A kind of visualization coal sample tank being used under high pressure low temperature environment and its application method
Technical field
A kind of visualization coal sample tank involved in the present invention and its application method, can be used in R&D institution and universities and colleges, to see
When examining the characteristic of change, particularly learning gas of the tank intrabody object in certain pressure with a temperature of, under the conditions of high pressure low temperature
When reaching the phase-state change point of gas, observable gas is turned under certain temperature, certain pressure from gas phase to liquid phase or solid phase
The process of change.
Background technology
The Gas Outburst as caused by coal-bed gas and blast are to endanger one of source of safety of coal mines, with mining depth
Increase, the environmental effect of gas becomes increasingly complex, characterization of adsorption and its water of the research gas in coal body under various environmental effects
The formation characteristic of compound, the clean and effective of gas problem and gas to solution Safety of Coal Mine Production, which is utilized, very important meaning
Justice.
Temperature drops to less than -161.5 DEG C and can just liquefied under methane gas normal pressure, warm if increase pressure is to 4.59MPa
Degree drops to -82.6 DEG C, can also liquefy, therefore in the research of high pressure low temperature is carried out to methane gas, if pressure and temperature reaches
To the transformation temperature of gas, if can intuitively observe that gas is become the dynamic process of liquid phase or solid phase by gas phase, we are grasped
The phase transition temperature and pressure of methane gas, and related gas absorption and Gas Hydrate generation research have it is very big
Help.
It is the characteristic research that sample is carried out using traditional completely enclosed tank body at this stage in R&D institution and universities and colleges,
Such as Publication No. CN203148927U, a kind of entitled coal sample tank and Publication No. CN202710542U, denomination of invention
, can only be by the change of pressure gauge or pressure sensor indirect reaction pressure inside the tank, it is impossible to straight for the Chinese patent of coal sample tank
The observation phase-state change process of gas in the sample under high pressure low temperature.
The content of the invention
The present invention is ensureing that tank body is high pressure resistant, resistance to low to solve the deficiency of existing traditional non-visual coal sample tank
On the premise of temperature, increase by a transparent plastic cylinder in lateral opening hole, the change of sample in tank is observed using high-definition camera.Although
High-definition camera can only observe the situation of change of sample surfaces gas, but because in sample the situation of change of gas be it is homogeneous,
Therefore its overall situation of change is also represent, this problem is solved well.
To achieve the above object, the present invention is adopted the following technical scheme that:A kind of visualization being used under high pressure low temperature environment
Coal sample tank, it includes tank body and cover, it is characterised in that wherein, and tank body is internally provided with coal sample chamber body, one of tank body
It is provided with side and is shaped as hollow cuboid, and the circular hole that the hollow space of the cuboid gradually reduces for diameter, according to
Secondary is one-level Circularhole diameter, two grades of Circularhole diameters, three-level Circularhole diameters;The hollow space is internally provided with transparent cylinder,
And the diameter of the transparent cylinder is less than two grades of Circularhole diameters so that both contact closely, the transparent cylinder bottom
Portion has a diameter to be less than the transparent cylinder ledge that the three-level Circularhole diameter, thickness are more than three-level circular hole thickness, so that
The transparent cylinder is in contact with the three-level circular hole by O-ring;Cylinder is provided with the outside of the transparent cylinder to fix
Body, the cylinder fixes outer diameter and is less than hollow one-level diameter, and surrounding is screw thread, the interior diameter of the cylinder fixed body with
Transparent column diameter is identical, and cylinder fixed body bottom is in sealing contact by O-ring and the hollow cuboid;In the cover
Portion is provided with annular groove, and the width of the annular groove and the tank body consistency of thickness, and the both sides of annular groove are respectively provided with screw thread,
There are two O-rings inside the annular groove of the cover, so that the cover and the tank body are in sealing contact, in the middle part of the cover
It is taper to be provided with the top of pressure tap and thermometer hole, and the pressure tap and thermometer hole, the pressure tap external connection pressure
Sensor, temperature sensor is directly fixed in thermometer hole by hollow special plug sealing and measures temperature in tank;It is described transparent
High-definition camera is provided with the outside of cylinder.
Further, preferably, the both sides of the cylinder fixed body are respectively provided with circular neck, tightening tool stretches into the circle
Cylinder fixed body is tightened on the hollow cuboid in shape neck.
Further, preferably, the both sides of the cover are respectively provided with circular neck, tightening tool stretches into the circular neck
It is interior that cover is tightened on the tank body.
