CN104478224A - Method for forming acid-etching quartz pendulous reed flexible beam - Google Patents

Method for forming acid-etching quartz pendulous reed flexible beam Download PDF

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CN104478224A
CN104478224A CN201410689983.4A CN201410689983A CN104478224A CN 104478224 A CN104478224 A CN 104478224A CN 201410689983 A CN201410689983 A CN 201410689983A CN 104478224 A CN104478224 A CN 104478224A
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flexible beam
quartz pendulum
acid solution
hydrofluoric acid
etching
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杜秀蓉
宋学富
孙元成
王慧
张晓强
王玉芬
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China Building Materials Academy CBMA
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China Building Materials Academy CBMA
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Abstract

本发明涉及石英摆片制造领域,尤其是一种酸刻蚀石英摆片挠性梁的成形方法。所述酸刻蚀石英摆片挠性梁的成形方法,包括以下步骤:第一步:将工装好的石英摆片挠性梁放入第一氢氟酸溶液中,在第一温度条件下,进行快速刻蚀,直至石英摆片挠性梁达到第一预设厚度;第二步:将第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中,在第二温度条件下,进行慢速刻蚀,直至石英摆片挠性梁达到第二预设厚度;其中:第一氢氟酸溶液的浓度大于第二氢氟酸溶液的浓度,第一氢氟酸溶液的浓度小于22mol/L;第一温度高于第二温度。所述酸刻蚀石英摆片挠性梁的成形方法缩短石英摆片挠性梁酸刻蚀时间;可对石英摆片挠性梁厚度进行控制精度。

The invention relates to the field of quartz pendulum manufacture, in particular to a method for forming a flexible beam of a quartz pendulum by acid etching. The forming method of the acid-etched quartz pendulum flexible beam comprises the following steps: the first step: putting the well-equipped quartz pendulum flexible beam into the first hydrofluoric acid solution, and under the first temperature condition, Perform rapid etching until the flexible beam of the quartz pendulum plate reaches the first preset thickness; the second step: put the flexible beam of the quartz pendulum plate with the first preset thickness into the second hydrofluoric acid solution, at the second temperature Under the conditions, carry out slow etching until the flexible beam of the quartz pendulum plate reaches the second preset thickness; wherein: the concentration of the first hydrofluoric acid solution is greater than the concentration of the second hydrofluoric acid solution, and the concentration of the first hydrofluoric acid solution The concentration is less than 22mol/L; the first temperature is higher than the second temperature. The forming method of acid-etching the flexible beam of the quartz pendulum plate shortens the acid etching time of the flexible beam of the quartz pendulum plate; the thickness of the flexible beam of the quartz pendulum plate can be controlled accurately.

Description

一种酸刻蚀石英摆片挠性梁的成形方法A method for forming flexible beams of acid-etched quartz pendulum plates

技术领域technical field

本发明涉及石英摆片挠性梁制造领域,尤其是一种酸刻蚀石英摆片挠性梁的成形方法。The invention relates to the field of manufacturing flexible beams of quartz swing plates, in particular to a method for forming flexible beams of quartz swing plates by acid etching.

背景技术Background technique

石英摆片挠性梁是石英挠性加速度计的核心元件,石英挠性加速度计主要用于惯性导航系统,其主要性能指标包括量程、分辨率、偏值重复性、标度因素重复性和非线性等,其性能指标中的量程和分辨率决定于石英摆片挠性梁的厚度和表面质量。The quartz pendulum flexible beam is the core component of the quartz flexible accelerometer. The quartz flexible accelerometer is mainly used in the inertial navigation system. Its main performance indicators include range, resolution, bias repeatability, scale factor repeatability and Linearity, etc., the range and resolution of its performance indicators are determined by the thickness and surface quality of the flexible beam of the quartz pendulum.

目前,公知的石英摆片挠性梁成形方法是利用氢氟酸与石英玻璃的化学反应使石英摆片挠性梁厚度减薄,使其刚度减小从而实现挠性弯曲。摆片平面刻图后,采用特制的酸蚀模具和氟硅橡胶掩膜,保护除石英摆片挠性梁外的其余部分,将其置于一定浓度和温度的氢氟酸溶液中进行酸刻蚀,通过测量“陪片”的酸蚀量计算酸蚀速率从而估算石英摆片挠性梁的厚度,即摆片石英摆片挠性梁“一步”成形法。“一步法”的酸刻蚀速率约为1.3um/min,石英摆片挠性梁加工时需要减薄的量为690um,则需要耗时530min。该方法进行酸刻蚀石英摆片挠性梁不仅耗时长,而且精度不高。At present, the known forming method of the flexible beam of the quartz pendulum plate is to use the chemical reaction of hydrofluoric acid and quartz glass to reduce the thickness of the flexible beam of the quartz pendulum plate, so as to reduce the stiffness and realize flexible bending. After engraving the plane of the pendulum plate, use a special acid-etching mold and a fluorosilicone rubber mask to protect the rest except the flexible beam of the quartz pendulum plate, and place it in a hydrofluoric acid solution of a certain concentration and temperature for acid etching The thickness of the flexible beam of the quartz pendulum plate is estimated by measuring the acid etching amount of the “companion plate” to calculate the acid etching rate, which is the “one-step” forming method of the flexible beam of the quartz pendulum plate. The acid etching rate of the "one-step method" is about 1.3um/min, and the amount of thinning required for the processing of the quartz pendulum flexible beam is 690um, which takes 530min. This method not only takes a long time to acid-etch the flexible beam of the quartz pendulum plate, but also has low precision.

