CN104523456A - Cosmetic composition and preparation method thereof - Google Patents
Cosmetic composition and preparation method thereof Download PDFInfo
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- CN104523456A CN104523456A CN201410828813.XA CN201410828813A CN104523456A CN 104523456 A CN104523456 A CN 104523456A CN 201410828813 A CN201410828813 A CN 201410828813A CN 104523456 A CN104523456 A CN 104523456A
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Abstract
The invention relates to a cosmetic composition. The cosmetic composition is prepared from the following components including cetyl PEG/PPG-10/1/poly(dimethylsiloxane), cyclopentasiloxane, pigments, poly(dimethylsiloxane), a silicon elastomer, octyl silicone oil, isononyl isononanoate, vitamin E, phenoxyethanol, boron nitride, essences, butanediol, Tween-60, betaine, glycerol, a crosslinked copolymer of acrylate/C10-30 alkylacrylate, sodium hyaluronate, poly sodium glutamate and water. The invention also provides a preparation method of the cosmetic composition. The cosmetic composition has the advantages of refreshing, oil free, high durability and the like. The preparation method is simple and is easy in operation.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of cosmetic composition and preparation method thereof.
Background technology
Making up, is use cosmetics and instrument, and play up the face of human body, face and other positions, draw, arrange, strengthen three-dimensional impression, adjustment shape and color, covers up defect, performance expression, thus reaches the object of beautifying visual experience.Make up, the exclusive natural beauty of personage can be shown; Can improve personage's original " shape ", " color ", " matter ", increase aesthetic feeling and glamour.Existing cosmetics, if life-time service causes certain damage by skin, if maintain improper, easily accelerate skin ageing; And existing cosmetic maintenance step is generally clean skin-spray cosmetic water-wipings emulsion or facial cream-painting sun screen-cosmetic-makeup removing-spray cosmetic water-wiping emulsion or facial cream, the maintenance practices step that cosmetic is forward and backward is as seen many and complicated, convenient not; In addition, existing cosmetics mostly more greasy, use salubrious not, and sweat meet water time dressing easily come off, use to people and bring inconvenience.
Summary of the invention
The object of the present invention is to provide the cosmetic composition of a kind of quick makeup, non-greasy, salubrious, lasting not de-adornment, the present invention simultaneously also provides the preparation method of this cosmetic composition.
For solving the problem, the technical solution adopted in the present invention is as follows:
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 2-4%, methyl cyclopentane siloxanes 4-6%, pigment 5-8%, polydimethylsiloxane 1-3%, silicone elastomer 4-6%, octyl group silicone oil 3-5%, isononyl isononanoate 3-5%, vitamin E 0.5-1%; Phenoxyethanol 0.3-0.5%, boron nitride 0.5-1.5%, essence 0.05-0.15%; Butanediol 3-8%, Tween-60 1-3%, betanin 2-4%, glycerol 5-7%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5-1%, hyaluronate sodium 0.1-0.2%, polyglutamic acid sodium 0.05-0.15%, surplus is water.
Cetyl PEG/PPG-10/1/ polydimethylsiloxane, English name CETYL PEG/PPG-10/1DIMETHICONE, uses as emulsifying agent.
Methyl cyclopentane siloxanes, decamethylcyclopentasiloxane, in cosmetics and personal care products, has the good compatibility with most alcohol and other cosmetic solvents.
Polydimethylsiloxane, has another name called silicone, has good lubricity, is easy to coating, not soiled laundry, does not hinder the advantages such as the normal function of skin.
Silicone elastomer, can make that dermal sensation is glossy, silkiness is smooth, non-greasy, can strengthen the aesthetic feeling of volatilization silicone oil, and skin is rubbed the viscosity that not balling-up reduces formula.
Octyl group silicone oil, can improve adhesion and greasy feeling in cosmetics, and the surface tension that simultaneously can reduce various oils is to promote vegetable oil, greasepaint, paraffin, the autgmentability of mineral oil and surface coverage, the obliterating time of minimizing cream class and cleaning mixture.
Vitamin E, uses as antioxidant, has slow down aging, reduces effect of wrinkle.
Butanediol, adsorbed water molecule, has very strong moisture-keeping function.
Tween-60, Chang Zuowei emulsifying agent, non-ionic surface active agent, solubilizing agent, wetting agent use.
Betanin is a kind of alkaline matter, has strong moisture pick-up properties, and Chang Zuowei wetting agent uses.
Acrylate/C10-30 alkyl acrylate cross-linked copolymer, a kind of high molecular surfactant.
