CN104489280B - A kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method - Google Patents
A kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method Download PDFInfo
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- CN104489280B CN104489280B CN201510019548.5A CN201510019548A CN104489280B CN 104489280 B CN104489280 B CN 104489280B CN 201510019548 A CN201510019548 A CN 201510019548A CN 104489280 B CN104489280 B CN 104489280B
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- 240000007263 Pinus koraiensis Species 0.000 title claims abstract description 42
- 235000011615 Pinus koraiensis Nutrition 0.000 title claims abstract description 42
- 239000003094 microcapsule Substances 0.000 title claims abstract description 16
- 239000000843 powder Substances 0.000 title claims abstract description 14
- 239000003674 animal food additive Substances 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 14
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 14
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 14
- 229930006000 Sucrose Natural products 0.000 claims abstract description 14
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 14
- 239000005720 sucrose Substances 0.000 claims abstract description 14
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims abstract description 13
- 229940083466 soybean lecithin Drugs 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000004615 ingredient Substances 0.000 claims description 24
- 239000000839 emulsion Substances 0.000 claims description 15
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 13
- 239000008158 vegetable oil Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 10
- 230000006837 decompression Effects 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000010298 pulverizing process Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 235000005687 corn oil Nutrition 0.000 claims description 5
- 239000002285 corn oil Substances 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 5
- 235000019198 oils Nutrition 0.000 claims description 5
- 238000012216 screening Methods 0.000 claims description 5
- 235000012424 soybean oil Nutrition 0.000 claims description 5
- 239000003549 soybean oil Substances 0.000 claims description 5
- 238000001694 spray drying Methods 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 239000004480 active ingredient Substances 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 5
- 230000012010 growth Effects 0.000 abstract description 4
- 206010059866 Drug resistance Diseases 0.000 abstract description 3
- 201000010099 disease Diseases 0.000 abstract description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 3
- 239000003814 drug Substances 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 239000003242 anti bacterial agent Substances 0.000 abstract description 2
- 229940088710 antibiotic agent Drugs 0.000 abstract description 2
- 238000009360 aquaculture Methods 0.000 abstract description 2
- 244000144974 aquaculture Species 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 239000003995 emulsifying agent Substances 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 241000588724 Escherichia coli Species 0.000 description 4
- 241000191967 Staphylococcus aureus Species 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 235000014590 basal diet Nutrition 0.000 description 3
- 230000037396 body weight Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 101000730040 Klebsiella pneumoniae Arylsulfatase Proteins 0.000 description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 244000052769 pathogen Species 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 2
- 240000005020 Acaciella glauca Species 0.000 description 1
- 235000018782 Dacrydium cupressinum Nutrition 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- 235000013697 Pinus resinosa Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000003698 anagen phase Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 235000018343 nutrient deficiency Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
Abstract
The present invention relates to a kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method, belong to feed additive field.Korean pine tower Essence 10 ~ 50 parts, soybean lecithin 0.5 ~ 3 part, maltodextrin 30 ~ 60 parts, sucrose 7 ~ 20 parts.Select Korean pine tower Essence to be core, soybean lecithin is emulsifying agent, with maltodextrin and sucrose for compound wall materials, by spray-dired method, and obtained Korean pine tower Essence microcapsule powder feed addictive.Advantage of the present invention is: composition all belong to safety, green, without medicine interpolation, have no drug resistance, can effective substitute antibiotics, meet healthy aquaculture developing direction; And active ingredient is carried out the oxidation that microencapsulation can avoid the active ingredient of raw material, strengthen the stability of result of use, extend the shelf life, the incidence that this feed addictive can promote the growth of pig, improve feed efficiency, reduces disease.
Description
Technical field
The invention belongs to feed additive field, be specifically related to a kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method.
Background technology
Microcapsules technology refers to solid, liquid or gas entrapment in small and closed capsule.There is the advantage reducing volatility, improve material stability.
The pinecone is the cone of Korean pine, removes seed and get final product.Because red pine growth belongs to nature pine tree more, do not have medicament residue, its pinecone is many as discarded object, and active ingredient cannot be utilized, and causes the wasting of resources to a certain degree.
Liposoluble constituent in the pinecone can leach as additive component by vegetable oil, vegetable oil itself is containing multiple nutritional components simultaneously, grease is added at each growth phase of pig, supplement and balance each nutrient, especially guaranteeing the balance of albumen and energy, the nutrition condition of pig can be improved, improve production performance, but grease is easily subject to the impact of external environment and becomes sour, and makes nutritional deficiency, and produces peculiar smell.
Summary of the invention
The invention provides a kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method, for effectively promoting the growth of pig, reducing the illness rate of pig, improving meat quality.