发明内容Contents of the invention

为了克服上述酸刻蚀石英摆片挠性梁“一步法”成形引起的石英摆片挠性梁厚度控制精度差和耗时时间长的不足,本发明提供了一种酸刻蚀石英摆片挠性梁的成形方法,该方法不仅能将石英摆片挠性梁的厚度控制精度提高至±1um,而且能大大降低反应时间。In order to overcome the disadvantages of poor thickness control accuracy and long time-consuming of the quartz pendulum flexible beam caused by the "one-step" forming of the acid-etched quartz pendulum flexible beam, the present invention provides an acid-etched quartz pendulum flexible beam. The forming method of the flexible beam, which can not only improve the thickness control accuracy of the quartz pendulum flexible beam to ±1um, but also greatly reduce the reaction time.

本发明的目的及解决其技术问题是采用以下技术方案来实现的。The purpose of the present invention and the solution to its technical problems are achieved by adopting the following technical solutions.

通过一种酸刻蚀石英摆片挠性梁的成形方法,包括以下步骤:A method for forming a flexible beam of a quartz pendulum by acid etching, comprising the following steps:

第一步:将工装好的石英摆片挠性梁放入第一氢氟酸溶液中,在第一温度条件下,进行快速刻蚀,直至所述石英摆片挠性梁达到第一预设厚度;The first step: Put the flexible beam of the quartz pendulum plate into the first hydrofluoric acid solution, and perform rapid etching under the first temperature condition until the flexible beam of the quartz pendulum plate reaches the first preset value. thickness;

第二步:将所述第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中,在第二温度条件下,进行慢速刻蚀,直至所述石英摆片挠性梁达到第二预设厚度;Step 2: Put the flexible beam of the quartz pendulum plate with the first preset thickness into the second hydrofluoric acid solution, and perform slow etching under the second temperature condition until the quartz pendulum plate is flexible. the beam reaches a second preset thickness;

其中:所述第一氢氟酸溶液的浓度大于所述第二氢氟酸溶液的浓度,所述第一氢氟酸溶液的浓度小于22mol/L;Wherein: the concentration of the first hydrofluoric acid solution is greater than the concentration of the second hydrofluoric acid solution, and the concentration of the first hydrofluoric acid solution is less than 22mol/L;

所述第一温度高于所述第二温度。The first temperature is higher than the second temperature.

优选地,Preferably,

所述第一氢氟酸溶液的浓度的18~22mol/L;18-22mol/L of the concentration of the first hydrofluoric acid solution;

所述第二氢氟酸溶液的浓度为10~15mol/L。The concentration of the second hydrofluoric acid solution is 10-15 mol/L.

优选地,Preferably,

所述第一温度为50~70℃;The first temperature is 50-70°C;

所述第二温度为20~30℃。The second temperature is 20-30°C.

优选地,Preferably,

在所述快速刻蚀过程中,在所述第一氢氟酸溶液中放入第一玻璃陪片,通过计算所述第一玻璃陪片在所述第一氢氟酸溶液中的第一酸刻蚀速率,进行估算测试所述第一预设厚度的第一预设时间;In the rapid etching process, the first glass companion is placed in the first hydrofluoric acid solution, and the first acid of the first glass companion in the first hydrofluoric acid solution is calculated Etching rate, the first preset time for estimating and testing the first preset thickness;

在所述慢速刻蚀过程中,在所述第二氢氟酸溶液中放入第二玻璃陪片,通过计算所述第二玻璃陪片在所述第二氢氟酸溶液中的第二酸刻蚀速率,进行估算测试所述第二预设厚度的第二预设时间。In the slow etching process, put a second glass companion in the second hydrofluoric acid solution, by calculating the second glass companion in the second hydrofluoric acid solution The acid etching rate is estimated and tested for a second preset time for the second preset thickness.

优选地,Preferably,

所述第一预设时间为180~300min;The first preset time is 180-300 minutes;

所述第二预设时间为30~50min。The second preset time is 30-50 minutes.

