CN104490642B - Natural insect wax hair protection trichogen and preparation method thereof - Google Patents
Natural insect wax hair protection trichogen and preparation method thereof Download PDFInfo
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- CN104490642B CN104490642B CN201410666928.3A CN201410666928A CN104490642B CN 104490642 B CN104490642 B CN 104490642B CN 201410666928 A CN201410666928 A CN 201410666928A CN 104490642 B CN104490642 B CN 104490642B
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Abstract
The present invention discloses a kind of natural insect wax hair protection trichogen and preparation method thereof, includes the raw material of following masses part：10~50 parts of insect wax, 90~50 parts of camellia seed oil.Insect wax is ground into powder, under water bath condition, Inesct Wax is added in camellia seed oil, after insect wax is dissolved completely in camellia seed oil stirring be cooled to room temperature to get to hair protection trichogen.The pure natural property of the plant extracts such as raw material insect wax and camellia seed oil used in the present invention and its it is peculiar the effect of be complementary to one another, mutually promote, make it that there are Small side effects, the advantages such as safe, nontoxic, not carcinogenic compared with chemical synthesis preparation for baldness.And compared to similar natural medicine as hair restorer, inventive formulation is simple and clear, and preparing process is simple and easy to do.On the other hand, this is also for the first time by insect wax and camellia seed oil composite usage in preparation for baldness, expands the range of plant source hair tonic articles for use.The preparation for baldness of the present invention is verified by experiments with trichogenous effect.
Description
Technical field
The invention belongs to natural biological arts, are related to a kind of natural insect wax hair protection trichogen and preparation method thereof.
Background technology
Hair plays a very important role the appearance of people, it not only has the function of beauty and protection scalp, together
When can also reflect the health status of body interior.But with people's the accelerating rhythm of life, the pollution of ambient water quality and harmful
There is alopecia, bald phenomenon or even have been extended to young man and women group in the factors such as the discharge of substance, more and more people
Body, it is greatly inconvenient and worried to bring.Therefore, the research and development of preparation for baldness, by medical field and cosmetics circle
Very big attention.
At present, in the market hair tonic articles for use are multifarious, and wherein most is all the preparation for baldness of chemicals synthesis, this kind of
Preparation for baldness easily allows user to generate certain dependence to this preparation for baldness often there are larger side effect.Therefore,
As people gradually deepen the understanding of chemical synthesis preparation for baldness drawback, people start to pursue natural, green, nontoxic pair again again
The plant resources for acting on and having multiple physiological to act on.In recent years, develop plant resources active material, develop fully natural green without
The hair tonic articles for use of toxic side effect are had become as one of most active theme of preparation for baldness industry development, have also had much use day in the market
Preparation for baldness hair growth, but their most complicated components, preparing process are comparatively laborious from different perspectives made of right drug.
Insect wax is to be gregariousness to form through refined in the wax secreted on the plants such as Chinese ash branch bar by the male worm of wax insect, is me
The distinctive resource insect product of state.It is recorded according to history records, Chinese wax has certain trichogenous effect, has in hair tonic articles for use field
Potential application value.At present, it using the preparation for baldness and related manufacturing processes of insect wax development, has not been reported.
Invention content
To solve big side effect existing for existing preparation for baldness and complicated component, the problems such as preparing process is cumbersome, it is of the invention
Purpose is to develop the hair protection trichogen and its preparation side that a kind of fully natural green has no toxic side effect, process for preparation is simple and practicable
Method.
The present invention is realized by following technical proposal：A kind of natural insect wax hair protection trichogen, including following masses part
Raw material：
10~50 parts of insect wax, 90~50 parts of camellia seed oil.
Further, which further includes 10~40 parts of the root of Dahurain angelica, 15~20 parts of mulberries, 15~35 parts of Radix Ophiopogonis, arbor-vitae
10~30 parts of leaf, 20~40 parts of Semen sesami nigrum, 10~40 parts of cultivated land, one kind in 5~20 parts of the fruit of glossy privet or arbitrary several.
Another object of the present invention is to provide a kind of preparation method of natural insect wax hair protection trichogen, by following each
Step：
(1) by the material preparation of following mass parts：10~50 parts of insect wax, 90~50 parts of camellia seed oil；
(2) insect wax is ground into powder；
(3) under 65~93 DEG C of water bath conditions, Inesct Wax is added in camellia seed oil, treats that insect wax is dissolved completely in
Stirring is cooled to room temperature to get to hair protection trichogen after camellia seed oil.
