CN104497673A - Paint pigment containing graphene and preparation method of paint pigment - Google Patents
Paint pigment containing graphene and preparation method of paint pigment Download PDFInfo
- Publication number
- CN104497673A CN104497673A CN201410814178.XA CN201410814178A CN104497673A CN 104497673 A CN104497673 A CN 104497673A CN 201410814178 A CN201410814178 A CN 201410814178A CN 104497673 A CN104497673 A CN 104497673A
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- oil
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses paint pigment containing graphene. The paint pigment is prepared from the following components in parts by weight: 20-35 parts of refined sunflower seed oil, 2-5 parts of printing ink adjusting oil, 5-20 parts of pigment color powder, 15-35 parts of barium sulfate, 5-10 parts of kaolin, 0.5-5 parts of graphene, 3-10 parts of nano silicon dioxide, 2-8 parts of refined linseed oil, 0.1-1.5 parts of aluminum stearate, 0.2-1.5 parts of bee wax, 0.5-2.0 parts of 422 glyceride maleic anhydride resin and 0.2-2 parts of BCM anti-mold agent. The paint pigment has the beneficial effects that firstly, due to addition of graphene, the paint pigment has good anti-electrostatic property, dust adsorption is avoided, and the friction property, the hardness and the adhesion property of the paint pigment are improved; secondly, due to addition of nano silicon dioxide, the antibacterial effect of the pigment is improved, the ultraviolet resistance is good, the aging resistance of the paint pigment is remarkably improved, and a drawing paint completed by using the paint pigment can be preserved for a relatively long time.
Description
Technical field
The invention belongs to oil colour field, be specifically related to a kind of oil colour of graphene-containing; The invention still further relates to the preparation method of the oil colour of this graphene-containing.
Background technology
Current pigment mainly includes watercolors, gouache color, oil colour, acrylic paints etc.; The basal component of oil colour the same with other drawing pigment by colorant, pigment extender, vehicle and some auxiliary material as plastotype agent, stablizer, slow dry agent or siccative etc. are formed.The various performances of oil colour can need by using different catalytic agent and subsidiary material to come suitably to be adjusted according to difference.
The quality of oil colour quality can have a huge impact the performance of painting skill, is also one of prerequisite determining paint life-span length.In recent years, along with the development of drawing industry, the requirement of people to oil colour is also more and more higher.The performances such as the tinting strength of oil colour, resistance to luminous power, opacifying power, transparency, oil number, toughness, ridity, plasticity-and levelling property some directly affect the effect of drawing a picture.
After using oil colour to complete works, usual needs dry for a long time, in the process; due to the electrostatic effect on picture; usually can adsorb some dusts or tiny hair, and be infiltrated storage by the oiliness surface permanent of picture, this have impact on the quality of oil painting largely.
In addition, oil colour progressively to high-end field development, domestic and international market total scale reaches multi-million dollar, and this also has higher requirement to the antistatic property of oil colour, ageing resistance, sticking power and resistance to cracking.
Summary of the invention
For deficiency of the prior art, an object of the present invention is to provide a kind of oil colour of graphene-containing, has good glossiness and antistatic property.Two of object of the present invention is to provide the preparation method of the oil colour of this graphene-containing.
The present invention is achieved through the following technical solutions.
An oil colour for graphene-containing, this oil colour comprises following component and weight proportion thereof: refining sunflower seed oil 20 ~ 35 parts; Printing stand linseed oil 2 ~ 5 parts; Pigment toner 5 ~ 20 parts; 15 ~ 35 parts, barium sulfate; Kaolin 5 ~ 10 parts; Graphene 0.5 ~ 5 part; Nano silicon 3 ~ 10 parts; Refining oleum lini 2 ~ 8 parts; Aluminum stearate 0.1 ~ 1.5 part; 0.2 ~ 1.5 part, beeswax; 422 maleficent acid resins 0.5 ~ 2.0 part; BCM mould inhibitor 0.2 ~ 2 part.
Graphene has the microtexture of sheet, and this structure makes electronics can conduct in the two-dimensional space of Graphene, and therefore Graphene has good conductivity, can be considered desirable conductive agent.In size and geometry, carbon black, carbon nanotube and Graphene can regard point, line, surface as abstractively, and they are inevitable different from the conductive contact interface of electrode active material.Obviously, the contact area between Graphene and active substance will significantly be greater than carbon nanotube and carbon black, and therefore for raising electric conductivity, comparatively carbon nanotube and carbon black be advantageously.
The interpolation of Graphene significantly can improve conductivity and the antistatic property of pigment, makes oil not easily attract dust, also can improve the performance index such as the rub resistance ability of pigment, hardness and sticking power.