优选地,Preferably,

通过光纤光谱测厚装置,测量所述石英摆片挠性梁的第一预设厚度和第二预设厚度;Measuring the first preset thickness and the second preset thickness of the quartz pendulum flexible beam through an optical fiber spectroscopic thickness measuring device;

所述光纤光谱测厚装置包括光纤光谱仪、光源、模具固定底座和光纤测量探头,所述光纤光谱仪和光源分别经光纤与所述光纤测量探头连接,所述模具固定底座用于固定所述石英摆片绕性梁,所述光纤测量探头垂直设置在固定在所述模具固定底座上的所述石英摆片绕性梁的一侧。The optical fiber spectrum thickness measuring device includes a fiber optic spectrometer, a light source, a mold fixing base and an optical fiber measuring probe, the fiber optic spectrometer and the light source are respectively connected to the optical fiber measuring probe through an optical fiber, and the mold fixing base is used to fix the quartz pendulum A sheet-wound beam, the optical fiber measuring probe is vertically arranged on one side of the quartz pendulum sheet-wound beam fixed on the mold fixing base.

优选地,Preferably,

所述第一预设厚度为40~60μm;The first preset thickness is 40-60 μm;

所述第二预设厚度为24~28μm。The second preset thickness is 24-28 μm.

优选地,Preferably,

通过氟硅橡胶掩膜将所述石英摆片挠性梁装模,形成工装好的石英摆片挠性梁。The flexible beam of the quartz pendulum plate is molded through a fluorosilicone rubber mask to form the flexible beam of the quartz pendulum plate that has been tooled.

优选地,Preferably,

将第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中时,使用去离子水冲洗残留酸液,并用无尘布吸干石英摆片挠性梁表面水分。When putting the flexible beam of the quartz pendulum plate with the first predetermined thickness into the second hydrofluoric acid solution, rinse the residual acid solution with deionized water, and dry the surface moisture of the flexible beam of the quartz pendulum plate with a dust-free cloth.

优选地,Preferably,

在进行快速刻蚀时,所述石英摆片挠性梁竖直放置在所述第一氢氟酸溶液中;When performing rapid etching, the flexible beam of the quartz pendulum plate is vertically placed in the first hydrofluoric acid solution;

在进行慢速刻蚀时,所述石英摆片挠性梁竖直放置在所述第二氢氟酸溶液中。When performing slow etching, the flexible beam of the quartz pendulum is vertically placed in the second hydrofluoric acid solution.

借由上述技术方案,本发明提出的一种酸刻蚀石英摆片挠性梁的成形方法至少具有下列优点:By virtue of the above-mentioned technical scheme, a method for forming the acid-etched quartz pendulum flexible beam proposed by the present invention has at least the following advantages:

1)缩短石英摆片挠性梁酸刻蚀时间;1) shorten the acid etching time of the quartz pendulum flexible beam;

2)避免橡胶掩膜酸溶造成的石英摆片挠性梁厚度不均和玻璃边缘毛刺;2) Avoid the uneven thickness of the flexible beam of the quartz pendulum plate and the burrs on the edge of the glass caused by the acid dissolution of the rubber mask;

3)可对石英摆片挠性梁厚度进行精确控制。3) The thickness of the flexible beam of the quartz pendulum can be precisely controlled.

上述说明仅是本发明技术方案的概述,为了能够更清楚了解本发明的技术手段,并可依照说明书的内容予以实施,以下以本发明的较佳实施例并配合附图详细说明如后。The above description is only an overview of the technical solutions of the present invention. In order to understand the technical means of the present invention more clearly and implement them according to the contents of the description, the preferred embodiments of the present invention and accompanying drawings are described in detail below.

附图说明Description of drawings

图1是本发明的工艺流程图;Fig. 1 is a process flow diagram of the present invention;

图2是本发明氟硅橡胶掩膜和与石英摆片挠性梁的工装结构图;Fig. 2 is the tooling structural diagram of fluorosilicone rubber mask of the present invention and flexible beam with quartz pendulum plate;

图3是本发明的在线测厚装置的结构示意图。Fig. 3 is a schematic structural view of the online thickness measuring device of the present invention.

具体实施方式Detailed ways

为更进一步阐述本发明为达成预定发明目的所采取的技术手段及功效,以下结合附图及较佳实施例,对依据本发明提出的一种酸刻蚀石英摆片挠性梁的成形方法,详细说明如后。In order to further explain the technical means and effects of the present invention to achieve the intended purpose of the invention, the following in conjunction with the accompanying drawings and preferred embodiments, a method for forming a flexible beam of acid-etched quartz pendulum proposed according to the present invention, Details are as follows.