The technical scheme that the present invention takes is: be made up of the raw material of following weight portion:
Korean pine tower Essence 10 ~ 50 parts, soybean lecithin 0.5 ~ 3 part, maltodextrin 30 ~ 60 parts, sucrose 7 ~ 20 parts.
Korean pine tower Essence of the present invention obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 5 ~ 15mm;
2) by the particle after pulverizing with w/v 1:(1 ~ 5) ratio join in vegetable oil, and together to pour in destilling tower;
3) passing into temperature is that the steam of 70 ~ 85 degrees Celsius carries out decompression distillation 3 ~ 5 hours, and pressure is 30 ~ 50kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio (1 ~ 4): 1 mixing.
Vegetable oil of the present invention is the one in soybean oil, palm fibre oil or corn oil.
The preparation method of a kind of Korean pine tower of the present invention Essence microcapsule powder pig's feed additive, is characterized in that comprising the following steps:
1) maltodextrin and sucrose are dissolved in the distilled water of 65 ~ 75 DEG C and stir;
2) add Korean pine tower Essence and soybean lecithin again to carry out stirring and form stable emulsion;
3) then by emulsion homogeneous 2 ~ 4 times;
4) making the emulsion after homogeneous enter EAT is that the spray drying tower of 90 ~ 130 DEG C carries out spraying dry;
5) after 20 ~ 60 order classifying screen screenings, finished product is obtained again.
Core of the present invention is Korean pine tower Essence, and emulsifying agent is soybean lecithin, and compound wall materials is maltodextrin and sucrose.
Using method of the present invention is: described feed addictive can directly add in pig's feed, and addition is 300 ~ 1000g/t; Or be mixed and made into premix, concentrate feed form feeding animals with other feed addictive or feedstuff.
Advantage of the present invention is employing safety, Korean pine tower Essence that is efficient, that have no drug resistance is core, has advantage that is antibacterial, disease-resistant, that improve immunity, strengthen nutrition; With maltodextrin and sucrose for core can well wrap up by wall material; Simultaneously the sweet taste of the rosin of core, Xin Xiang and wall material is all the taste that pig is liked; Use microcapsule embedded technology can prevent the loss of Korean pine tower Essence active ingredient, reduce external environment to the destruction of raw material, reduce the volatilization loss in packaging, storage, transport and use procedure, strengthen effect stability, extend the shelf life.
Feed addictive of the present invention can kill the harmful levels of pathogens of the enteron aisle such as Escherichia coli, staphylococcus aureus, maintains the balance of enteric microorganism, thus reduces the illness rate of pig, improves the survival rate of pig; Supplementing of various nutrients can improve meat quality, makes its nutrition more perfect; Rosin, Xin Xiang and sweet taste have the effect luring and search for food to pig, can increase the feed intake of pig, make feed decompose digestion and accelerate, improve production performance and the efficiency of feed utilization of pig, promote that it grows.
Feed addictive of the present invention is not containing any antibiotic composition, belong to antibiotic substitute, ensure pig industry safe, efficiently raise, composition all belong to safety, green, without medicine interpolation, have no drug resistance, can effective substitute antibiotics, meet healthy aquaculture developing direction; And active ingredient is carried out the oxidation that microencapsulation can avoid the active ingredient of raw material, strengthen the stability of result of use, extend the shelf life, the incidence that can promote the growth of pig, improve feed efficiency, reduce disease.
Detailed description of the invention
Embodiment 1
Be made up of the raw material of following weight portion:
Korean pine tower Essence 10 parts, soybean lecithin 0.5 part, maltodextrin 30 parts, sucrose 7 parts;
Preparation method is as follows:
1) maltodextrin and sucrose are dissolved in the distilled water of 65 DEG C and stir;
2) add Korean pine tower Essence and soybean lecithin again to carry out stirring and form stable emulsion;
3) then by emulsion homogeneous 2 times;
4) making the emulsion after homogeneous enter EAT is that the spray drying tower of 90 DEG C carries out spraying dry;
5) after 20 order classifying screen screenings, finished product is obtained again;
Described Korean pine tower Essence obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 5mm;
2) particle after pulverizing is joined in vegetable oil with the ratio of w/v 1:1, and together pour in destilling tower;
3) passing into temperature is that the steam of 70 degrees Celsius carries out decompression distillation 3 hours, and pressure is 30kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio 1:1 mixing;
Described vegetable oil is the one in soybean oil, palm fibre oil or corn oil.