Hyaluronate sodium is one of formation of human body skin, is the widest glutinous sugar of one acidity of people's distribution in vivo, is present in the substrate of connective tissue, has good moisture-keeping function.
Polyglutamic acid sodium, No. CAS: 28829-38-1, there is good wetting agent effect.
Phenoxyethanol, antiseptic, has good bactericidal action.
Boron nitride, greasy property is good, skin can also be made to have gloss simultaneously.
In the present invention, preferred scheme is that described cosmetic composition is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 5-8%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 3-5%, isononyl isononanoate 3-5%, vitamin E 0.5-1%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%; Butanediol 3-8%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5-1%, hyaluronate sodium 0.1-0.2%, polyglutamic acid sodium 0.1%, surplus is water.
In the present invention, preferred scheme is that described cosmetic composition is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 6%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 4%, isononyl isononanoate 5%, vitamin E 0.5%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%; Butanediol 7%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.1%, polyglutamic acid sodium 0.1%, surplus is water.
The present invention also provides the preparation method of this cosmetic composition, it is characterized in that comprising the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then be heated to dissolve, obtain the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then heat while stirring, be heated to 90-100 DEG C, then constant temperature 18-22min, then be cooled to 75-85 DEG C, obtain the second material system;
C. the second material system that b step obtained adds in the first material system, and stirring and emulsifying 23-27min at the temperature of 75-90 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
In the present invention, preferred scheme is all adopt Steam Heating in described a step and b step.
In the present invention, preferred scheme is that in described step c, the second material system is slowly added in the first material system by filter.
In the present invention, preferred scheme is that described b step is specially: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then heat while stirring, be heated to 95 DEG C, then constant temperature 20min, then be cooled to 80 DEG C, obtain the second material system.
In the present invention, preferred scheme is that described step c is specially: the second material system that b step obtained adds in the first material system, and stirring and emulsifying 25min at the temperature of 85 DEG C, obtains mixed material system.
Compared with prior art, the invention has the advantages that: cosmetic composition of the present invention, can makeup fast, to skin with salubrious, comfortable sensation; In addition, these cosmetics also have the feature of lasting de-adornment, when running into antiperspirant, water, also more stable, avoid people to need repeatedly to refine the make-up and the inconvenience that brings; In addition, the preparation method of cosmetic composition of the present invention, has the advantages such as simple, easy to operate, is suitable for industrial mass production.
Detailed description of the invention
Embodiment 1
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 6%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 4%, isononyl isononanoate 5%, vitamin E 0.5%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%; Butanediol 7%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.1%, polyglutamic acid sodium 0.1%, surplus is water.
The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 95 DEG C, then constant temperature 20min, then be cooled to 80 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 25min at the temperature of 85 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Embodiment 2
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 5%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 3%, isononyl isononanoate 3%, vitamin E 0.5%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%; Butanediol 3%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5%, hyaluronate sodium 0.1%, polyglutamic acid sodium 0.1%, surplus is water.
The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 90 DEG C, then constant temperature 18min, then be cooled to 75 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 23min at the temperature of 75 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Embodiment 3
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 8%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 3-5%, isononyl isononanoate 5%, vitamin E 1%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%; Butanediol 8%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.2%, polyglutamic acid sodium 0.1%, surplus is water.
The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 100 DEG C, then constant temperature 22min, then be cooled to 85 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 27min at the temperature of 75-90 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Embodiment 4
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 2%, methyl cyclopentane siloxanes 6%, pigment 5%, polydimethylsiloxane 3%, silicone elastomer 4%, octyl group silicone oil 5%, isononyl isononanoate 3%, vitamin E 1%; Phenoxyethanol 0.3%, boron nitride 1.5%, essence 0.05%; Butanediol 8%, Tween-60 1%, betanin 4%, glycerol 5%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.1%, polyglutamic acid sodium 0.15%, surplus is water.
The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 98 DEG C, then constant temperature 19min, then be cooled to 78 DEG C, obtain the second material system;
C. just b step obtains the second material system and slowly adds in the first material system by filter, and stirring and emulsifying 26min at the temperature of 83 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Embodiment 5
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 4%, methyl cyclopentane siloxanes 4%, pigment 8%, polydimethylsiloxane 1%, silicone elastomer 6%, octyl group silicone oil 3%, isononyl isononanoate 5%, vitamin E 0.5%; Phenoxyethanol 0.5%, boron nitride 0.5%, essence 0.15%; Butanediol 3%, Tween-60 3%, betanin 2%, glycerol 7%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5%, hyaluronate sodium 0.2%, polyglutamic acid sodium 0.05%, surplus is water.
