CN104497780A - Heat resistant anticorrosive paint and preparation method thereof - Google Patents
Heat resistant anticorrosive paint and preparation method thereof Download PDFInfo
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- CN104497780A CN104497780A CN201410671698.XA CN201410671698A CN104497780A CN 104497780 A CN104497780 A CN 104497780A CN 201410671698 A CN201410671698 A CN 201410671698A CN 104497780 A CN104497780 A CN 104497780A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
- C09D161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09D161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F218/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid
- C08F218/02—Esters of monocarboxylic acids
- C08F218/04—Vinyl esters
- C08F218/08—Vinyl acetate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F292/00—Macromolecular compounds obtained by polymerising monomers on to inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a heat resistant anticorrosive paint, which is characterized by being prepared from the following raw materials by weight: 30-35 parts of phenolic resin, 1-3 parts of tetramethylsilane, 7-9 parts of 200 # solvent oil, 3-5 parts of dolomite powder, 3-5 parts of bauxite, 2-3 parts of sodium diacetate, 1-3 parts of glycollic amide, 23-26 parts of glyceride maleic anhydride resin, 2-4 parts of aluminum tripolyphosphate, 2-3 parts of selenium acetylacetone, 1-2 parts of ethylenebisoctadecanamide, 1-2 parts of an antioxidant 168, 5-7 parts of talcum powder, 3-4 parts of hollow fiber, 3-5 parts of a hollow ceramic powder, 12-16 parts of xylene and 4-7 parts of an additive. The paint of the invention has the advantages of excellent permeability, strong adhesive force, no cracking or spalling, long performance resistance time, and no color change, light loss or pulverization. The coating has good corrosion resistance, heat resistance, good mechanical strength, excellent protective performance and good decorative effect, can be irradiated by ultraviolet for a long term without damage, can be widely used in the outdoor power distribution cabinet body and shows substantial effect.
Description
Technical field
The present invention relates to a kind of paint and preparation method thereof, particularly a kind of Heat-resistance anti-corrosion paint and preparation method thereof.
Background technology
Coating, is called paint in Chinese tradition name.China's coating circle more authoritative " coating process " book is definition like this: " coating is a kind of material, and this material can be coated in article surface by different construction technologies, forms adhere well, has some strength, continuous print solid film.The film common name film of such formation, also known as paint film or coating." antifouling paste be for body surface can be used for protect interior of articles be not corroded one class paint.In recent years, mostly adopt industry anti-corrosion paint to protect the surface of the materials such as metal, make it from corrosion, work-ing life more lengthened.
Summary of the invention
The object of this invention is to provide a kind of Heat-resistance anti-corrosion paint and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of Heat-resistance anti-corrosion paint, is made up of the raw material of following weight part: resol 30-35, tetramethylsilane 1-3,200 ﹟ solvent oil 7-9, ground dolomite 3-5, bauxitic clay 3-5, sodium Diacetate 2-3, diglycollic amide 1-3, maleficent acid resin 23-26, aluminium triphosphate 2-4, methyl ethyl diketone selenium 2-3, ethylene group bis-stearamides 1-2, antioxidant 1681-2, talcum powder 5-7, hollow fiber 3-4, hollow ceramic powder 3-5, dimethylbenzene 12-16, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: calcium propionate 3-5, sulfuration oleic acid 1-2, hydrochloric acid wood oil 4-6, Silane coupling agent KH550 2-3, two ten four carbon alcohols ester 1-2, aluminum nitride powder 2-3, Sodium dehydroacetate 0.7-1.4, 2-amino-2-methyl-1-propanol 2-3, quaternary ammonium salt-modified organobentonite 2-3, tertbutyl peroxide 1-2, fatty alcohol-polyoxyethylene ether 1-2, vinyl acetate 5-8, vinylformic acid 3-5, ethanol 10-15, silver powder 3-4, expanded graphite 6-8, sheet cobalt powder 8-11, dilute sulphuric acid 0.4-0.8, preparation method is that sheet cobalt powder, silver powder, aluminum nitride powder, expanded graphite, ethanol, dilute sulphuric acid mix by (1), and temperature controls to react 20-30 minute at 70-80 ° of C, leaves standstill precipitation pressed powder for subsequent use, (2) product of hydrochloric acid wood oil, sulfuration oleic acid, vinyl acetate, vinylformic acid, fatty alcohol-polyoxyethylene ether and step (1) is mixed, carry out mechanical blending by high speed dispersion, then add tertbutyl peroxide stirring reaction 1-2 hour, (3) Silane coupling agent KH550 is added in the ethanol of 3-6 weight part, is sprayed onto after mixing on the product of step (2), then add all the other surplus materialss high speed dispersion 0.5-1 hour.