本发明提供的一种酸刻蚀石英摆片挠性梁的成形方法(具体工艺流程参见图1),包括以下步骤:A kind of forming method (see Fig. 1 for specific technical process) of acid-etched quartz pendulum plate flexible beam provided by the present invention, comprises the following steps:

第一步:将工装好的石英摆片挠性梁放入第一氢氟酸溶液中,在第一温度条件下,进行快速刻蚀,直至所述石英摆片挠性梁达到第一预设厚度;The first step: Put the flexible beam of the quartz pendulum plate into the first hydrofluoric acid solution, and perform rapid etching under the first temperature condition until the flexible beam of the quartz pendulum plate reaches the first preset value. thickness;

第二步:将所述第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中,在第二温度条件下,进行慢速刻蚀,直至所述石英摆片挠性梁达到第二预设厚度;其中:所述第一氢氟酸溶液的浓度大于所述第二氢氟酸溶液的浓度,所述第一氢氟酸溶液的浓度小于22mol/L;所述第一温度高于所述第二温度。Step 2: Put the flexible beam of the quartz pendulum plate with the first preset thickness into the second hydrofluoric acid solution, and perform slow etching under the second temperature condition until the quartz pendulum plate is flexible. The beam reaches the second preset thickness; wherein: the concentration of the first hydrofluoric acid solution is greater than the concentration of the second hydrofluoric acid solution, and the concentration of the first hydrofluoric acid solution is less than 22mol/L; the second hydrofluoric acid solution A temperature is higher than the second temperature.

通过第一氢氟酸溶液对所述石英摆片挠性梁进行快速刻蚀,能够加快所述石英摆片挠性梁刻蚀至第二预设厚度的反应时间。通过第二氢氟酸溶液对所述石英摆片挠性梁进行慢速刻蚀,能有效控制所述石英摆片挠性梁到第二预设厚度的精度。The rapid etching of the flexible beam of the quartz pendulum plate by the first hydrofluoric acid solution can speed up the reaction time for etching the flexible beam of the quartz pendulum plate to the second preset thickness. Slowly etching the flexible beam of the quartz pendulum plate through the second hydrofluoric acid solution can effectively control the precision of the flexible beam of the quartz pendulum plate to the second preset thickness.

优选地,所述第一氢氟酸溶液的浓度的18~22mol/L。Preferably, the concentration of the first hydrofluoric acid solution is 18-22 mol/L.

优选地,所述第二氢氟酸溶液的浓度为10~15mol/L。Preferably, the concentration of the second hydrofluoric acid solution is 10-15 mol/L.

优选地,本发明中,所述第一氢氟酸溶液和所述第二氢氟酸溶液,均采用优级纯(GR)氢氟酸溶液进行配置。Preferably, in the present invention, both the first hydrofluoric acid solution and the second hydrofluoric acid solution are configured with superior grade (GR) hydrofluoric acid solution.

优选地,所述优级纯(GR)氢氟酸溶液的含量≥40%,浓度约为22.8mol/L。将所述优级纯(GR)氢氟酸溶液与水或者其他溶剂稀释到所需浓度;加热稀释后的所述优级纯(GR)氢氟酸溶液并充分搅拌,使所述优级纯(GR)氢氟酸溶液在酸蚀容器中浓度、温度分布均匀;待所述优级纯(GR)氢氟酸溶液温度恒定后(波动<±0.5℃)方可进行酸蚀速率标定,然后进行所述石英摆片挠性梁的酸刻蚀加工。Preferably, the content of the superior grade pure (GR) hydrofluoric acid solution is ≥ 40%, and the concentration is about 22.8 mol/L. The superior grade pure (GR) hydrofluoric acid solution is diluted to the required concentration with water or other solvents; the superior grade pure (GR) hydrofluoric acid solution after heating and dilution is fully stirred to make the superior grade pure The concentration and temperature distribution of (GR) hydrofluoric acid solution in the acid etching container is uniform; the acid etching rate calibration can only be carried out after the temperature of the superior grade pure (GR) hydrofluoric acid solution is constant (fluctuation<±0.5°C), and then The acid etching process of the flexible beam of the quartz pendulum plate is carried out.

优选地,所述第一温度为50~70℃。Preferably, the first temperature is 50-70°C.

优选地,所述第二温度为20~30℃。Preferably, the second temperature is 20-30°C.