The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 94 DEG C, then constant temperature 19min, then be cooled to 77 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 24min at the temperature of 81 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Comparative example 1
A kind of cosmetic composition, its composite formula is identical with the formula in embodiment 1; The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 85 DEG C, then constant temperature 24min, then be cooled to 73 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 20min at the temperature of 91 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Comparative example 2
A kind of cosmetic composition, its composite formula is identical with the formula in embodiment 2; The preparation method of this cosmetic composition comprises the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then dissolving with being steam heated to, obtaining the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then Steam Heating is used while stirring, be heated to 105 DEG C, then constant temperature 17min, then be cooled to 87 DEG C, obtain the second material system;
C. the second material system that b step obtained slowly adds in the first material system by filter, and stirring and emulsifying 30min at the temperature of 73 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
Comparative example 3
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 5%, methyl cyclopentane siloxanes 3%, pigment 6%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 4%, isononyl isononanoate 6%, vitamin E 1.2%; Phenoxyethanol 0.6%, boron nitride 1%, essence 0.2%; Butanediol 6%, Tween-60 2%, betanin 3%, glycerol 4%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.2%, polyglutamic acid sodium 0.15%, surplus is water.
This cosmetic composition adopts the preparation method in embodiment 3 to be prepared.
Comparative example 4
A kind of cosmetic composition, it is made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 1.5%, methyl cyclopentane siloxanes 3.8%, pigment 7%, polydimethylsiloxane 4%, silicone elastomer 3%, octyl group silicone oil 4%, isononyl isononanoate 5%, vitamin E 1.2%; Phenoxyethanol 0.3%, boron nitride 1%, essence 0.1%; Butanediol 9%, Tween-60 2%, betanin 5%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.8%, hyaluronate sodium 0.2%, polyglutamic acid sodium 0.15%, surplus is water.
This cosmetic composition adopts the preparation method in embodiment 4 to be prepared.
Experimental example
The compound used for cosmetic that Example 1-5, comparative example 1-4 are obtained, then 180 volunteers are selected, it is one group that every 20 volunteers compile, make up with the cosmetic composition that embodiment 1-5, comparative example 1-4 are obtained respectively, then the salubrious degree of these cosmetics, greasy feeling and persistence are evaluated.
Salubrious degree and greasy feeling all adopt sensory evaluation, and Appraising subject is the volunteer using the cosmetic composition that obtains of embodiment 1-5, comparative example 1-4 corresponding, wherein clearly spend employings " without obviously clearly feeling, more clearly and very salubrious " three indexs; Three indexs that greasy degree adopts " without greasy feeling, generally greasy and very greasy ", concrete outcome refers to following table 1-2:
The salubrious degree test data table of table 1: embodiment 1-5, comparative example 1-4 cosmetic composition
Note: the digitized representation in table be number, as embodiment 1 and without obviously clearly feel 0 in crossing form, represent, use in the volunteer of the cosmetic composition of embodiment 1, nobody feels without obviously clearly feeling.
Data as can be seen from this form, adopt the cosmetic composition that the inventive method is obtained, human body sensory is salubrious, and wherein the effect of embodiment 1 is optimum.
The greasy degree test data table of table 2: embodiment 1-5, comparative example 1-4 cosmetic composition
Note: the digitized representation in table be number, as embodiment 1 and without obviously clearly feel 20 in crossing form, expression, use in the volunteer of the cosmetic composition of embodiment 1, feeling-realization cosmetic is 20 people without the number of greasy feeling.
Data as can be seen from this form, adopt the cosmetic composition that the inventive method is obtained, and human body sensory is without greasy, and wherein the effect of embodiment 1 is optimum.
The persistence of the cosmetic composition obtained for embodiment 1-5, comparative example 1-4 is tested, and the index of test comprises: cosmetics come off the time naturally volunteer face; Volunteer is (general motion amount) at the volley, and cosmetics come off the time volunteer face; Averaged the above-mentioned time, concrete data refer to following table 3:
The persistence test data table of table 3: embodiment 1-5, comparative example 1-4 cosmetic composition
Data as can be seen from upper table, adopt the cosmetic composition that the inventive method is obtained, the duration of cosmetics is long, even if in motor process, human body, also can at long period not de-adornment under the situation of sweating, highly stable, wherein the effect of embodiment 1 is optimum.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (8)
1. a cosmetic composition, it is characterized in that being made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 2-4%, methyl cyclopentane siloxanes 4-6%, pigment 5-8%, polydimethylsiloxane 1-3%, silicone elastomer 4-6%, octyl group silicone oil 3-5%, isononyl isononanoate 3-5%, vitamin E 0.5-1%; Phenoxyethanol 0.3-0.5%, boron nitride 0.5-1.5%, essence 0.05-0.15%, butanediol 3-8%, Tween-60 1-3%, betanin 2-4%, glycerol 5-7%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5-1%, hyaluronate sodium 0.1-0.2%, polyglutamic acid sodium 0.05-0.15%, surplus is water.
