CN104513584A - Modified epoxy-connected paint and preparing method thereof - Google Patents
Modified epoxy-connected paint and preparing method thereof Download PDFInfo
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- CN104513584A CN104513584A CN201310449975.8A CN201310449975A CN104513584A CN 104513584 A CN104513584 A CN 104513584A CN 201310449975 A CN201310449975 A CN 201310449975A CN 104513584 A CN104513584 A CN 104513584A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention relates to modified epoxy-connected paint and a preparing method thereof. An A component of the paint is prepared by adding epoxy resin into a mixed solvent of xylene, n-butanol and cyclohexanone, adding copolymer of vinyl chloride and vinyl isobutyl ether, chlorinated rubber, acrylic resin, wet-method sericite, mica iron oxide, fumed silica, talcum powder, titanium dioxide, a polymethylalkyl siloxane solution and polyamide wax, mixing, stirring, and grinding. A B component of the paint is prepared by mixing a cashew nut shell oil modified phenolic aldehyde amine curing agent and a phenolic aldehyde amine curing agent, and stirring uniformly. During using, the A component and the B component are mixed uniformly. The paint can be used for intermediate paint of anti-corrosive primer, and antifouling paint, or chlorinated rubber finish or decorative finish so as to ensure good adhesive force.
Description
Technical field
The present invention relates to a kind of modified epoxy and connect coating and manufacture method, for rust-inhibiting paint and antifouling varnish or chlorinated rubber finish or the intermediate coat decorating finish paint.
Background technology
Existing epoxy resin intermediate coat, its weak point is that rate of drying is slow, long construction period, and the finish paint narrow range be suitable for it.
Summary of the invention
The object of this invention is to provide a kind of rate of drying fast, short construction period, and the modified epoxy good with multiple topcoat sticking power is connected coating and manufacture method.
A kind of modified epoxy of the present invention connects coating, it is characterized in that by 1 parts by weight epoxy resin, 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, 0.4 weight part pimelinketone, 0.01 ~ 0.8 weight part chlorinated polyether resin, 0.01 ~ 0.8 weight part chlorinated rubber, 0.01 ~ 0.8 parts by weight propylene acid resin, 0.4 ~ 0.8 weight part wet method sericite, 0.1 ~ 0.9 parts by weight mica ferric oxide, 0.01 ~ 0.1 weight part aerosil, 0.5 ~ 1.5 weight part talcum powder, 0.5 ~ 1.5 weight part titanium dioxide, 0.01 ~ 0.1 weight part gathers methyl alkyl siloxane solution, 0.01 ~ 0.02 weight parts of polyamide wax composition component A, B component is formed by the cashew nut oil modified phenolic aldehyde amine curing agent of 0.01 ~ 0.3 weight part and 1 parts by weight of phenolic amine curing agent.
Preferably modified epoxy connects coating, it is characterized in that by 1 parts by weight epoxy resin, 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, 0.4 weight part pimelinketone, 0.2 weight part chlorinated polyether resin, 0.2 weight part chlorinated rubber, 0.2 parts by weight propylene acid resin, 0.6 weight part wet method sericite, 0.5 parts by weight mica ferric oxide, 0.02 weight part aerosil, 0.6 weight part talcum powder, 0.6 weight part titanium dioxide, 0.02 weight part gathers methyl alkyl siloxane solution, 0.01 weight parts of polyamide wax forms component A; B component is formed by the cashew nut oil modified phenolic aldehyde amine curing agent of 0.2 weight part and 1 parts by weight of phenolic amine curing agent.
Modified epoxy connects the manufacture method of coating, 1 parts by weight epoxy resin is it is characterized in that to join 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.4 weight part pimelinketone, dispersing and dissolving in addition, add 0.1 ~ 0.8 weight part chlorinated polyether resin again, 0.1 ~ 0.8 weight part chlorinated rubber, 0.1 ~ 0.8 parts by weight propylene acid resin, after high-speed stirring, 0.4 ~ 0.8 weight part wet method sericite is added when stirring, 0.1 ~ 0.9 parts by weight mica ferric oxide, 0.01 ~ 0.1 weight part aerosil, 0.5 ~ 1.5 weight part talcum powder, 0.5 ~ 1.5 weight part titanium dioxide, 0.01 ~ 0.1 weight part gathers methyl alkyl siloxane solution, 0 ~ 0.02 weight parts of polyamide wax, then this coating component A is made with sand mill grinding 0.5 ~ 1h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.01 ~ 0.3 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component.