反应时间决定于氢氟酸浓度和反应温度,第一步选择18~22mol/L,50~70℃,在高温高氢氟酸浓度下尽量缩短酸刻蚀的时间,将酸刻蚀时间控制在5小时之内,一方面是比一步法节省时间,更重要的是减少橡胶掩膜因为长时间浸泡在酸液中造成的酸溶现象。温度不适宜高于70℃是考虑到橡胶在高温下的酸溶加快。第二步选择温度20~30℃,氢氟酸浓度为10~15mol/L,酸刻蚀速率慢,目的在于提高对最终挠性梁厚度的控制精度。The reaction time depends on the concentration of hydrofluoric acid and the reaction temperature. In the first step, choose 18-22mol/L, 50-70°C, and try to shorten the acid etching time at high temperature and high hydrofluoric acid concentration, and control the acid etching time at Within 5 hours, on the one hand, it saves time compared with the one-step method, and more importantly, it reduces the acid-dissolving phenomenon caused by the rubber mask being soaked in the acid solution for a long time. The temperature should not be higher than 70°C because of the accelerated acid dissolution of rubber at high temperature. In the second step, the temperature is selected to be 20-30° C., the concentration of hydrofluoric acid is 10-15 mol/L, and the acid etching rate is slow, so as to improve the control precision of the thickness of the final flexible beam.

现有的一步法,一般氢氟酸的浓度是15.6mol/L,温度为40℃,在这个条件下酸刻蚀摆片的挠性梁需要大约9~10小时,橡胶掩膜在此条件下浸泡9~10小时,酸溶尺寸可达2mm,这样引起的挠性梁刻蚀后边缘不整齐毛刺多。并且,由于石英摆片挠性梁的厚度要求为24~28um,以上述刻蚀速率估算所得刻蚀时间并不能精确控制其厚度,极易发生到达计算时间取出后摆片石英摆片挠性梁厚度不在24~28um范围内,导致摆片石英摆片挠性梁加工成品率低;此外氟硅橡胶掩膜在氢氟酸溶液中浸泡530min发生酸溶,一方面造成掩膜边缘渗酸使玻璃边缘出现毛刺,另一方面酸溶胶质粘附在石英摆片挠性梁表面引起酸蚀不均,造成石英摆片挠性梁厚度均匀性差。In the existing one-step method, the concentration of hydrofluoric acid is generally 15.6mol/L, and the temperature is 40°C. Under this condition, it takes about 9 to 10 hours to acid-etch the flexible beam of the pendulum piece. Under this condition, the rubber mask After soaking for 9 to 10 hours, the acid-soluble size can reach 2mm, and the edges of the flexible beams caused by this will be irregular and have many burrs after etching. Moreover, since the thickness of the flexible beam of the quartz pendulum is required to be 24-28um, the etching time estimated by the above etching rate cannot accurately control its thickness, and it is very easy to occur that the flexible beam of the quartz pendulum is taken out after the calculated time is reached. The thickness is not within the range of 24-28um, resulting in a low yield of the flexible beam of the quartz pendulum plate; in addition, the fluorosilicone rubber mask is soaked in the hydrofluoric acid solution for 530 minutes and acid-dissolved. There are burrs on the edge, and on the other hand, the acid soluble colloid adheres to the surface of the flexible beam of the quartz pendulum plate, causing uneven acid etching, resulting in poor thickness uniformity of the flexible beam of the quartz pendulum plate.

在快速刻蚀时,所述橡胶掩膜在18~22mol/L,50~70℃的条件下也会发生酸溶,但由于其浸泡时间短,发生酸溶的尺寸约为0.5mm。在慢速刻蚀时,在10~15mol/L,20~30℃条件,由于其温度、氢氟酸浓度低,并且浸泡时间小于1小时,几乎观测不到酸溶现象。During rapid etching, the rubber mask will also be acid-dissolved under the conditions of 18-22mol/L, 50-70°C, but due to its short immersion time, the acid-dissolved size is about 0.5mm. During slow etching, under the conditions of 10-15mol/L, 20-30°C, due to the low temperature and concentration of hydrofluoric acid, and the immersion time is less than 1 hour, almost no acid-dissolving phenomenon can be observed.

优选地,在所述快速刻蚀过程中,在所述第一氢氟酸溶液中放入第一玻璃陪片,通过计算所述第一玻璃陪片在所述第一氢氟酸溶液中的第一酸刻蚀速率,进行估算测试所述第一预设厚度的第一预设时间;Preferably, during the rapid etching process, a first glass companion is placed in the first hydrofluoric acid solution, and by calculating the a first acid etch rate, a first preset time for estimating and testing the first preset thickness;

优选地,在所述慢速刻蚀过程中,在所述第二氢氟酸溶液中放入第二玻璃陪片,通过计算所述第二玻璃陪片在所述第二氢氟酸溶液中的第二酸刻蚀速率,进行估算测试所述第二预设厚度的第二预设时间。Preferably, during the slow etching process, a second glass companion is placed in the second hydrofluoric acid solution, and by calculating the amount of the second glass companion in the second hydrofluoric acid solution The second acid etching rate is used to estimate and test the second preset thickness for a second preset time.