2. cosmetic composition according to claim 1, it is characterized in that being made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 5-8%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 3-5%, isononyl isononanoate 3-5%, vitamin E 0.5-1%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%, butanediol 3-8%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 0.5-1%, hyaluronate sodium 0.1-0.2%, polyglutamic acid sodium 0.1%, surplus is water.
3. cosmetic composition according to claim 1, it is characterized in that being made up of the following component according to percent by weight: cetyl PEG/PPG-10/1/ polydimethylsiloxane 3%, methyl cyclopentane siloxanes 5%, pigment 6%, polydimethylsiloxane 2%, silicone elastomer 5%, octyl group silicone oil 4%, isononyl isononanoate 5%, vitamin E 0.5%; Phenoxyethanol 0.4%, boron nitride 1%, essence 0.1%, butanediol 7%, Tween-60 2%, betanin 3%, glycerol 6%, acrylate/C10-30 alkyl acrylate cross-linked copolymer 1%, hyaluronate sodium 0.1%, polyglutamic acid sodium 0.1%, surplus is water.
4. the preparation method of cosmetic composition according to claim 1, is characterized in that comprising the steps:
A. oil phase preparation: by the cetyl PEG/PPG-10/1/ polydimethylsiloxane of formula ratio, methyl cyclopentane siloxanes, pigment, polydimethylsiloxane, silicone elastomer, octyl group silicone oil, isononyl isononanoate, vitamin E mixing, then be heated to dissolve, obtain the first material system;
B. aqueous phase preparation: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then heat while stirring, be heated to 90-100 DEG C, then constant temperature 18-22min, then be cooled to 75-85 DEG C, obtain the second material system;
C. the second material system that b step obtained adds in the first material system, and stirring and emulsifying 23-27min at the temperature of 75-90 DEG C, obtains mixed material system;
D. then, in the mixed material system obtained through step c, add the phenoxyethanol of formula ratio, boron nitride and essence, stir, be cooled to room temperature, obtain product.
5. the preparation method of cosmetic composition according to claim 4, is characterized in that: all adopt Steam Heating in described a step and b step.
6. the preparation method of cosmetic composition according to claim 4, is characterized in that: in described step c, the second material system is slowly added in the first material system by filter.
7. the preparation method of cosmetic composition according to claim 4, it is characterized in that described b step is specially: by the butanediol of formula ratio, Tween-60, betanin, glycerol, acrylate/C10-30 alkyl acrylate cross-linked copolymer, hyaluronate sodium, polyglutamic acid sodium and water mixing, then heat while stirring, be heated to 95 DEG C, then constant temperature 20min, then be cooled to 80 DEG C, obtain the second material system.
8. the preparation method of cosmetic composition according to claim 4, is characterized in that described step c is specially: the second material system that b step obtained adds in the first material system, and stirring and emulsifying 25min at the temperature of 85 DEG C, obtains mixed material system.
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| CN201410828813.XA CN104523456A (en) | 2014-12-26 | 2014-12-26 | Cosmetic composition and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1471903A (en) * | 2002-06-26 | 2004-02-04 | �ź㴫 | Water in oil emulsion powdery cream |
| US7455847B1 (en) * | 2001-02-20 | 2008-11-25 | Comestic Laboratories Of America, A Division Of St. Ives Laboratories, Inc. | Pigmented cosmetic composition and methods related thereto |
| CN103491942A (en) * | 2011-04-29 | 2014-01-01 | 莱雅公司 | Emulsion w/si foundation |
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2014
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7455847B1 (en) * | 2001-02-20 | 2008-11-25 | Comestic Laboratories Of America, A Division Of St. Ives Laboratories, Inc. | Pigmented cosmetic composition and methods related thereto |
| CN1471903A (en) * | 2002-06-26 | 2004-02-04 | �ź㴫 | Water in oil emulsion powdery cream |
| CN103491942A (en) * | 2011-04-29 | 2014-01-01 | 莱雅公司 | Emulsion w/si foundation |
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