Further, it is stainless steel preferably, the material of the cylinder fixed body is as tank body, cover material
Make.
Further, preferably, the pressure tap is into and out stomata, the temperature sensor directly passes through hollow special silk
Stifled sealing is fixed on the temperature in measurement tank body in thermometer hole.
Further, preferably, the size of the coal sample chamber body is high 100mm, interior diameter is 50mm.
Further, preferably, the high-definition camera is fixedly installed by camera bracket, and the camera bracket
The inside of the stationary cylinder is arranged on, can freely be moved forward and backward.
Further, preferably, the transparent cylinder is high pressure resistant, low temperature resistant transparent cylinder.
In addition, present invention also offers it is a kind of be used for high pressure low temperature environment under visualization coal sample tank application method, its
It is characterised by, it comprises the following steps:
(1) O-ring and transparent cylinder are put into the hollow cuboid of the side of tank body in order first, then will
Cylinder fixed body is screwed into by specific purpose tool by circular neck in hollow cuboid;
(2) and then by the cover open, coal sample needed for experiment is loaded in the coal sample chamber body, special tool is then used
Tool tightens coal sample cover by circular neck, and ensures that the O-ring in cover annular groove makes coal sample tank top seal air tight;
Hollow pipeline is inserted in pressure tap, and the pipeline passes through hollow special plug, makes the plug and pressure tap week
Enclose to be threadedly coupled, to ensure that pressure tap is air tight, the pressure sensor in the pipeline external connection is passed by the pressure
Sensor measures the pressure in the coal sample chamber body, and the pipeline is also inflatable and deflatable pipeline;Pass through silk in the thermometer hole
Stifled connection temperature sensor, and temperature sensor and pressure sensor are connected to computer by data wire, pass through computer
To show the real-time change of pressure and temperature;
(3) after the installation is complete, under the premise of loading coal sample and ensureing that coal sample tank is gastight, it is filled with into coal sample tank
Experimental gas is placed in the insulating box of setting experimental temperature to required pressure, and by coal sample tank;
(4) high-definition camera, is opened, suitable position is placed it in using camera bracket, regulation surrounding light compensating lamp
Brightness makes its imaging clearly become clear, and when phase-state change occurs for gas in tank, high-definition camera can be by picture concerned and image
Data logging is in computer.
The beneficial effects of the present invention are, the present invention solves the deficiency of existing traditional non-visual coal sample tank,
Ensure that tank body is high pressure resistant, on the premise of low temperature, increase by a transparent plastic cylinder in lateral opening hole, utilize high-definition camera observation tank
The change of interior sample.Although high-definition camera can only observe the situation of change of sample surfaces gas, because gas in sample
Situation of change is homogeneous, therefore also represent its overall situation of change.
Brief description of the drawings
Fig. 1 is a kind of sectional view of visualization coal sample tank being used under high pressure low temperature environment of the present invention;
Fig. 2 is that a kind of structure of the transparent cylinder of visualization coal sample tank being used under high pressure low temperature environment of the present invention is shown
It is intended to;
Fig. 3 is hollow cuboid and the fixation of a kind of visualization coal sample tank being used under high pressure low temperature environment of the present invention
Side view after cylinder installation;
Fig. 4 is hollow cuboid and the fixation of a kind of visualization coal sample tank being used under high pressure low temperature environment of the present invention
Schematic three dimensional views after cylinder installation;
Wherein, the circular neck of 1- tank bodies, 2- coal sample chambers body, 3- covers, 4- pressure taps, 5- thermometer holes, 6,10-, 7-O types
Circle, the hollow cuboids of 8-, 9- transparent cylinders, 11- cylinders fixed body, 12- high-definition cameras, 13- camera brackets, 14-
Transparent cylinder ledge, 15- one-levels Circularhole diameter, bis- grades of Circularhole diameters of 16-, 17- three-level Circularhole diameters.
Embodiment
Come to carry out the present invention detailed description below in conjunction with accompanying drawing.It should be appreciated, however, that accompanying drawing has been provided only more
Understand the present invention well, they should not be interpreted as limitation of the present invention.