Preferably modified epoxy connects the manufacture method of coating, 1 parts by weight epoxy resin is it is characterized in that to join 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.7 weight part pimelinketone, dispersing and dissolving in addition, add 0.2 weight part chlorinated polyether resin again, 0.2 weight part chlorinated rubber, 0.2 parts by weight propylene acid resin, after high-speed stirring, 0.6 weight part wet method sericite is added when stirring, 0.5 parts by weight mica ferric oxide, 0.02 weight part aerosil, 0.6 weight part talcum powder, 0.6 weight part titanium dioxide, 0.02 weight part gathers methyl alkyl siloxane solution, 0.01 weight parts of polyamide wax, then this coating component A is made with sand mill grinding 1h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.2 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component.
Modified epoxy of the present invention connects coating and manufacture method, by epoxy resin solution, chlorinated polyether resin solution, chlorinated rubber solution, acrylic resin soln, add a small amount of auxiliary agent, and the color stuffing of some amount is formulated.A large amount of hydroxyls and ether isopolarity group is had in the epoxy molecule structure used in the fabrication process, epoxy group(ing) active in the curing process and primer coating form very firmly chemical bond, enhance the sticking power with primer coating, and make that coating is hard, snappiness good.The chlorinated polyether resin used, chlorinated rubber and acrylic resin are single-component thermosetting resin, and rate of drying is fast, and favorable solubility, therefore during brushing surface lacquering, meeting and finish paint film forming matter produce infiltration to a certain degree, make it have good sticking power.Modified epoxy connects the advantage that coating combines epoxy resin and chlorinated polyether resin, chlorinated rubber, acrylic resin, all have good sticking power, and rate of drying is fast with rust-proofing primer and finish paint.The wet method sericite used is made up of two-layer silicon-oxy tetrahedron and one deck alumina octahedral, is very thin flaky material, can improves the anti-water-permeable of paint film, improves paint film intensity.The iron mica used has shielding effect, overlapped by thin slice particle, makes moisture and corrosive medium diffusion admittance extend and be obstructed, increases preservative efficacy.The aerosil used can improve anti-settling property and the sag prevention performance of coating, poly-methyl alkyl siloxane solution reduces the surface tension of coating system, improve flowing and levelling property and the bubble contributed in elimination coating, and avoid the formation of Bei Nade whirlpool.The polyamide wax used contributes to the thixotropy and the application property that improve coating, improves the stability in storage of coating.
The present invention's beneficial effect compared with prior art
1, modified epoxy of the present invention connects coating, and its coating rate of drying is fast, short construction period
2, excellent with rust-proofing primer, antifouling varnish, chlorinated rubber finish, decoration finish paint sticking power.
Embodiment
Embodiment 1
Modified epoxy of the present invention connects manufacture method-1 of coating.In stainless charging basket, first add 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, 0.4 weight part pimelinketone mixes, adding 1 parts by weight epoxy resin again makes it dissolve in advance, then 0.2 weight part chlorinated polyether resin is added, 0.2 weight part chlorinated rubber, 0.2 parts by weight propylene acid resin, after high-speed stirring 0.5h, 0.6 weight part wet method sericite is added when stirring, 0.5 parts by weight mica ferric oxide, 0.02 weight part aerosil, 0.6 weight part talcum powder, 0.6 weight part titanium dioxide, 0.02 weight part gathers methyl alkyl siloxane solution, 0.01 weight parts of polyamide wax, then sand mill circular grinding 0.5 ~ 1h is used, namely obtain chlorinated polyether resin modified epoxy and connect coating component A-1, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.2 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component-1.
Embodiment 2
Modified epoxy of the present invention connects manufacture method-2 of coating.Connect the chlorinated polyether resin of mixed 0.6 weight part in coating at the modified epoxy that embodiment 1 is identical, make modified epoxy and connect coating component A-2.
The application property of modified epoxy connection coating and coating adhesion experimental result are in table 1.
Table 1
Tin-free self-polishing antifouling paint used and epoxy resin antirust bottom paint are Tianjin Cnpc Boxing Engineering Technology Co., Ltd.'s product, and all the other starting material are commercially available.