A kind of Heat-resistance anti-corrosion paint of the present invention, be made up of following concrete steps:
(1) ground dolomite, bauxitic clay, talcum powder, hollow fiber, hollow ceramic powder are added in the mixed solvent of 200 ﹟ solvent oils and dimethylbenzene, ultrasonic disperse 20-30 minute, adds antioxidant 168, auxiliary agent continues stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add resol, maleficent acid resin, methyl ethyl diketone selenium, ethylene group bis-stearamides, 1200-1400 rev/min of lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Advantage of the present invention is: coating of the present invention has superior penetrating quality, cohesive force is not strong, easy to crack, peel off, and resistance to light application time is long, loss of gloss efflorescence not easy to change, this coating not only has good heat-resisting, antiseptic property, also has good physical strength and barrier propterty, good decorating effect, can for a long time by the irradiation of UV-light, destroying does not appear in coating, can be widely used in the cabinet of outdoor change power distribution cabinet, Be very effective.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of Heat-resistance anti-corrosion paint, is made up of the raw material of following weight part (kilogram): resol 34, tetramethylsilane 2,200 ﹟ solvent oil 8, ground dolomite 4, bauxitic clay 3, sodium Diacetate 2, diglycollic amide 1, maleficent acid resin 25, aluminium triphosphate 3, methyl ethyl diketone selenium 2, ethylene group bis-stearamides 1, antioxidant 1681, talcum powder 5, hollow fiber 3, hollow ceramic powder 3, dimethylbenzene 14, auxiliary agent 4;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): calcium propionate 5, sulfuration oleic acid 2, hydrochloric acid wood oil 4, Silane coupling agent KH550 2, two ten four carbon alcohols esters 1, aluminum nitride powder 3, Sodium dehydroacetate 0.9,2-amino-2-methyl-1-propanol 2, quaternary ammonium salt-modified organobentonite 2, tertbutyl peroxide 1, fatty alcohol-polyoxyethylene ether 1, vinyl acetate 8, vinylformic acid 4, ethanol 14, silver powder 3, expanded graphite 7, sheet cobalt powder 9, dilute sulphuric acid 0.6; Preparation method is that sheet cobalt powder, silver powder, aluminum nitride powder, expanded graphite, ethanol, dilute sulphuric acid mix by (1), and temperature controls to react 20-30 minute at 70-80 ° of C, leaves standstill precipitation pressed powder for subsequent use; (2) product of hydrochloric acid wood oil, sulfuration oleic acid, vinyl acetate, vinylformic acid, fatty alcohol-polyoxyethylene ether and step (1) is mixed, carry out mechanical blending by high speed dispersion, then add tertbutyl peroxide stirring reaction 1-2 hour; (3) Silane coupling agent KH550 is added in the ethanol of 3-6 weight part, is sprayed onto after mixing on the product of step (2), then add all the other surplus materialss high speed dispersion 0.5-1 hour.
A kind of Heat-resistance anti-corrosion paint of the present invention, be made up of following concrete steps:
(1) ground dolomite, bauxitic clay, talcum powder, hollow fiber, hollow ceramic powder are added in the mixed solvent of 200 ﹟ solvent oils and dimethylbenzene, ultrasonic disperse 20-30 minute, adds antioxidant 168, auxiliary agent continues stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add resol, maleficent acid resin, methyl ethyl diketone selenium, ethylene group bis-stearamides, 1200-1400 rev/min of lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Paint paint film of the present invention is smooth, without lump, and hardness: 3H, sticking power: 1 grade, thermotolerance experiment (300 ° of C, 120h): paint film is complete, do not come off, alkali resistance experiment (72h): non-foaming, wrinkle resistant, do not come off, acid resistance experiment (72h): non-foaming, wrinkle resistant, does not come off, artificial ageing resistance is tested: 1500h is non-foaming, do not peel off, flawless, and electromagnetic shielding rate is tested: 42dB.
Claims (2)
1. a Heat-resistance anti-corrosion paint, it is characterized in that, be made up of the raw material of following weight part: resol 30-35, tetramethylsilane 1-3,200 ﹟ solvent oil 7-9, ground dolomite 3-5, bauxitic clay 3-5, sodium Diacetate 2-3, diglycollic amide 1-3, maleficent acid resin 23-26, aluminium triphosphate 2-4, methyl ethyl diketone selenium 2-3, ethylene group bis-stearamides 1-2, antioxidant 1681-2, talcum powder 5-7, hollow fiber 3-4, hollow ceramic powder 3-5, dimethylbenzene 12-16, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: calcium propionate 3-5, sulfuration oleic acid 1-2, hydrochloric acid wood oil 4-6, Silane coupling agent KH550 2-3, two ten four carbon alcohols ester 1-2, aluminum nitride powder 2-3, Sodium dehydroacetate 0.7-1.4, 2-amino-2-methyl-1-propanol 2-3, quaternary ammonium salt-modified organobentonite 2-3, tertbutyl peroxide 1-2, fatty alcohol-polyoxyethylene ether 1-2, vinyl acetate 5-8, vinylformic acid 3-5, ethanol 10-15, silver powder 3-4, expanded graphite 6-8, sheet cobalt powder 8-11, dilute sulphuric acid 0.4-0.8, preparation method is that sheet cobalt powder, silver powder, aluminum nitride powder, expanded graphite, ethanol, dilute sulphuric acid mix by (1), and temperature controls to react 20-30 minute at 70-80 ° of C, leaves standstill precipitation pressed powder for subsequent use, (2) product of hydrochloric acid wood oil, sulfuration oleic acid, vinyl acetate, vinylformic acid, fatty alcohol-polyoxyethylene ether and step (1) is mixed, carry out mechanical blending by high speed dispersion, then add tertbutyl peroxide stirring reaction 1-2 hour, (3) Silane coupling agent KH550 is added in the ethanol of 3-6 weight part, is sprayed onto after mixing on the product of step (2), then add all the other surplus materialss high speed dispersion 0.5-1 hour.
