CN104492850A - Production method of high-finish steel tube - Google Patents

Production method of high-finish steel tube Download PDF

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Publication number
CN104492850A
CN104492850A CN201410720037.1A CN201410720037A CN104492850A CN 104492850 A CN104492850 A CN 104492850A CN 201410720037 A CN201410720037 A CN 201410720037A CN 104492850 A CN104492850 A CN 104492850A
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steel tube
production method
adjustment
heating
cold
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CN201410720037.1A
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CN104492850B (en
Inventor
吕黎红
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Vallourec Tianda Anhui Co Ltd
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Anhui Tianda Oil Pipe Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/06Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of tubes or metal hoses; Combined procedures for making tubes, e.g. for making multi-wall tubes
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23FNON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
    • C23F17/00Multi-step processes for surface treatment of metallic material involving at least one process provided for in class C23 and at least one process covered by subclass C21D or C22F or class C25

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatment Of Articles (AREA)
  • Heat Treatment Of Steel (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

The invention discloses a production method of a high-finish steel tube. A 38*3mm round billet used in the production method is made of 20# steel. The production method comprises the following steps: heating billet: heating the round billet (phi 50mm) which passes the inspection in an annular heating furnace at 1200 DEG C+/-10 DEG C, holding the temperature for 50+/-5min and tapping; punching: selecting a mandrel plug (phi 50mm) and an ejector rod ((phi 38mm), adjusting the distance of a roller of a puncher to be 40mm, the spacing of guide plates to be 48mm, the extend distance of the mandrel plug to be 31mm and rolling reduction to be 16% and adjusting other parameters, then punching, wherein the punched capillaries have the specification of phi 52*4mm. The production method has the advantages that the surface quality of the steel tube is guaranteed; the surface of the produced steel tube is smooth and high in finish and is identical to the surface of a bright steel tube without being subjected to oxidization thermal treatment and moreover the property of the steel tube is not affected; in addition, the production cost is reduced greatly.