As Figure 1-4, the invention provides a kind of visualization coal sample tank being used under high pressure low temperature environment, it includes tank
Body 1 and cover 3, wherein, being internally provided with coal sample chamber body 2, a side of tank body 1 of tank body 1, which be provided with, to be shaped as
Empty cuboid 8, and the hollow space of hollow cuboid 8 is circular hole that diameter gradually reduces, be followed successively by one-level Circularhole diameter 15,
Two grades of Circularhole diameters 16, three-level Circularhole diameters 17;Hollow space is internally provided with transparent cylinder 9, and transparent cylinder 9 is straight
Footpath is less than two grades of Circularhole diameters 16 so that both contact closely, and the bottom of transparent cylinder 9 has a diameter to be less than three-level Circularhole diameter
17th, thickness is more than the transparent cylinder ledge 14 of the thickness of three-level Circularhole diameter 17, so that transparent cylinder 9 is justified with three-level
Bore dia 17 is in contact by O-ring;The outside of transparent cylinder 9 is provided with cylinder fixed body 11, the overall diameter of cylinder fixed body 11
Less than the one-level diameter of hollow cuboid, and surrounding is screw thread, interior diameter and the diameter phase of transparent column 9 of cylinder fixed body 11
Together, the bottom of cylinder fixed body 11 is in sealing contact by O-ring and hollow cuboid 8;Cover 3 is internally provided with annular groove, and
The width of annular groove and the consistency of thickness of tank body 1, and the both sides of annular groove are respectively provided with screw thread, have two inside the annular groove of cover 3
Individual O-ring 7, so that cover 3 and tank body 1 are in sealing contact, the middle part of cover 3 is provided with pressure tap 4 and thermometer hole 5, and pressure tap 4 and survey
The top in warm hole 5 is taper, and the external connection pressure sensor of pressure tap 4, temperature sensor directly passes through hollow special plug
The temperature of measurement tank interior in thermometer hole 5;The outside of transparent cylinder 9 is provided with high-definition camera 12.
In the present embodiment, the both sides of cylinder fixed body 11 are respectively provided with circular neck 10, and tightening tool stretches into the circle
Cylinder fixed body 11 is tightened on hollow cuboid 8 in neck 10.The both sides of cover 3 are respectively provided with circular neck 6, twist
Clamping tool, which is stretched into, is tightened to cover 3 on tank body 1 in circular neck 6.The material of cylinder fixed body 11 and tank body 1, cover 3
Material is the same, is that stainless steel makes.Pressure tap 4 is into and out stomata, and temperature sensor is directly sealed by hollow special plug
It is fixed on the temperature in the internal measurement tank body of thermometer hole 5.The size of coal sample chamber body 2 is high 100mm, and interior diameter is 50mm.It is high
Clear camera 12 is fixedly installed by camera bracket 13, and camera bracket 13 is arranged on the inside of cylinder fixed body 11.
In addition, present invention also offers it is a kind of be used for high pressure low temperature environment under visualization coal sample tank application method, its
Comprise the following steps:
(1) O-ring and transparent cylinder 9 are put into the hollow cuboid 8 of the side of tank body 1 in order first, connect
And be screwed into cylinder fixed body 11 in hollow cuboid by circular neck 10 by specific purpose tool;
(2) and then by cover 3 open, coal sample needed for experiment is loaded in coal sample chamber body 2, then passed through with specific purpose tool
Circular neck 6 tightens coal sample cover 3, and ensures that the O-ring 7 in cover annular groove makes coal sample tank top seal air tight;Surveying
Hollow pipeline is inserted in pressure hole 4, and pipeline passes through hollow special plug, makes to be threadedly coupled around plug and pressure tap 4,
To ensure that pressure tap is air tight, the pressure sensor in pipeline external connection is measured in coal sample chamber body 2 by pressure sensor
Pressure, the pipeline is also inflatable and deflatable pipeline;Temperature sensor is connected by plug in thermometer hole 5, and temperature is passed
Sensor and pressure sensor are connected to computer by data wire, and the real-time change of pressure and temperature is shown by computer;
(3) after the installation is complete, under the premise of loading coal sample and ensureing that coal sample tank is gastight, it is filled with into coal sample tank
Experimental gas is placed in the insulating box of setting experimental temperature to required pressure, and by coal sample tank;
(4) high-definition camera 12 is opened, suitable position is placed it in using camera bracket 13, surrounding light compensating lamp is adjusted
Brightness its imaging clearly is become clear, when phase-state change occurs for gas in tank, high-definition camera 12 can by picture concerned and
Image data is recorded in computer.
Embodiment of above is merely to illustrate the present invention, and not limitation of the present invention, about the common of technical field
Technical staff, without departing from the spirit and scope of the present invention, can also make a variety of changes and modification, therefore all
Equivalent technical scheme falls within scope of the invention, and scope of patent protection of the invention should be defined by the claims.