Embodiment 3
1 parts by weight epoxy resin is joined 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.4 weight part pimelinketone, dispersing and dissolving in addition, add 0.1 weight part chlorinated polyether resin again, 0.1 weight part chlorinated rubber, 0.1 parts by weight propylene acid resin, after high-speed stirring, 0.4 weight part wet method sericite is added when stirring, 0.1 parts by weight mica ferric oxide, 0.01 weight part aerosil, 0.5 weight part talcum powder, 0.5 weight part titanium dioxide, 0.01 weight part gathers methyl alkyl siloxane solution, then this coating component A is made with sand mill grinding 0.5h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.01 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component.
Embodiment 4
1 parts by weight epoxy resin is joined 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.4 weight part pimelinketone, dispersing and dissolving in addition, add 0.8 weight part chlorinated polyether resin again, 0.8 weight part chlorinated rubber, 0.8 parts by weight propylene acid resin, after high-speed stirring, 0.8 weight part wet method sericite is added when stirring, 0.9 parts by weight mica ferric oxide, 0.1 weight part aerosil, 1.5 weight part talcum powder, 1.5 weight part titanium dioxides, 0.1 weight part gathers methyl alkyl siloxane solution, 0.02 weight parts of polyamide wax, then this coating component A is made with sand mill grinding 1h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.3 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component.
Claims (4)
1. a modified epoxy connects coating, it is characterized in that by 1 parts by weight epoxy resin, 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, 0.4 weight part pimelinketone, 0.01 ~ 0.8 weight part chlorinated polyether resin, 0.01 ~ 0.8 weight part chlorinated rubber, 0.01 ~ 0.8 parts by weight propylene acid resin, 0.4 ~ 0.8 weight part wet method sericite, 0.1 ~ 0.9 parts by weight mica ferric oxide, 0.01 ~ 0.1 weight part aerosil, 0.5 ~ 1.5 weight part talcum powder, 0.5 ~ 1.5 weight part titanium dioxide, 0.01 ~ 0.1 weight part gathers methyl alkyl siloxane solution, 0.01 ~ 0.02 weight parts of polyamide wax composition component A, B component is formed by the cashew nut oil modified phenolic aldehyde amine curing agent of 0.01 ~ 0.3 weight part and 1 parts by weight of phenolic amine curing agent.
2. modified epoxy according to claim 1 connects coating, it is characterized in that by 1 parts by weight epoxy resin, 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, 0.4 weight part pimelinketone, 0.2 weight part chlorinated polyether resin, 0.2 weight part chlorinated rubber, 0.2 parts by weight propylene acid resin, 0.6 weight part wet method sericite, 0.5 parts by weight mica ferric oxide, 0.02 weight part aerosil, 0.6 weight part talcum powder, 0.6 weight part titanium dioxide, 0.02 weight part gathers methyl alkyl siloxane solution, 0.01 weight parts of polyamide wax forms component A; B component is formed by the cashew nut oil modified phenolic aldehyde amine curing agent of 0.2 weight part and 1 parts by weight of phenolic amine curing agent.
3. the manufacture method of a modified epoxy connection coating according to claim 1, 1 parts by weight epoxy resin is it is characterized in that to join 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.4 weight part pimelinketone, dispersing and dissolving in addition, add 0.1 ~ 0.8 weight part chlorinated polyether resin again, 0.1 ~ 0.8 weight part chlorinated rubber, 0.1 ~ 0.8 parts by weight propylene acid resin, after high-speed stirring, 0.4 ~ 0.8 weight part wet method sericite is added when stirring, 0.1 ~ 0.9 parts by weight mica ferric oxide, 0.01 ~ 0.1 weight part aerosil, 0.5 ~ 1.5 weight part talcum powder, 0.5 ~ 1.5 weight part titanium dioxide, 0.01 ~ 0.1 weight part gathers methyl alkyl siloxane solution, 0 ~ 0.02 weight parts of polyamide wax, then this coating component A is made with sand mill grinding 0.5 ~ 1h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.01 ~ 0.3 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component, during use, component A is mixed with B component.