具体地,所述第一预设时间为180~300min;所述第二预设时间为30~50min。Specifically, the first preset time is 180-300 minutes; the second preset time is 30-50 minutes.

从而,能够大大缩短所述石英摆片挠性梁加工时所需要消耗的工时。Therefore, the man-hours required for processing the quartz pendulum plate flexible beam can be greatly shortened.

优选地,所述第一预设厚度为40~60μm。Preferably, the first preset thickness is 40-60 μm.

优选地,所述第二预设厚度为24~28μm。Preferably, the second preset thickness is 24-28 μm.

优选地,通过光纤光谱测厚装置或千分尺,测量所述石英摆片挠性梁的第一预设厚度和第二预设厚度。Preferably, the first preset thickness and the second preset thickness of the quartz pendulum flexible beam are measured by an optical fiber spectroscopic thickness measuring device or a micrometer.

优选地,通过氟硅橡胶掩膜将所述石英摆片挠性梁装模,形成工装好的石英摆片挠性梁。Preferably, the flexible beam of the quartz pendulum plate is molded through a fluorosilicone rubber mask to form the flexible beam of the quartz pendulum plate that has been tooled.

所述氟硅橡胶掩膜和与所述石英摆片挠性梁的工装结构(参见图2),所述氟硅橡胶掩膜2紧贴在所述石英摆片挠性梁1表面,仅在所述石英摆片挠性梁1处镂空,使其暴露在所述第一氢氟酸溶液和所述第二氢氟酸溶液中发生化学反应,从而减薄厚度。The fluorosilicone rubber mask and the tooling structure (see Fig. 2) with the flexible beam of the quartz pendulum plate, the fluorosilicone rubber mask 2 is close to the surface of the flexible beam 1 of the quartz pendulum plate, only The flexible beam 1 of the quartz pendulum plate is hollowed out so that it is exposed to the first hydrofluoric acid solution and the second hydrofluoric acid solution to undergo a chemical reaction, thereby reducing the thickness.

优选地,先用特制的酸蚀模具和氟硅橡胶掩膜将石英摆片挠性梁装模。为保证所述石英摆片挠性梁尺寸精度和表面质量,装模过程中需保证所述酸蚀模具、氟硅橡胶掩膜、所述石英摆片挠性梁三者的定位精度和所述石英摆片挠性梁表面的洁净度。Preferably, the flexible beam of the quartz pendulum plate is molded first with a special acid etching mold and a fluorosilicone rubber mask. In order to ensure the dimensional accuracy and surface quality of the flexible beam of the quartz pendulum plate, the positioning accuracy of the acid etching mold, the fluorosilicone rubber mask, and the flexible beam of the quartz pendulum plate and the The cleanliness of the surface of the flexible beam of the quartz pendulum.

优选地,将第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中时,使用去离子水冲洗残留酸液,并用无尘布吸干石英摆片挠性梁表面水分。从而能够避免从所述第一氢氟酸溶液中取出的石英摆片挠性梁,由于表面残留的第一氢氟酸溶液,而影响所述第二氢氟酸溶液的浓度。Preferably, when the flexible beam of the quartz pendulum plate with the first preset thickness is put into the second hydrofluoric acid solution, the residual acid solution is rinsed with deionized water, and the moisture on the surface of the flexible beam of the quartz pendulum plate is blotted dry with a dust-free cloth . Therefore, it can be avoided that the flexible beam of the quartz pendulum taken out from the first hydrofluoric acid solution affects the concentration of the second hydrofluoric acid solution due to the first hydrofluoric acid solution remaining on the surface.

优选地,在所述快速刻蚀过程中,在所述第一氢氟酸溶液中放入第一玻璃陪片,通过计算所述第一玻璃陪片在所述第一氢氟酸溶液中的第一酸刻蚀速率,进行估算测试所述第一预设厚度的时间;Preferably, during the rapid etching process, a first glass companion is placed in the first hydrofluoric acid solution, and by calculating the a first acid etch rate, the time for estimating and testing the first preset thickness;

优选地,在所述慢速刻蚀过程中,在所述第二氢氟酸溶液中放入第二玻璃陪片,通过计算所述第二玻璃陪片在所述第二氢氟酸溶液中的第二酸刻蚀速率,进行估算测试所述第二预设厚度的时间。Preferably, during the slow etching process, a second glass companion is placed in the second hydrofluoric acid solution, and by calculating the amount of the second glass companion in the second hydrofluoric acid solution The second acid etching rate is used to estimate the time for testing the second preset thickness.

优选地,在进行快速刻蚀时,所述石英摆片挠性梁竖直放置在所述第一氢氟酸溶液中。Preferably, when performing rapid etching, the flexible beam of the quartz pendulum plate is vertically placed in the first hydrofluoric acid solution.