Nano silicon has physiological inertia, high absorbability, carrier is commonly used in the preparation of sterilant, when nano silicon makes carrier, adsorbable antibacterial ion, reach the object that sterilization is antibacterial, in the present invention, nano silicon coordinates the use of BCM mould inhibitor, and anti-mold effect can be made more lasting, be convenient to the long-term preservation of paintings, especially in the environment of some warm moist.In addition, the specific surface area of nano silicon is large, porosity is high, Active sites is many containing a large amount of hydroxyls and unsaturated residual bond, has good lubrication, can improve feel when drawing a picture.And nano silicon, as the lower-cost filler auxiliary agent of one, has extremely strong uv-absorbing, infrared external reflection characteristic.Show through ultraviolet-visible spectrophotometer test, it to the uv absorption rate within wavelength 400nm up to more than 70%, also more than 70% is reached to the infrared reflectivity beyond wavelength 800nm, therefore, be added with the ageing-resistant performance that nano silicon can significantly improve oil colour in this pigment, the paint longer-term enable is preserved.
The interpolation of 422 maleficent acid resins, can make oil colour fast drying, and dried paintings are hard, bright, not yellowing, alkaline-resisting, water-fast, resistance to gasoline, good stability.
The applicant, on the basis of many experiments, by adjusting component proportion further, drawing preferred component formula, having following component and weight proportion thereof: refining sunflower seed oil 28 ~ 30 parts; Printing stand linseed oil 3.5 ~ 4 parts; Pigment toner 11 ~ 13 parts; 24 ~ 26 parts, barium sulfate; Kaolin 7 ~ 9 parts; Graphene 2 ~ 3 parts; Nano silicon 7 ~ 8 parts; Refining oleum lini 4 ~ 5 parts; Aluminum stearate 0.7 ~ 1 part; 0.7 ~ 1.4 part, beeswax; 422 maleficent acid resins 0.8 ~ 1.5 part; BCM mould inhibitor 1 ~ 1.5 part.
The invention still further relates to a kind of oil colour preparation method of graphene-containing, comprise the following steps: a. gets the beeswax, aluminum stearate and the refining Semen Lini oil that meet composition weight proportioning and carries out blended, heating and melting, obtains freezing oily A; B. get the 422 maleficent acid resins that meet composition weight proportioning and refining Semen Lini oil carries out blended, heating and melting, obtain gloss varnish B; C. getting all the other components meeting weight proportion, together with freezing oily A and gloss varnish B carries out blended, obtaining finished product through grinding.
In step of the present invention, adopt the mode of component raw material melt blending in batches, improve mixed effect, be convenient to the dispersed of raw material.
As preferably, in described step a, the weight ratio of beeswax, aluminum stearate and refining Semen Lini oil is 2:1:2; In described step b, the weight ratio of 422 maleficent acid resins and refining Semen Lini oil is 1:4.
Compared with prior art, the present invention has following beneficial effect: 1) be added with Graphene, has good antistatic property, prevents attract dust, improves the rub resistance ability of oil colour, hardness and sticking power; 2) be added with nano silicon, can improve the antibacterial effect of pigment, and have good uvioresistant ability, can significantly improve the ageing-resistant performance of oil colour, the paint longer-term enable is preserved.
Embodiment
Below in conjunction with embodiment, the present invention is described further.Be below component and the weight proportion of embodiment 1 to embodiment 7.
Embodiment 1: refining sunflower seed oil 30 parts; Printing stand linseed oil 5 parts; Pigment toner 20 parts; 26 parts, barium sulfate; Kaolin 5 parts; Graphene 2 parts; Nano silicon 7 parts; Refining oleum lini 2 parts; Aluminum stearate 1.5 parts; 0.7 part, beeswax; 422 maleficent acid resins 0.5 part; BCM mould inhibitor 0.3 part.
Embodiment 2: refining sunflower seed oil 20 parts; Printing stand linseed oil 5 parts; Pigment toner 20 parts; 35 parts, barium sulfate; Kaolin 5 parts; Graphene 5 parts; Nano silicon 3 parts; Refining oleum lini 2 parts; Aluminum stearate 0.7 part; 1.5 parts, beeswax; 422 maleficent acid resins 0.8 part; BCM mould inhibitor 2 parts.
Embodiment 3: refining sunflower seed oil 35 parts; Printing stand linseed oil 2 parts; Pigment toner 13 parts; 15 parts, barium sulfate; Kaolin 10 parts; Graphene 3 parts; Nano silicon 10 parts; Refining oleum lini 8 parts; Aluminum stearate 0.8 part; 1.2 parts, beeswax; 422 maleficent acid resins 0.5 part; BCM mould inhibitor 1.5 parts.
Embodiment 4: refining sunflower seed oil 28 parts; Printing stand linseed oil 3.5 parts; Pigment toner 13 parts; 26 parts, barium sulfate; Kaolin 9 parts; Graphene 0.5 part; Nano silicon 10 parts; Refining oleum lini 5 parts; Aluminum stearate 1 part; 0.1 part, beeswax; 422 maleficent acid resins 2 parts; BCM mould inhibitor 1.9 parts.