4. modified epoxy according to claim 3 connects the manufacture method of coating, 1 parts by weight epoxy resin is it is characterized in that to join 0.8 parts by weight of xylene, 0.2 part by weight of n-butanol, in the mixed solvent of 0.4 weight part pimelinketone, dispersing and dissolving in addition, add 0.2 weight part chlorinated polyether resin again, 0.2 weight part chlorinated rubber, 0.2 parts by weight propylene acid resin, after high-speed stirring, 0.6 weight part wet method sericite is added when stirring, 0.5 parts by weight mica ferric oxide, 0.02 weight part aerosil, 0.6 weight part talcum powder, 0.6 weight part titanium dioxide, 0.02 weight part gathers methyl alkyl siloxane solution, 0.01 weight parts of polyamide wax, then this coating component A is made with sand mill grinding 1h, the cashew nut oil modified phenolic aldehyde amine curing agent of 0.2 weight part is mixed with 1 parts by weight of phenolic amine curing agent and forms this coating B component, during use, component A is mixed with B component.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310449975.8A CN104513584B (en) | 2013-09-27 | 2013-09-27 | A kind of modified epoxy connection coating and manufacture method |
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| CN201310449975.8A CN104513584B (en) | 2013-09-27 | 2013-09-27 | A kind of modified epoxy connection coating and manufacture method |
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| CN104513584B CN104513584B (en) | 2017-03-15 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104777725A (en) * | 2015-04-17 | 2015-07-15 | 广西藤县通轩立信化学有限公司 | Method for preparing adhesive resin composition for toner |
| CN105017914A (en) * | 2015-07-21 | 2015-11-04 | 厦门双瑞船舶涂料有限公司 | Method for preparing connection paint from rosin-modified acrylate |
| CN110724436A (en) * | 2019-10-24 | 2020-01-24 | 厦门双瑞船舶涂料有限公司 | Epoxy grafted acrylate self-layering connecting paint and preparation method thereof |
| CN113214708A (en) * | 2021-04-27 | 2021-08-06 | 武汉双虎涂料有限公司 | Bottom surface containing type connecting coating and preparation method thereof |
| CN116814125A (en) * | 2023-06-29 | 2023-09-29 | 厦门双瑞船舶涂料有限公司 | Connecting paint capable of improving cracking resistance of anti-fouling coating after soaking and preparation method thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10157004A (en) * | 1996-09-30 | 1998-06-16 | William J Brinton | Anticorrosive film, composite material, and coating method |
| CN100487070C (en) * | 2006-07-12 | 2009-05-13 | 海洋化工研究院 | Solvent-free expansion type fire-proof epoxy coating and its preparation method |
| CN102329585B (en) * | 2010-07-12 | 2013-10-23 | 上海海鹰粘接科技有限公司 | Leak-blocking adhesive and preparation method thereof |
| CN102558989A (en) * | 2010-12-09 | 2012-07-11 | 海洋化工研究院 | Anti-fouling coating material with excellent compatibility and use thereof |
-
2013
- 2013-09-27 CN CN201310449975.8A patent/CN104513584B/en active Active
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104777725A (en) * | 2015-04-17 | 2015-07-15 | 广西藤县通轩立信化学有限公司 | Method for preparing adhesive resin composition for toner |
| CN105017914A (en) * | 2015-07-21 | 2015-11-04 | 厦门双瑞船舶涂料有限公司 | Method for preparing connection paint from rosin-modified acrylate |
| CN105017914B (en) * | 2015-07-21 | 2017-03-22 | 厦门双瑞船舶涂料有限公司 | Method for preparing connection paint from rosin-modified acrylate |
| CN110724436A (en) * | 2019-10-24 | 2020-01-24 | 厦门双瑞船舶涂料有限公司 | Epoxy grafted acrylate self-layering connecting paint and preparation method thereof |
| CN113214708A (en) * | 2021-04-27 | 2021-08-06 | 武汉双虎涂料有限公司 | Bottom surface containing type connecting coating and preparation method thereof |
| CN113214708B (en) * | 2021-04-27 | 2022-06-14 | 武汉双虎涂料股份有限公司 | Bottom surface containing type connecting coating and preparation method thereof |
| CN116814125A (en) * | 2023-06-29 | 2023-09-29 | 厦门双瑞船舶涂料有限公司 | Connecting paint capable of improving cracking resistance of anti-fouling coating after soaking and preparation method thereof |
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| CN104513584B (en) | 2017-03-15 |
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