优选地,在进行慢速刻蚀时,所述石英摆片挠性梁竖直放置在所述第二氢氟酸溶液中,从而保证挠性梁两侧反应产物均匀扩散。Preferably, when performing slow etching, the flexible beam of the quartz pendulum plate is vertically placed in the second hydrofluoric acid solution, so as to ensure uniform diffusion of reaction products on both sides of the flexible beam.

具体的工作步骤包括:将工装好的石英摆片挠性梁和第一玻璃陪片放入所述第一氢氟酸溶液中,在所述第一温度条件下进行快速刻蚀,刻蚀1小时后,将第一玻璃陪片取出,测量所述第一玻璃陪片的厚度,以此计算快速刻蚀速率v1;根据v1估算所述石英摆片挠性梁减薄至40~60μm的快速刻蚀时间t1,当快速刻蚀时间t1达到后,将其从第一氢氟酸溶液中取出,用去离子水冲洗干净,并用无尘布吸干所述石英摆片挠性梁表面水分;测量所述石英摆片挠性梁的厚度,如测量结果大于60μm则放回所述第一氢氟酸溶液中继续酸蚀;若测量结果在40~60μm范围内,则进行慢速刻蚀。在慢速刻蚀时,将快速刻蚀后的到达第一预设厚度的所述石英摆片挠性梁和第二玻璃陪片放入第二氢氟酸溶液中,在第二温度条件下,进行反应。刻蚀10分钟后,取出所述第二玻璃陪片,测量所述第二玻璃陪片厚度,以此计算慢速刻蚀速率v2;根据v2估算所述石英摆片挠性梁减薄至24~28μm的刻蚀时间t2,当到达第二步刻蚀时间t2后,将所述石英摆片挠性梁从所述第二氢氟酸溶液中取出,用去离子水冲洗干净,并用无尘布吸干石英摆片挠性梁表面水分,测量所述石英摆片挠性梁的厚度,如测量结果大于28μm则放回第二氢氟酸溶液中继续酸蚀;若测量结果在24~28um范围内,则慢速刻蚀完成。将所述石英摆片挠性梁从所述酸蚀模具和所述橡胶掩膜中拆卸出来,并清洗干净储存。The specific working steps include: putting the flexible beam of the quartz swing piece and the first glass companion piece into the first hydrofluoric acid solution, performing rapid etching under the first temperature condition, etching 1 Hours later, the first glass companion was taken out, and the thickness of the first glass companion was measured to calculate the rapid etching rate v1; according to v1, the fast rate at which the flexible beam of the quartz pendulum was thinned to 40-60 μm was estimated. Etching time t1, when the rapid etching time t1 is reached, take it out from the first hydrofluoric acid solution, rinse it with deionized water, and dry the surface moisture of the flexible beam of the quartz pendulum with a dust-free cloth; Measure the thickness of the flexible beam of the quartz pendulum plate, if the measurement result is greater than 60 μm, put it back into the first hydrofluoric acid solution to continue acid etching; if the measurement result is in the range of 40-60 μm, perform slow etching. When etching at a slow rate, put the flexible beam of the quartz pendulum plate and the second glass companion plate that have reached the first preset thickness after rapid etching into the second hydrofluoric acid solution, and under the second temperature condition , to react. After etching for 10 minutes, take out the second glass companion, and measure the thickness of the second glass companion, so as to calculate the slow etching rate v2; according to v2, estimate that the flexible beam of the quartz pendulum is thinned to 24 ~28μm etching time t2, when the second etching time t2 is reached, the flexible beam of the quartz pendulum plate is taken out from the second hydrofluoric acid solution, rinsed with deionized water, and cleaned with a dust-free Dry the moisture on the surface of the flexible beam of the quartz pendulum plate, measure the thickness of the flexible beam of the quartz pendulum plate, if the measurement result is greater than 28 μm, put it back into the second hydrofluoric acid solution to continue acid etching; if the measurement result is 24 ~ 28um Within the range, the slow etching is completed. The quartz pendulum flexible beam is disassembled from the acid etching mold and the rubber mask, cleaned and stored.

所述刻蚀速率(v1和v2)是指单位时间内石英摆片挠性梁双面厚度的去除量,单位为μm/min。The etching rate (v1 and v2) refers to the removal amount of the double-sided thickness of the flexible beam of the quartz pendulum plate per unit time, and the unit is μm/min.