2. a kind of Heat-resistance anti-corrosion paint according to claim 1, is characterized in that, be made up of following concrete steps:
(1) ground dolomite, bauxitic clay, talcum powder, hollow fiber, hollow ceramic powder are added in the mixed solvent of 200 ﹟ solvent oils and dimethylbenzene, ultrasonic disperse 20-30 minute, adds antioxidant 168, auxiliary agent continues stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add resol, maleficent acid resin, methyl ethyl diketone selenium, ethylene group bis-stearamides, 1200-1400 rev/min of lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410671698.XA CN104497780A (en) | 2014-11-21 | 2014-11-21 | Heat resistant anticorrosive paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410671698.XA CN104497780A (en) | 2014-11-21 | 2014-11-21 | Heat resistant anticorrosive paint and preparation method thereof |
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| CN104497780A true CN104497780A (en) | 2015-04-08 |
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| CN201410671698.XA Pending CN104497780A (en) | 2014-11-21 | 2014-11-21 | Heat resistant anticorrosive paint and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105349015A (en) * | 2015-12-08 | 2016-02-24 | 常熟市裕茗企业管理咨询有限公司 | Device for monitoring environmental noise |
| CN106048215A (en) * | 2016-06-05 | 2016-10-26 | 扬州派德粉末冶金有限公司 | Preparation method of metallurgical adhesive |
| CN106752196A (en) * | 2016-12-01 | 2017-05-31 | 浙江汉农建设有限公司 | The pillar of building in the style of the ancients |
| CN114316842A (en) * | 2022-01-13 | 2022-04-12 | 东莞市刚刚好玩具有限公司 | Spray glue for handheld model and preparation method and spray process thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051376A (en) * | 1989-11-01 | 1991-05-15 | 崔殿华 | Anti-rust oil with colour hard film |
| CN101265377A (en) * | 2008-05-13 | 2008-09-17 | 福建师范大学 | Method for preparing environment-friendly type ink preparing oil used for hectograph |
| CN101838489A (en) * | 2010-05-31 | 2010-09-22 | 刘昆虎 | Undersurface syncretic anti-corrosion paint |
| CN103602208A (en) * | 2013-10-10 | 2014-02-26 | 安徽真信涂料有限公司 | High-temperature-resistant flame-retardant rust-resisting paint and preparation method thereof |
| CN103694843A (en) * | 2013-11-29 | 2014-04-02 | 安徽祈艾特电子科技有限公司 | Environment-friendly anticorrosive yellowing-resistant amino resin paint |
-
2014
- 2014-11-21 CN CN201410671698.XA patent/CN104497780A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051376A (en) * | 1989-11-01 | 1991-05-15 | 崔殿华 | Anti-rust oil with colour hard film |
| CN101265377A (en) * | 2008-05-13 | 2008-09-17 | 福建师范大学 | Method for preparing environment-friendly type ink preparing oil used for hectograph |
| CN101838489A (en) * | 2010-05-31 | 2010-09-22 | 刘昆虎 | Undersurface syncretic anti-corrosion paint |
| CN103602208A (en) * | 2013-10-10 | 2014-02-26 | 安徽真信涂料有限公司 | High-temperature-resistant flame-retardant rust-resisting paint and preparation method thereof |
| CN103694843A (en) * | 2013-11-29 | 2014-04-02 | 安徽祈艾特电子科技有限公司 | Environment-friendly anticorrosive yellowing-resistant amino resin paint |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105349015A (en) * | 2015-12-08 | 2016-02-24 | 常熟市裕茗企业管理咨询有限公司 | Device for monitoring environmental noise |
| CN106048215A (en) * | 2016-06-05 | 2016-10-26 | 扬州派德粉末冶金有限公司 | Preparation method of metallurgical adhesive |
| CN106752196A (en) * | 2016-12-01 | 2017-05-31 | 浙江汉农建设有限公司 | The pillar of building in the style of the ancients |
| CN114316842A (en) * | 2022-01-13 | 2022-04-12 | 东莞市刚刚好玩具有限公司 | Spray glue for handheld model and preparation method and spray process thereof |
| CN114316842B (en) * | 2022-01-13 | 2023-05-26 | 东莞市刚刚好玩具有限公司 | Spraying adhesive for hand models, preparation method thereof and spraying process |
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Application publication date: 20150408 |
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