixed reactor, comprises bearing 1, motor 2 and paddle 3.
Bearing 1 is one piece of fixed head, and motor 2 to be fixed on fixed head and to make its rotating shaft perpendicular to fixed head.The rotating shaft of motor 2 is fixed with driving wheel 21.
Paddle 3 comprises a house steward 31 and is connected to the multiple axial arm 32 of house steward 31 bottom, and is fixed on the agitating fins 33 of axial arm 32 outer wall.All axial arm 32 parallel connection access house stewards 31, all axial arms 32 are all parallel to each other with house steward 31 and arrange, axial arm 32 is uniformly distributed along the circumference of paddle 3.
House steward 31 passes fixed head and is rotatably installed on fixed head by bearing 4, house steward 31 is fixed with belt pulley 34, and belt pulley 34 is linked by belt 35 and driving wheel 21.The top of house steward 31 is provided with pipeline swivel joint 5.Pipeline swivel joint 5 is connected with air inlet pipe 6, air inlet pipe 6 is communicated with outside feeder.Pipeline swivel joint 5 is prior art, can to realize while two pipelines rotate mutually can also between two pipelines convey materials.
Paddle 3 is when rotating, and due to centrifugal action, axial arm 32 easily rocks.In order to increase the stability of each axial arm 32, being provided with one piece of stiffener 7 in the bottom of axial arm 32 and all axial arms 32 are fixed together, leave certain intervals between each axial arm 32 and be parallel to each other.
Agitating fins 33 is that axis that is multiple and arm 32 vertically is uniformly distributed.Agitating fins 33 is projected as ellipse along its thickness direction.
The sidewall of axial arm 32 has multiple venthole 36, and the axis of venthole 36 arm 32 is vertically uniformly distributed.The quantity of venthole 36 is corresponding with agitating fins 33, and each venthole 36 is positioned at the below of agitating fins 33.Such arrangement is conducive to agitating fins 33 and impacts into minute bubbles by from venthole 36 bubble out, is conducive to gas-liquid mixed.
The radially projecting of venthole 36 arm is vertically triangle, and this leg-of-mutton summit is towards stiffener 7.The bottom of bearing 1 is fixed with beam 8, and beam 8 is annular, for reducing the noise produced by vibration.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (8)

1. for an agitating device for gas-liquid mixed reactor, comprise bearing, this bearing is provided with paddle and drives the motor of described paddle, it is characterized in that, described paddle comprises:
Be rotatably installed in the hollow shaft on bearing, this hollow shaft is provided with some ventholes;
Be fixed on hollow shaft top and with the belt pulley of motor linkage;
Be arranged on hollow shaft top and the pipeline swivel joint be communicated with hollow shaft inside;
Be fixed on the multiple agitating fins on hollow shaft outer wall.
2., as claimed in claim 1 for the agitating device of gas-liquid mixed reactor, it is characterized in that, described hollow shaft comprises:
Through bearing and the house steward be rotatably assorted with bearing, described belt pulley and pipeline swivel joint are installed on this house steward;
Access house steward in parallel, and to be parallel to each other at least two axial arms arranged with house steward, described venthole is positioned on axial arm;
Be fixedly connected on the stiffener of all axial arm bottoms.
3. as claimed in claim 2 for the agitating device of gas-liquid mixed reactor, it is characterized in that, the axis of described agitating fins arm is vertically uniformly distributed.
4., as claimed in claim 3 for the agitating device of gas-liquid mixed reactor, it is characterized in that, described agitating fins is projected as ellipse along its thickness direction.
5. as claimed in claim 1 for the agitating device of gas-liquid mixed reactor, it is characterized in that, the axis of described venthole arm is vertically uniformly distributed.
6. as claimed in claim 1 for the agitating device of gas-liquid mixed reactor, it is characterized in that, described venthole quantity and each venthole corresponding with agitating fins is positioned at below corresponding agitating fins.
7. as claimed in claim 1 for the agitating device of gas-liquid mixed reactor, it is characterized in that, the radially projecting of described venthole arm is vertically triangle, and this leg-of-mutton summit is towards stiffener.
8., as claimed in claim 1 for the agitating device of gas-liquid mixed reactor, it is characterized in that, described rest base is fixed with beam.
CN201410816085.0A 2014-12-24 2014-12-24 A kind of agitating device for gas-liquid mixed reactor Active CN104525016B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107580525A (en) * 2015-05-11 2018-01-12 阿克沃拉技术有限公司 For producing the apparatus and method of bubble in a liquid
CN109135790A (en) * 2018-08-29 2019-01-04 张立升 asphalt production equipment

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103611455A (en) * 2013-10-23 2014-03-05 山东正泰重工科技有限公司 Air-type ingredient stirring machine
CN204338047U (en) * 2014-12-24 2015-05-20 浙江林江化工股份有限公司 A kind of agitating device for gas-liquid mixed reactor

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103611455A (en) * 2013-10-23 2014-03-05 山东正泰重工科技有限公司 Air-type ingredient stirring machine
CN204338047U (en) * 2014-12-24 2015-05-20 浙江林江化工股份有限公司 A kind of agitating device for gas-liquid mixed reactor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107580525A (en) * 2015-05-11 2018-01-12 阿克沃拉技术有限公司 For producing the apparatus and method of bubble in a liquid
US10898867B2 (en) 2015-05-11 2021-01-26 Akvola Technologies GmbH Device and method for generating gas bubbles in a liquid
CN109135790A (en) * 2018-08-29 2019-01-04 张立升 asphalt production equipment

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Address after: 312369, No. three, No. 8, Shangyu Industrial Park, Hangzhou Bay, Zhejiang, Shaoxing

Patentee after: Zhejiang Jitai New Material Co., Ltd

Address before: 312369, No. three, No. 8, Shangyu Industrial Park, Hangzhou Bay, Zhejiang, Shaoxing

Patentee before: ZHEJIANG LINJIANG CHEMICAL Co.,Ltd.