Description

A kind of production method of best bright finish steel pipe
Technical field
The present invention relates to steel pipe's production field, specifically belong to a kind of production method of best bright finish steel pipe.
Background technology
Along with the development of modern technologies, more and more higher to the surface quality requirements of steel pipe.Particularly some steamless steel pipe for heat exchangers, propose very high requirement to steel tube surface fineness.After traditional solid drawn tube finished product heat treatment, oxidation is serious.And adopting non-oxidizing bright heat treatment, equipment cost is high, technical sophistication.
Summary of the invention
The object of this invention is to provide a kind of production method of best bright finish steel pipe, solve and do not using under the heat treated condition of non-oxidizing bright, make steel tube surface reach the requirement of best bright finish.Neither increase cost, reach the instructions for use of steel pipe simultaneously.
Technical scheme of the present invention is as follows:
A production method for best bright finish steel pipe, select material to be No. 20 steel, be of a size of the circular pipe blank of 38 × 3mm, include following operating procedure:
1, heating of pipe blank: φ 50mm circular pipe blank is through after the assay was approved, and circular pipe blank is sent into rotary heating furnace heating, heating-up temperature is 1200 DEG C ± 10 DEG C, is incubated after 50 ± 5 minutes and taps;
2, bore a hole: select φ 40mm top, φ 38mm push rod, adjustment piercer roll distance is the laggard eleven punch 11s of parameter such as 40mm, guide plate spacing 48mm, top head front-extending quantity 31mm, drafts 16%, and pierced shell is φ 52 × 4mm;
3, pickling, phosphatization, saponification: in adjustment pickle, sulfuric acid concentration is between 9% ~ 15%, Fe 2+≤ 200g/L, pickle temperature remains between 30 DEG C ~ 65 DEG C, by the pickling of φ 52 × 4mm hollow billet, cylinder is played after soaking 15min, rinse well with clear water, in adjustment Phosphating Solution, total acidity is between 16mol/L ~ 28mol/L, free acid is between 0.1mol/L ~ 1.0mol/L, Phosphating Solution temperature keeps 50 DEG C ~ 70 DEG C, by hollow billet phosphatization clean for pickling afterflush, cylinder is played after phosphating time 10 ~ 15min, rinse with clear water again, content of fatty acid>=1.0BN in adjustment saponification liquor, temperature is between 60 DEG C ~ 80 DEG C, by the hollow billet saponification after phosphatization, cylinder is played after saponification time 5min ~ 8min,
4, cold-drawn: select the external mold of φ 38mm and the internal mold of φ 32mm, carry out draw at the Drawing Force being no less than 36 tons, draw goes out φ 38 × 3mm hollow forging;
5, heat treatment: the normalized treatment of the φ 38 × 3mm hollow forging after cold-drawn being carried out 900 DEG C ± 10 DEG C, temperature retention time 20 ~ 30 minutes, air cooling;
6, again select φ 38mm external mold after hollow forging heat treatment, φ 32mm internal mold carries out indeformable cold-drawn, and Drawing Force is not less than 10 tons.This time draw does not change steel pipe sizes size, utilizes the interior epipolar restriction of cold drawing die to carry out oxide skin cleaning, makes steel tube surface smooth, highly polished, and do not change steel tube performance;
7, align: the production tube after heat treatment is carried out straightening processing, action≤0.2% total length after aligning; ≤ 1.5mm is bent apart from pipe end every meter;
8, cut: according to technological specification adjustment cutting machine, as requested steel pipe is cut, after cutting, cut tiltedly≤1.6mm
9, inspection warehouse-in: according to specification, outward appearance is carried out to production tube, size tests, store.
Advantage of the present invention is as follows:
Adopt the production technology after improving, ensure that the surface quality of steel pipe, steel tube surface is smooth, highly polished, consistent with the heat treated steel tube surface of non-oxidizing bright, does not affect steel tube performance again.Greatly reduce production cost.Five, the technique after improving and traditional handicraft compare the technique after improvement increase after heat treatment together with indeformable cold-drawn, make steel tube surface smooth, highly polished, and do not change steel tube performance.Traditional production technology oxidation is serious, and surface quality is poor.And adopt non-oxidizing bright heat treatment, although steel tube surface quality is good, highly polished, because equipment manufacturing cost is high, heat treatment cost is high, causes production cost significantly to improve.
Detailed description of the invention
A production method for best bright finish steel pipe, select material to be No. 20 steel, be of a size of the circular pipe blank of 38 × 3mm, include following operating procedure:
1, heating of pipe blank: φ 50mm circular pipe blank is through after the assay was approved, and circular pipe blank is sent into rotary heating furnace heating, heating-up temperature is 1200 DEG C ± 10 DEG C, is incubated after 50 ± 5 minutes and taps;
2, bore a hole: select φ 40mm top, φ 38mm push rod, adjustment piercer roll distance is the laggard eleven punch 11s of parameter such as 40mm, guide plate spacing 48mm, top head front-extending quantity 31mm, drafts 16%, and pierced shell is φ 52 × 4mm;
3, pickling, phosphatization, saponification: in adjustment pickle, sulfuric acid concentration is between 9% ~ 15%, Fe 2+≤ 200g/L, pickle temperature remains between 30 DEG C ~ 65 DEG C, by the pickling of φ 52 × 4mm hollow billet, cylinder is played after soaking 15min, rinse well with clear water, in adjustment Phosphating Solution, total acidity is between 16mol/L ~ 28mol/L, free acid is between 0.1mol/L ~ 1.0mol/L, Phosphating Solution temperature keeps 50 DEG C ~ 70 DEG C, by hollow billet phosphatization clean for pickling afterflush, cylinder is played after phosphating time 10 ~ 15min, rinse with clear water again, content of fatty acid>=1.0BN in adjustment saponification liquor, temperature is between 60 DEG C ~ 80 DEG C, by the hollow billet saponification after phosphatization, cylinder is played after saponification time 5min ~ 8min,
4, cold-drawn: select the external mold of φ 38mm and the internal mold of φ 32mm, carry out draw at the Drawing Force being no less than 36 tons, draw goes out φ 38 × 3mm hollow forging;
5, heat treatment: the normalized treatment of the φ 38 × 3mm hollow forging after cold-drawn being carried out 900 DEG C ± 10 DEG C, temperature retention time 20 ~ 30 minutes, air cooling;
6, again select φ 38mm external mold after hollow forging heat treatment, φ 32mm internal mold carries out indeformable cold-drawn, and Drawing Force is not less than 10 tons.This time draw does not change steel pipe sizes size, utilizes the interior epipolar restriction of cold drawing die to carry out oxide skin cleaning, makes steel tube surface smooth, highly polished, and do not change steel tube performance;
7, align: the production tube after heat treatment is carried out straightening processing, action≤0.2% total length after aligning; ≤ 1.5mm is bent apart from pipe end every meter;
8, cut: according to technological specification adjustment cutting machine, as requested steel pipe is cut, after cutting, cut tiltedly≤1.6mm
9, inspection warehouse-in: according to specification, outward appearance is carried out to production tube, size tests, store.
After traditional production technology Steel Pipe Heat process, namely align, cut, check warehouse-in, steel pipe is due to heat-treatment oxidation effect, and surface exists oxide skin.And adopt the heat treatment of non-oxidizing bright heat-treatment furnace, although ensure that the surface quality of steel pipe, equipment manufacturing cost is high, and production cost significantly improves.Adopt the production technology after improving to carry out indeformable cold-drawn after heat treatment, do not change steel pipe sizes size, only only pass through outer mold in cold-drawn and carry out the cleaning of oxide skin, make steel tube surface smooth, highly polished.And steel tube performance does not change.
The steel tube performance contrast table (with grade of steel for 20, specification is 38x3mm is example) that traditional processing technology and present invention process are produced.