Further, the raw material of step (1) further include 10~40 parts of the root of Dahurain angelica, 15~20 parts of mulberries, 15~35 parts of Radix Ophiopogonis,
10~30 parts of cacumen biotae, 20~40 parts of Semen sesami nigrum, 10~40 parts of cultivated land, one kind in 5~20 parts of the fruit of glossy privet or arbitrary several, and
Concentrate is made, then added in the hair protection trichogen of the step (3) in said components according to the following steps：
A, said components are ground into powder；
B, the powder of step A is extracted into 8~10h as solvent with absolute ethyl alcohol and obtains extracting solution, then by extracting solution into
Row concentration, obtains concentrate.
The insect wax is ground into 20~80 mesh powders.
The root of Dahurain angelica, mulberries, Radix Ophiopogonis, cacumen biotae, Semen sesami nigrum, cultivated land, ligustrum lucidum powder are broken into 20~80 mesh powders.
Gained hair protection trichogen is paste, suitable for closed preservation at normal temperatures.In use, hair protection trichogen is applied to root of hair
Skin surface.
Wherein, the root of Dahurain angelica：Nature and flavor：Acrid flavour, it is warm-natured；Return：Lung, spleen, stomach；With relieving exterior syndrome and dispelling cold, dispelling wind and arresting itching, promoting blood circulation row
The effect of purulence, myogenic pain relieving.Mulberries：Nature and flavor：It is sweet, sour, cold in nature；Return：Liver and kidney channel, the heart channel of Hang-Shaoyin；It with nourishing yin and nourishing blood, promotes the production of body fluid, moistens
The effect of intestines, is cured mainly because what kidney deficiency and liver and deficiency of blood essence were lost has a dizzy spell, soreness of waist tinnitus, poliosis, insomnia and dreamful sleep, Tianjin wound
Yearningly, it quenches one's thirst, dry constipation of intestines.Radix Ophiopogonis：Nature and flavor：Sweet, slight bitter is slightly cold；Return：The heart, lung, stomach；With nourishing Yin and promoting production of body fluid, moistening lung clears away heart-fire
Effect cures mainly dryness of the lung dry cough, cough for deficiency of Yin consumptive disease, larynx numbness pharyngalgia, injury thirst, Heat Diabetes, vexed insomnia, dry constipation of intestines.Arbor-vitae
Leaf：Nature and flavor：Bitterness is trembled with fear；Return：The heart, liver, large intestine channel；With cool blood, hemostasis, wind-damp dispelling dissipates pyogenic infections and other effects, cures mainly haematemesis, nosebleed
Blood, hematuria, bloody flux, intestines wind, uterine bleeding, arthralgia pain due to rheumatism, bacillary dysentery, hypertension, cough, erysipelas, mumps, scald.Semen sesami nigrum：
Nature and flavor：Sweet and neutral；Return liver, kidney, large intestine channel；With filling liver kidney, the effect of benefiting essence-blood, ease constipation is dry；For dizzy, tinnitus ear
It is deaf, poliosis, post disease alopecia, dry constipation of intestines.Cultivated land：Nature and flavor：Sweet, warm；Return：Liver Channel, kidney channel；With enrich blood moist, strengthening the essence
The effect of filling out marrow.The fruit of glossy privet：Nature and flavor：It is sweet, bitter, it is cool in nature；Return：Liver, kidney channel；Effect：It tonifies the liver and kidney, crow must improving eyesight；For liver kidney
The deficiency of Yin, soreness of waist tinnitus, poliosis；Unseeing, poor vision；Fever due to yin deficiency, stomach trouble and gout and and hyperuricemia.
In the formula of the present invention, Chinese wax has trichogenous effect；Unsaturated fatty acid content in camellia seed oil
Up to 90%, containing abundant vitamin A, E, D, K and other antioxidants, it can play a very good protection, make to hair
Hair is smooth shiny black, is easy to arrange, and has potential application value in terms of hair care.Alopecia is generally acknowledged to lose with the human body kidney deficiency of blood
Related, mulberries, Radix Ophiopogonis, cacumen biotae, Semen sesami nigrum, cultivated land, the fruit of glossy privet, root of Dahurain angelica etc. are mainly that filling liver kidney, benefiting essence-blood or kidney tonifying are cool
Blood class drug has good controlling nocturnal emission with astringent drugs to act on, and controlling nocturnal emission with astringent drugs is then conducive to hair tonic, in addition, also having the function of certain black hair hair care.
It is of the invention that there are following advantages compared with existing preparation for baldness：Raw material insect wax and camellia seed oil used in the present invention
Wait plant extracts pure natural property and its it is peculiar the effect of be complementary to one another, mutually promote, make its compared with chemical synthesis preparation for baldness have
There are the advantages such as Small side effects, safe, nontoxic, not carcinogenic.And compared to similar natural medicine as hair restorer, the present invention
It is formulated simple and clear, preparing process is simple and easy to do.On the other hand, this is also that insect wax and camellia seed oil composite usage exist for the first time
In preparation for baldness, the range of plant source hair tonic articles for use is expanded.The preparation for baldness of the present invention is verified by experiments with promotion hair growth
Effect.