The present embodiment is applied to piglet, and 300 body weight are divided into two groups the pig of 30 kilograms substantially, often organizes 100, two groups of basal diets of feeding are consistent, and one group is control group, and one group is the Korean pine tower Essence microcapsule powder feed addictive that with the addition of 300g/t, feed 23 days, result is as follows:
Embodiment 2
Be made up of the raw material of following weight portion:
Korean pine tower Essence 30 parts, soybean lecithin 1.8 parts, maltodextrin 45 parts, sucrose 13.5 parts;
Preparation method is as follows:
1) maltodextrin and sucrose are dissolved in the distilled water of 70 DEG C and stir;
2) add Korean pine tower Essence and soybean lecithin again to carry out stirring and form stable emulsion;
3) then by emulsion homogeneous 3 times;
4) making the emulsion after homogeneous enter EAT is that the spray drying tower of 110 DEG C carries out spraying dry;
5) after 40 order classifying screen screenings, finished product is obtained again.
Described Korean pine tower Essence obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 10mm;
2) particle after pulverizing is joined in vegetable oil with the ratio of w/v 1:3, and together pour in destilling tower;
3) passing into temperature is that the steam of 77.5 degrees Celsius carries out decompression distillation 4 hours, and pressure is 40kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio 2.5:1 mixing.
Vegetable oil of the present invention is the one in soybean oil, palm fibre oil or corn oil.
The present embodiment is applied to piglet, and 300 body weight are divided into two groups the pig of 70 kilograms substantially, often organizes 100, two groups of basal diets of feeding are consistent, and one group is control group, and one group is the Korean pine tower Essence microcapsule powder feed addictive that with the addition of 800g/t, feed 30 days, result is as follows:
Embodiment 3
Be made up of the raw material of following weight portion:
Korean pine tower Essence 50 parts, soybean lecithin 3 parts, maltodextrin 60 parts, sucrose 20 parts;
Preparation method is as follows:
1) maltodextrin and sucrose are dissolved in the distilled water of 75 DEG C and stir;
2) add Korean pine tower Essence and soybean lecithin again to carry out stirring and form stable emulsion;
3) then by emulsion homogeneous 4 times;
4) making the emulsion after homogeneous enter EAT is that the spray drying tower of 130 DEG C carries out spraying dry;
5) after 60 order classifying screen screenings, finished product is obtained again.
Described Korean pine tower Essence obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 15mm;
2) particle after pulverizing is joined in vegetable oil with the ratio of w/v 1:5, and together pour in destilling tower;
3) passing into temperature is that the steam of 85 degrees Celsius carries out decompression distillation 5 hours, and pressure is 50kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio 4:1 mixing.
Vegetable oil of the present invention is the one in soybean oil, palm fibre oil or corn oil.
The present embodiment is applied to piglet, and 300 body weight are divided into two groups the pig of 100 kilograms substantially, often organizes 45, two groups of basal diets of feeding are consistent, and one group is control group, and one group is the Korean pine tower Essence microcapsule powder feed addictive that with the addition of 1000g/t, feed 21 days, result is as follows:
Effect of the present invention is further illustrated below by In vitro Bactericidal Experiments.
Using the several frequently seen harmful bacteria of Escherichia coli, staphylococcus aureus, Klebsiella Pneumoniae as test strains, use feed addictive to be dissolved in the distilled water of sterilizing and carry out antibacterial tests, plating medium drum rim dripping method is adopted to observe the situation of cultivation several bacterium after 24 hours, to the test situation of Escherichia coli, staphylococcus aureus, Klebsiella Pneumoniae as following table:
Feed addictive of the present invention can kill the harmful levels of pathogens of the enteron aisle such as Escherichia coli, staphylococcus aureus.
Claims (4)
1. a Korean pine tower Essence microcapsule powder pig's feed additive, it is characterized in that being made up of the raw material of following weight portion:
Korean pine tower Essence 10 ~ 50 parts, soybean lecithin 0.5 ~ 3 part, maltodextrin 30 ~ 60 parts, sucrose 7 ~ 20 parts;
Described Korean pine tower Essence obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 5 ~ 15mm;
2) by the particle after pulverizing with w/v 1:(1 ~ 5) ratio join in vegetable oil, and together to pour in destilling tower;
3) passing into temperature is that the steam of 70 ~ 85 degrees Celsius carries out decompression distillation 3 ~ 5 hours, and pressure is 30 ~ 50kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio (1 ~ 4): 1 mixing.
2. a kind of Korean pine tower Essence microcapsule powder pig's feed additive according to claim 1, is characterized in that, described vegetable oil is the one in soybean oil, palm fibre oil or corn oil.