Embodiment 5: refining sunflower seed oil 34 parts; Printing stand linseed oil 4 parts; Pigment toner 11 parts; 24 parts, barium sulfate; Kaolin 7 parts; Graphene 5 parts; Nano silicon 8 parts; Refining oleum lini 4 parts; Aluminum stearate 0.1 part; 0.4 part, beeswax; 422 maleficent acid resins 1.5 parts; BCM mould inhibitor 1 part.
Embodiment 6: refining sunflower seed oil 35 parts; Printing stand linseed oil 5 parts; Pigment toner 5 parts; 30 parts, barium sulfate; Kaolin 7 parts; Graphene 4 parts; Nano silicon 7 parts; Refining oleum lini 4 parts; Aluminum stearate 1 part; 1 part, beeswax; 422 maleficent acid resins 0.8 part; BCM mould inhibitor 0.2 part.
Embodiment 7: refining sunflower seed oil 30 parts; Printing stand linseed oil 3.8 parts; Pigment toner 13 parts; 26 parts, barium sulfate; Kaolin 9 parts; Graphene 3 parts; Nano silicon 7 parts; Refining oleum lini 4.2 parts; Aluminum stearate 0.7 part; 1.4 parts, beeswax; 422 maleficent acid resins 0.7 part; BCM mould inhibitor 1.2 parts.
The component of Example 1 to embodiment 7, carries out following operation: beeswax, aluminum stearate and refining Semen Lini oil are carried out blended, heating and melting by a., obtains freezing oily A respectively; B. 422 maleficent acid resins and refining Semen Lini oil are carried out blended, heating and melting, obtain gloss varnish B; C. will freeze oily A, gloss varnish B and all the other components carries out blended, obtains finished product through grinding.
In above embodiment, Graphene is purchased from Ningbo Mo Xi Science and Technology Ltd., and nano silicon particle diameter is between 40nm ~ 60nm.
The performance test of the oil colour prepared by embodiment 1 ~ 7 is as follows:
The performance test results as can be seen from table, oil colour of the present invention has good electroconductibility and wear resisting property, and anti-mildew.
Protection scope of the present invention includes but not limited to above embodiment, and protection scope of the present invention is as the criterion with claims, and any replacement that those skilled in the art will find apparent that, distortion, improvement made this technology all falls into protection scope of the present invention.
Claims (4)
1. an oil colour for graphene-containing, is characterized in that, this oil colour comprises following component and weight proportion thereof: refining sunflower seed oil 20 ~ 35 parts; Printing stand linseed oil 2 ~ 5 parts; Pigment toner 5 ~ 20 parts; 15 ~ 35 parts, barium sulfate; Kaolin 5 ~ 10 parts; Graphene 0.5 ~ 5 part; Nano silicon 3 ~ 10 parts; Refining oleum lini 2 ~ 8 parts; Aluminum stearate 0.1 ~ 1.5 part; 0.2 ~ 1.5 part, beeswax; 422 maleficent acid resins 0.5 ~ 2.0 part; BCM mould inhibitor 0.2 ~ 2 part.
2. the oil colour of a kind of graphene-containing according to claim 1, is characterized in that, this oil colour comprises following component and weight proportion thereof: refining sunflower seed oil 28 ~ 30 parts; Printing stand linseed oil 3.5 ~ 4 parts; Pigment toner 11 ~ 13 parts; 24 ~ 26 parts, barium sulfate; Kaolin 7 ~ 9 parts; Graphene 2 ~ 3 parts; Nano silicon 7 ~ 8 parts; Refining oleum lini 4 ~ 5 parts; Aluminum stearate 0.7 ~ 1 part; 0.7 ~ 1.4 part, beeswax; 422 maleficent acid resins 0.8 ~ 1.5 part; BCM mould inhibitor 1 ~ 1.5 part.
3. the oil colour preparation method of a kind of graphene-containing described in any one of the claims, it is characterized in that, comprise the following steps: a. gets the beeswax, aluminum stearate and the refining Semen Lini oil that meet composition weight proportioning and carries out blended, heating and melting, obtains freezing oily A; B. get the 422 maleficent acid resins that meet composition weight proportioning and refining Semen Lini oil carries out blended, heating and melting, obtain gloss varnish B; C. getting all the other components meeting weight proportion, together with freezing oily A and gloss varnish B carries out blended, obtaining finished product through grinding.