Specific embodiment
Below by embodiment, the present invention will be further described.
Embodiment 1
(1) by the material preparation of following mass parts：20 parts of insect wax, 80 parts of camellia seed oil；
(2) insect wax is ground into 20 mesh powders；
(3) under 65 DEG C of water bath conditions, Inesct Wax is added in camellia seed oil, treats that insect wax is dissolved completely in oil tea
Stirring is cooled to room temperature to get to hair protection trichogen after seed oil.
Embodiment 2
(1) by the material preparation of following mass parts：30 parts of insect wax, 70 parts of camellia seed oil；
(2) insect wax is ground into 40 mesh powders；
(3) it stocks up by following mass parts：10 parts of the root of Dahurain angelica, mulberries 20 parts, 30 parts of Semen sesami nigrum, and said components are ground into
40 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
10h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 75 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
Embodiment 3
(1) by the material preparation of following mass parts：50 parts of insect wax, 50 parts of camellia seed oil；
(2) insect wax is ground into 60 mesh powders；
(3) it stocks up by following mass parts：35 parts of Radix Ophiopogonis, 20 parts of cacumen biotae, and said components are ground into 20 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
9h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 93 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
Embodiment 4
(1) by the material preparation of following mass parts：10 parts of insect wax, 90 parts of camellia seed oil；
(2) insect wax is ground into 60 mesh powders；
(3) it stocks up by following mass parts：40 parts of the root of Dahurain angelica, and said components are ground into 60 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
8h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 80 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
Embodiment 5
(1) by the material preparation of following mass parts：20 parts of insect wax, 80 parts of camellia seed oil；
(2) insect wax is ground into 40 mesh powders；
(3) it stocks up by following mass parts：30 parts of the root of Dahurain angelica, 15 parts of mulberries, 25 parts of Radix Ophiopogonis, 30 parts of cacumen biotae, Semen sesami nigrum 20
Part, 20 parts of cultivated land, 10 parts of the fruit of glossy privet, and said components are ground into 80 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
9h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 93 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
Embodiment 6
(1) by the material preparation of following mass parts：40 parts of insect wax, 60 parts of camellia seed oil；
(2) insect wax is ground into 80 mesh powders；
(3) it stocks up by following mass parts：18 parts of mulberries, 15 parts of Radix Ophiopogonis, 10 parts of cacumen biotae, 40 parts of Semen sesami nigrum, cultivated land 40
Part, 5 parts of the fruit of glossy privet, and said components are ground into 60 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
10h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 85 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
Embodiment 7
(1) by the material preparation of following mass parts：45 parts of insect wax, 55 parts of camellia seed oil；
(2) insect wax is ground into 40 mesh powders；
(3) it stocks up by following mass parts：10 parts of cultivated land, 20 parts of the fruit of glossy privet, and said components are ground into 60 mesh powders；
(4) powder of step (3) with filter paper is wrapped, solvent is made with absolute ethyl alcohol, is placed in Soxhlet extractor and is carried
10h is taken to obtain extracting solution, then extracting solution is concentrated with Rotary Evaporators, obtains concentrate；
(5) under 77 DEG C of water bath conditions, the Inesct Wax of step (2) is added in camellia seed oil, treats that insect wax is complete
It is dissolved in after camellia seed oil to stir and be cooled to room temperature, add concentrate obtained by step (4) to get to hair protection trichogen.
The zoopery of hair protection trichogen is as follows obtained by Examples 1 to 7：
The kunming mice 21 that weight is 18~22g is taken, health loses hair or feathers mouse back Bilateral Symmetry without pregnant, face of losing hair or feathers
Product is about 3cm × 3cm, and when depilation pays attention to not damaging mouse skin in order to avoid cutaneous permeability.By mouse be divided into 7 groups it is each right
Examples 1 to 7 is answered, every group 3, every group applies gained hair protection trichogen in Examples 1 to 7 outside on the left of mouse hair removal section,
Per medication 1 time is applied beyond the highest heavens, continuous 30 days, right side was smeared nothing, as blank control.Since mouse is there are individual difference,
19 experiment mices are shared after continuous use 15~24 days, left side ratio right side first grows hair, and left side hair is apparent than right side
It is dense.2 mouse are invalid (each corresponding embodiment 3 and 5), total effective rate 90.9%.
Comparative example 1：It is same as Example 1, but without using insect wax.
The kunming mice 10 that weight is 18~22g is taken, health loses hair or feathers mouse back Bilateral Symmetry without pregnant, face of losing hair or feathers
Product is about 3cm × 3cm, and when depilation pays attention to not damaging mouse skin in order to avoid cutaneous permeability.On the left of mouse hair removal section
The outer preparation for baldness for applying embodiment 1 and preparing per medication 1 time is applied beyond the highest heavens, continuous 30 days, applies preparation for baldness prepared by comparative example 1 outside right side,
Per painting medication beyond the highest heavens 1 time, continuous 30 days.As a result, left side ratio right side first grows hair, and left side hair is apparent denser than right side, and
Hair color is glossy, and mouse continuous use first grows hair in left side after 23 days, and right side of mice also grows hair after the 27th day, but left side hair is apparent
It is denser than right side hair, and the length of left side hair is also longer than right side hair.