3. the preparation method of a kind of Korean pine tower Essence microcapsule powder pig's feed additive as claimed in claim 1, is characterized in that comprising the following steps:
1) maltodextrin and sucrose are dissolved in the distilled water of 65 ~ 75 DEG C and stir;
2) add Korean pine tower Essence and soybean lecithin again to carry out stirring and form stable emulsion;
3) then by emulsion homogeneous 2 ~ 4 times;
4) making the emulsion after homogeneous enter EAT is that the spray drying tower of 90 ~ 130 DEG C carries out spraying dry;
5) after 20 ~ 60 order classifying screen screenings, finished product is obtained again.
4. the preparation method of a kind of Korean pine tower Essence microcapsule powder pig's feed additive according to claim 3, it is characterized in that, described Korean pine tower Essence obtains by the following method:
1) pulverized by the pinecone of Korean pine, its grain diameter is 5 ~ 15mm;
2) particle after pulverizing is joined in vegetable oil with the ratio of 1:1 ~ 5, and together pour in destilling tower;
3) passing into temperature is that the steam of 70 ~ 85 degrees Celsius carries out decompression distillation 3 ~ 5 hours, and pressure is 30 ~ 50kpa;
4) obtain volatile ingredient and oil-soluble ingredients simultaneously;
5) volatile ingredient obtained and oil-soluble ingredients are carried out volume ratio (1 ~ 4): 1 mixing.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510019548.5A CN104489280B (en) | 2015-01-15 | 2015-01-15 | A kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510019548.5A CN104489280B (en) | 2015-01-15 | 2015-01-15 | A kind of Korean pine tower Essence microcapsule powder pig's feed additive and preparation method |
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| Publication Number | Publication Date |
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| CN104489280B true CN104489280B (en) | 2016-04-27 |
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| CN115644321B (en) * | 2022-11-15 | 2023-03-03 | 潍坊天普阳光饲料科技有限公司 | Feed additive for preventing and treating pig diarrhea and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1545923A (en) * | 2003-12-03 | 2004-11-17 | 广州优宝工业有限公司 | Natural beta-carotene microcapsule and method for making same |
| CN102550610A (en) * | 2010-12-07 | 2012-07-11 | 菲勒斯株式会社 | Natural germicide containing phytoncide extracted from Korean pine cones and fruit disease controlling material containing the same |
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2015
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1545923A (en) * | 2003-12-03 | 2004-11-17 | 广州优宝工业有限公司 | Natural beta-carotene microcapsule and method for making same |
| CN102550610A (en) * | 2010-12-07 | 2012-07-11 | 菲勒斯株式会社 | Natural germicide containing phytoncide extracted from Korean pine cones and fruit disease controlling material containing the same |
Non-Patent Citations (1)
| Title |
|---|
| 红松松塔、松子壳研究进展及在畜牧业中应用可行性分析;王智航等;《国外畜牧学(猪与禽)》;20090725(第04期);88－90 * |
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Application publication date: 20150408 Assignee: JILIN PAINUO BIOTECHNOLOGY Co.,Ltd. Assignor: Zhao Xiaoyuan Contract record no.: 2016220000007 Denomination of invention: Korean pine cone essence micro-capsule powder pig feedstuff additive and preparation method License type: Exclusive License Record date: 20160418 |
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Effective date of registration: 20161206 Address after: 130000 Changchun Province, Guangzhou City, North District, high tech North Main Street, No. 3333 Patentee after: JILIN PAINUO BIOTECHNOLOGY Co.,Ltd. Address before: 130000 Jilin province Changchun Exhibition Street home Fulin Patentee before: Zhao Xiaoyuan |
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Effective date of registration: 20190807 Address after: 3333 Shengbei Street, Beihu Science and Technology Development Zone, Changchun City, Jilin Province, 130000 Patentee after: Jilin Songwei Eco-industrial Chain Technology Co.,Ltd. Address before: 130000 Changchun Province, Guangzhou City, North District, high tech North Main Street, No. 3333 Patentee before: JILIN PAINUO BIOTECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20201013 Address after: 3333 Shengbei Street, Beihu Science and Technology Development Zone, Changchun City, Jilin Province, 130000 Patentee after: JILIN PAINUO BIOTECHNOLOGY Co.,Ltd. Address before: 3333 Shengbei Street, Beihu Science and Technology Development Zone, Changchun City, Jilin Province, 130000 Patentee before: Jilin Songwei Eco-industrial Chain Technology Co.,Ltd. |
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Effective date of registration: 20221122 Address after: 161003 Longtou Village, Angangxi District, Qiqihar City, Heilongjiang Province Patentee after: Heilongjiang Leyun Recycling Agricultural Biotechnology Co.,Ltd. Address before: No. 3333, Shengbei street, Beihu science and Technology Development Zone, Changchun City, Jilin Province Patentee before: JILIN PAINUO BIOTECHNOLOGY Co.,Ltd. |