Claims (1)

1. a production method for best bright finish steel pipe, select material to be No. 20 steel, be of a size of the circular pipe blank of 38 × 3mm, it is characterized in that, include following operating procedure:
(1), heating of pipe blank: φ 50mm circular pipe blank is through after the assay was approved, and circular pipe blank is sent into rotary heating furnace heating, heating-up temperature is 1200 DEG C ± 10 DEG C, is incubated after 50 ± 5 minutes and taps;
(2), perforation: select φ 40mm top, φ 38mm push rod, adjustment piercer roll distance is the laggard eleven punch 11s of parameter such as 40mm, guide plate spacing 48mm, top head front-extending quantity 31mm, drafts 16%, and pierced shell is φ 52 × 4mm;
(3), pickling, phosphatization, saponification: in adjustment pickle, sulfuric acid concentration is between 9% ~ 15%, Fe 2+≤ 200g/L, pickle temperature remains between 30 DEG C ~ 65 DEG C, by the pickling of φ 52 × 4mm hollow billet, cylinder is played after soaking 15min, rinse well with clear water, in adjustment Phosphating Solution, total acidity is between the mol/L of 16mol/L ~ 28, free acid is between 0.1 mol/L ~ 1.0 mol/L, Phosphating Solution temperature keeps 50 DEG C ~ 70 DEG C, by hollow billet phosphatization clean for pickling afterflush, cylinder is played after phosphating time 10 ~ 15min, rinse with clear water again, content of fatty acid>=1.0BN in adjustment saponification liquor, temperature is between 60 DEG C ~ 80 DEG C, by the hollow billet saponification after phosphatization, cylinder is played after saponification time 5min ~ 8min,
(4), cold-drawn: select the external mold of φ 38mm and the internal mold of φ 32mm, carry out draw at the Drawing Force being no less than 36 tons, draw goes out φ 38 × 3mm hollow forging;
(5), heat treatment: the normalized treatment of the φ 38 × 3mm hollow forging after cold-drawn being carried out 900 DEG C ± 10 DEG C, temperature retention time 20 ~ 30 minutes, air cooling;
(6), φ 38mm external mold is again selected after hollow forging heat treatment, φ 32mm internal mold carries out indeformable cold-drawn, Drawing Force is not less than 10 tons, this time draw does not change steel pipe sizes size, the interior epipolar restriction of cold drawing die is utilized to carry out oxide skin cleaning, make steel tube surface smooth, highly polished, and do not change steel tube performance;
(7), align: the production tube after heat treatment is carried out straightening processing, action≤0.2% total length after aligning; ≤ 1.5mm is bent apart from pipe end every meter;
(8), cutting: according to technological specification adjustment cutting machine, as requested steel pipe is cut, cut tiltedly≤1.6mm after cutting;
(9), inspection warehouse-in: according to specification, outward appearance is carried out to production tube, size tests, store.
CN201410720037.1A 2014-12-02 2014-12-02 A kind of production method of best bright finish steel pipe Active CN104492850B (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105834234A (en) * 2016-03-29 2016-08-10 重庆钢铁(集团)有限责任公司 Two-pass continuous drawing method for producing cold-drawn steel pipe
CN105834237A (en) * 2016-03-29 2016-08-10 重庆钢铁(集团)有限责任公司 Pierced billet chemical treatment method for reducing frequency of cold drawing
CN106216950A (en) * 2016-07-29 2016-12-14 新昌县长城空调部件有限公司 Gas-fired kitchen pipeline manufacturing process
CN107520271A (en) * 2017-08-03 2017-12-29 常熟市异型钢管有限公司 The production technology of the special-shaped steel high pressure seamless pipe of waste heat boiler
CN108127003A (en) * 2017-12-06 2018-06-08 江苏银环精密钢管有限公司 A kind of manufacturing method of drilling tool 23CrNi3Mo steel alloy seamless pipes
CN109457098A (en) * 2018-12-28 2019-03-12 江苏建中新材料科技有限公司 A kind of process improving mild steel steel strength
CN109604342A (en) * 2018-11-14 2019-04-12 张家港华程特种材料股份有限公司 A kind of processing method of seamless steel pipe
CN111041404A (en) * 2019-12-09 2020-04-21 朗瑞(泰州)金属工具有限公司 Heat treatment method for steel pipe plug
CN113618408A (en) * 2021-08-06 2021-11-09 南京斯迈柯特种金属装备股份有限公司 Thick-wall alloy preparation and processing technology
CN115572894A (en) * 2022-09-08 2023-01-06 衢州垣发机械有限公司 Inner tube of automobile friction shock absorber and preparation process thereof