Claims (4)
1. a kind of natural insect wax hair protection trichogen, it is characterised in that be made of the raw material of following masses part：
10~50 parts of insect wax, 90~50 parts of camellia seed oil
10~40 parts of the root of Dahurain angelica, 15~20 parts of mulberries
15~35 portions of Radix Ophiopogonis, 10~30 parts of cacumen biotae
20~40 parts of Semen sesami nigrum, 10~40 parts of cultivated land
5~20 parts of the fruit of glossy privet.
2. a kind of preparation method of natural insect wax hair protection trichogen, it is characterised in that pass through following each step：
（1）By the material preparation of following mass parts：
10~50 parts of insect wax, 90~50 parts of camellia seed oil
10~40 parts of the root of Dahurain angelica, 15~20 parts of mulberries
15~35 portions of Radix Ophiopogonis, 10~30 parts of cacumen biotae
20~40 parts of Semen sesami nigrum, 10~40 parts of cultivated land
5~20 parts of the fruit of glossy privet；
（2）Insect wax is ground into powder for 10~50 parts；
（3）Under 65~93 DEG C of water bath conditions, Inesct Wax is added in camellia seed oil, treats that insect wax is dissolved completely in oil tea
Stirring is cooled to room temperature after seed oil；
（4）By 10~40 parts of the root of Dahurain angelica, 15~20 parts of mulberries, 15~35 parts of Radix Ophiopogonis, 10~30 parts of cacumen biotae, Semen sesami nigrum 20~40
Part, 10~40 parts of cultivated land, 5~20 parts of the fruit of glossy privet are ground into powder；
（5）By step（4）Powder 8~10h extracted as solvent with absolute ethyl alcohol obtain extracting solution, then extracting solution is carried out
Concentration, obtains concentrate；
（6）By step（5）Concentrate be added to step（3）The camellia seed oil added with Inesct Wax in, must take care of hair life
Send out agent.
3. preparation method according to claim 2, it is characterised in that：The insect wax is ground into 20~80 mesh powders.
4. preparation method according to claim 2, it is characterised in that：The root of Dahurain angelica, mulberries, Radix Ophiopogonis, cacumen biotae, black sesame
Fiber crops, cultivated land, ligustrum lucidum powder are broken into 20~80 mesh powders.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410666928.3A CN104490642B (en) | 2014-11-20 | 2014-11-20 | Natural insect wax hair protection trichogen and preparation method thereof |
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|---|---|---|---|
| CN201410666928.3A CN104490642B (en) | 2014-11-20 | 2014-11-20 | Natural insect wax hair protection trichogen and preparation method thereof |
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| CN104490642A CN104490642A (en) | 2015-04-08 |
| CN104490642B true CN104490642B (en) | 2018-07-06 |
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| CN106511184B (en) * | 2016-12-27 | 2019-08-16 | 福建春辉生物工程有限公司 | A kind of baby shampoo and preparation method thereof containing tea seed cake |
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| CN101019813A (en) * | 2006-02-14 | 2007-08-22 | 天津天隆农业科技有限公司 | Hair care article containing octacosanol and its prepn |
| CN101129317A (en) * | 2007-08-02 | 2008-02-27 | 袁仲元 | Hair-growing hair-blackening liquid formula |
| CN104107375B (en) * | 2014-08-06 | 2017-03-15 | 圣原健康产业有限公司 | Chinese medicine composition that hair care is sent out admittedly and its preparation method and application |
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Inventor after: Ma Jinju Inventor after: Ma Liyi Inventor after: Chen Xiaoming Inventor after: Zhang Hong Inventor after: Zhang Zhongquan Inventor after: Wang Youqiong Inventor after: Duan Qiongfen Inventor after: Zheng Hua Inventor before: Ma Jinju Inventor before: Ma Liyi Inventor before: Zhang Hong Inventor before: Zhang Zhongquan Inventor before: Wang Youqiong Inventor before: Duan Qiongfen Inventor before: Zheng Hua |
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Free format text: CORRECT: INVENTOR; FROM: MA JINJU MA LIYI ZHANG HONG ZHANG ZHONGQUAN WANG YOUQIONG DUAN QIONGFEN ZHENG HUA TO: MA JINJU MA LIYI CHEN XIAOMING ZHANG HONG ZHANG ZHONGQUAN WANG YOUQIONG DUAN QIONGFEN ZHENG HUA |
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