4. the oil colour preparation method of a kind of graphene-containing according to claim 3, is characterized in that, in described step a, the weight ratio of beeswax, aluminum stearate and refining Semen Lini oil is 2:1:2; In described step b, the weight ratio of 422 maleficent acid resins and refining Semen Lini oil is 1:4.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410814178.XA CN104497673B (en) | 2014-12-23 | 2014-12-23 | A kind of oil colour of graphene-containing |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410814178.XA CN104497673B (en) | 2014-12-23 | 2014-12-23 | A kind of oil colour of graphene-containing |
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| CN104497673A true CN104497673A (en) | 2015-04-08 |
| CN104497673B CN104497673B (en) | 2017-11-24 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106957551A (en) * | 2017-05-11 | 2017-07-18 | 台州瑞祥教育科技有限公司 | A kind of oil colour of quick-drying freedom from cracking and preparation method thereof |
| CN108034355A (en) * | 2018-01-15 | 2018-05-15 | 傅雨菲 | A kind of blueness oil painting composite pigment and its preparation method and application |
| CN108192400A (en) * | 2017-12-19 | 2018-06-22 | 宋吕阳光 | A kind of pigment of drawing and preparation method thereof |
| CN111393916A (en) * | 2020-05-25 | 2020-07-10 | 苏州德加画材科技有限公司 | Antistatic aging-resistant oil painting pigment |
| CN111925679A (en) * | 2020-08-20 | 2020-11-13 | 新乡学院 | Oil painting pigment for fine arts |
| CN111944345A (en) * | 2020-08-24 | 2020-11-17 | 天长市嘉丰美术用品有限公司 | High-color-rendering oil painting pigment and production process thereof |
| CN112646404A (en) * | 2020-12-29 | 2021-04-13 | 盐城工业职业技术学院 | Antibacterial pigment and preparation method thereof |
| CN115725208A (en) * | 2021-08-30 | 2023-03-03 | 福建波普画材科技有限公司 | Pigment for art painting and preparation method thereof |
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| CN1955234A (en) * | 2005-10-25 | 2007-05-02 | 樊官保 | Photogravure ink equal to cut ink and its application |
| CN104151903A (en) * | 2014-08-21 | 2014-11-19 | 宁波高新区康大美术新材料有限公司 | Graphene-containing high-luster propylene pigment and preparation method thereof |
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2014
- 2014-12-23 CN CN201410814178.XA patent/CN104497673B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1955234A (en) * | 2005-10-25 | 2007-05-02 | 樊官保 | Photogravure ink equal to cut ink and its application |
| CN104151903A (en) * | 2014-08-21 | 2014-11-19 | 宁波高新区康大美术新材料有限公司 | Graphene-containing high-luster propylene pigment and preparation method thereof |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106957551A (en) * | 2017-05-11 | 2017-07-18 | 台州瑞祥教育科技有限公司 | A kind of oil colour of quick-drying freedom from cracking and preparation method thereof |
| CN108192400A (en) * | 2017-12-19 | 2018-06-22 | 宋吕阳光 | A kind of pigment of drawing and preparation method thereof |
| CN108034355A (en) * | 2018-01-15 | 2018-05-15 | 傅雨菲 | A kind of blueness oil painting composite pigment and its preparation method and application |
| CN111393916A (en) * | 2020-05-25 | 2020-07-10 | 苏州德加画材科技有限公司 | Antistatic aging-resistant oil painting pigment |
| CN111925679A (en) * | 2020-08-20 | 2020-11-13 | 新乡学院 | Oil painting pigment for fine arts |
| CN111925679B (en) * | 2020-08-20 | 2021-08-17 | 新乡学院 | Oil painting pigment for fine arts |
| CN111944345A (en) * | 2020-08-24 | 2020-11-17 | 天长市嘉丰美术用品有限公司 | High-color-rendering oil painting pigment and production process thereof |
| CN112646404A (en) * | 2020-12-29 | 2021-04-13 | 盐城工业职业技术学院 | Antibacterial pigment and preparation method thereof |
| CN115725208A (en) * | 2021-08-30 | 2023-03-03 | 福建波普画材科技有限公司 | Pigment for art painting and preparation method thereof |
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| Publication number | Publication date |
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| CN104497673B (en) | 2017-11-24 |
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Effective date of registration: 20180205 Address after: The island Daxie Development Zone Road 315812 No. 291 Zhejiang city of Ningbo Province Patentee after: Ningbo Conda Art Supplies Group Co., Ltd. Address before: Room 401-4, room No. 5, Yang Fan Road, Ningbo hi tech Zone, Zhejiang, Zhejiang Patentee before: Ningbo High-tech Zone Kangda Art New Materials Co.,Ltd. |
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Address after: The island Daxie Development Zone Road 315812 No. 291 Zhejiang city of Ningbo Province Patentee after: Ningbo Kangda Art Painting Material Group Co.,Ltd. Address before: The island Daxie Development Zone Road 315812 No. 291 Zhejiang city of Ningbo Province Patentee before: CONDA (NINGBO) ART MATERIAL MFG Co.,Ltd. |
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