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JP2003311317A (en) * 2002-04-18 2003-11-05 Sumitomo Metal Ind Ltd Method for manufacturing seamless tube
CN101767114A (en) * 2009-12-23 2010-07-07 攀枝花新钢钒股份有限公司 Method for removing oxide skin in tube blank of seamless steel tube
CN102233365A (en) * 2011-07-11 2011-11-09 徐州市全球通精密钢管有限公司 Manufacturing process of small-diameter seamless steel tubes
CN102345035A (en) * 2010-07-30 2012-02-08 宝鸡市海鹏金属材料有限公司 Production process for titanium and nickel shape memory alloy material
CN203389984U (en) * 2013-07-30 2014-01-15 无锡大金高精度冷拔钢管有限公司 Special equipment for producing high-rigidity cold-drawn steel pipe
CN103691760A (en) * 2013-12-17 2014-04-02 上海奉贤钢管厂 Preparation process of stainless steel tube
CN103846304A (en) * 2012-11-28 2014-06-11 常州盛德无缝钢管有限公司 ND steel seamless steel pipe production process
CN103909111A (en) * 2014-03-27 2014-07-09 攀钢集团成都钢钒有限公司 Titanium alloy seamless tube and production method thereof

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Publication number Priority date Publication date Assignee Title
JP2003311317A (en) * 2002-04-18 2003-11-05 Sumitomo Metal Ind Ltd Method for manufacturing seamless tube
CN101767114A (en) * 2009-12-23 2010-07-07 攀枝花新钢钒股份有限公司 Method for removing oxide skin in tube blank of seamless steel tube
CN102345035A (en) * 2010-07-30 2012-02-08 宝鸡市海鹏金属材料有限公司 Production process for titanium and nickel shape memory alloy material
CN102233365A (en) * 2011-07-11 2011-11-09 徐州市全球通精密钢管有限公司 Manufacturing process of small-diameter seamless steel tubes
CN103846304A (en) * 2012-11-28 2014-06-11 常州盛德无缝钢管有限公司 ND steel seamless steel pipe production process
CN203389984U (en) * 2013-07-30 2014-01-15 无锡大金高精度冷拔钢管有限公司 Special equipment for producing high-rigidity cold-drawn steel pipe
CN103691760A (en) * 2013-12-17 2014-04-02 上海奉贤钢管厂 Preparation process of stainless steel tube
CN103909111A (en) * 2014-03-27 2014-07-09 攀钢集团成都钢钒有限公司 Titanium alloy seamless tube and production method thereof

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105834237A (en) * 2016-03-29 2016-08-10 重庆钢铁(集团)有限责任公司 Pierced billet chemical treatment method for reducing frequency of cold drawing
CN105834234A (en) * 2016-03-29 2016-08-10 重庆钢铁(集团)有限责任公司 Two-pass continuous drawing method for producing cold-drawn steel pipe
CN105834234B (en) * 2016-03-29 2018-01-16 重庆钢铁(集团)有限责任公司 A kind of method that two passage even pulls out production cold drawing steel tube
CN106216950B (en) * 2016-07-29 2018-11-16 新昌县长城空调部件股份有限公司 Gas-fired kitchen pipeline manufacturing process
CN106216950A (en) * 2016-07-29 2016-12-14 新昌县长城空调部件有限公司 Gas-fired kitchen pipeline manufacturing process
CN107520271A (en) * 2017-08-03 2017-12-29 常熟市异型钢管有限公司 The production technology of the special-shaped steel high pressure seamless pipe of waste heat boiler
CN108127003A (en) * 2017-12-06 2018-06-08 江苏银环精密钢管有限公司 A kind of manufacturing method of drilling tool 23CrNi3Mo steel alloy seamless pipes
CN109604342A (en) * 2018-11-14 2019-04-12 张家港华程特种材料股份有限公司 A kind of processing method of seamless steel pipe
CN109457098A (en) * 2018-12-28 2019-03-12 江苏建中新材料科技有限公司 A kind of process improving mild steel steel strength
CN111041404A (en) * 2019-12-09 2020-04-21 朗瑞(泰州)金属工具有限公司 Heat treatment method for steel pipe plug
CN111041404B (en) * 2019-12-09 2024-03-15 朗瑞(泰州)金属工具有限公司 Heat treatment method for steel pipe plug
CN113618408A (en) * 2021-08-06 2021-11-09 南京斯迈柯特种金属装备股份有限公司 Thick-wall alloy preparation and processing technology
CN113618408B (en) * 2021-08-06 2022-07-29 南京斯迈柯特种金属装备股份有限公司 Thick-wall alloy preparation and processing technology
CN115572894A (en) * 2022-09-08 2023-01-06 衢州垣发机械有限公司 Inner tube of automobile friction shock absorber and preparation process thereof

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