通过本发明所提供的一种酸刻蚀石英摆片挠性梁的成形方法,不仅能够大大缩短所述石英摆片挠性梁加工时所需要消耗的工时,并且能够精确控制所述石英摆片挠性梁的厚度,减少所述石英摆片挠性梁加工中次品率,不同批次加工的摆片厚度重复性高。另一方面,能够减少所述氟硅橡胶掩膜边缘渗酸使玻璃边缘出现毛刺的现象,以及能够减少酸溶胶质粘附在所述石英摆片挠性梁表面引起酸蚀不均的现象,从而能够使酸刻蚀完成的所述石英摆片挠性梁厚度均匀、边缘缺陷减少。Through the forming method of the acid-etched quartz pendulum flexible beam provided by the present invention, not only can greatly shorten the man-hours required for processing the quartz pendulum flexible beam, but also can precisely control the quartz pendulum plate The thickness of the flexible beam reduces the defective rate in the processing of the quartz pendulum flexible beam, and the repeatability of the thickness of the pendulum plate processed in different batches is high. On the other hand, it can reduce the phenomenon of burrs on the edge of the glass due to acid seepage at the edge of the fluorosilicone rubber mask, and can reduce the phenomenon of uneven acid etching caused by the adhesion of acid sol colloid on the surface of the flexible beam of the quartz pendulum plate, Therefore, the thickness of the flexible beam of the quartz pendulum piece completed by acid etching can be uniform and the edge defects can be reduced.

本发明用来测量所述石英摆片挠性梁的厚度的方法,可以用光纤进行测量,也可以用千分尺进行测量。The method of the present invention for measuring the thickness of the flexible beam of the quartz pendulum plate can be measured by optical fiber or by a micrometer.

下面以厚度为720μm的石英摆片挠性梁,进行进一步说明。将工装好的厚度为720μm的石英摆片挠性梁,按照上述工艺流程进行反应,具体反应条件为:Further description will be given below using a flexible beam of a quartz pendulum plate with a thickness of 720 μm. The quartz pendulum flexible beam with a thickness of 720 μm after tooling was reacted according to the above process, and the specific reaction conditions were as follows:

实施例1:所述第一氢氟酸溶液的浓度为18.4mol/L,所述第二氢氟酸溶液的浓度为13.5mol/L;所述第一温度为50℃,所述第二温度为30℃;所述第一预设厚度为50μm,所述第二预设厚度为26μm。Embodiment 1: the concentration of the first hydrofluoric acid solution is 18.4mol/L, and the concentration of the second hydrofluoric acid solution is 13.5mol/L; the first temperature is 50°C, and the second temperature 30° C.; the first preset thickness is 50 μm, and the second preset thickness is 26 μm.

通过计算可以得知,所述快速刻蚀速率v1为2.65μm/min,所述慢速刻蚀速率v2为0.75μm/min。It can be known through calculation that the fast etching rate v1 is 2.65 μm/min, and the slow etching rate v2 is 0.75 μm/min.

在上述条件下,快速刻蚀过程中达到第一预设厚度所消耗的时间t1为252min,慢速刻蚀过程中达到第二预设厚度所消耗的时间t2为32min。将厚度为720μm的石英摆片挠性梁酸刻蚀至26μm,总消耗的时间为284min。Under the above conditions, the time t1 consumed to reach the first predetermined thickness during the fast etching process is 252 minutes, and the time t2 consumed to reach the second predetermined thickness during the slow etching process is 32 minutes. The flexible beam of the quartz pendulum with a thickness of 720 μm is acid-etched to 26 μm, and the total time consumed is 284 min.

实施例2:所述第一氢氟酸溶液的浓度为18.4mol/L,所述第二氢氟酸溶液的浓度为13.5mol/L;所述第一温度为60℃,所述第二温度为25℃;所述第一预设厚度为50μm,所述第二预设厚度为26μm。Embodiment 2: the concentration of the first hydrofluoric acid solution is 18.4mol/L, and the concentration of the second hydrofluoric acid solution is 13.5mol/L; the first temperature is 60°C, and the second temperature 25°C; the first preset thickness is 50 μm, and the second preset thickness is 26 μm.

通过计算可以得知,所述快速刻蚀速率v1为3.23μm/min,所述慢速刻蚀速率v2为0.5μm/min。It can be known through calculation that the fast etching rate v1 is 3.23 μm/min, and the slow etching rate v2 is 0.5 μm/min.

在上述条件下,快速刻蚀过程中达到第一预设厚度所消耗的时间t1为207min,慢速刻蚀过程中达到第二预设厚度所消耗的时间t2为48min。将厚度为720μm的石英摆片挠性梁酸刻蚀至26μm,总消耗的时间为255min。Under the above conditions, the time t1 taken to reach the first preset thickness during the fast etching process is 207 minutes, and the time t2 taken to reach the second preset thickness during the slow etching process is 48 minutes. The flexible beam of the quartz pendulum with a thickness of 720 μm is acid-etched to 26 μm, and the total consumption time is 255 min.

实施例3:所述第一氢氟酸溶液的浓度为20.7mol/L,所述第二氢氟酸溶液的浓度为13.5mol/L;所述第一温度为65℃,所述第二温度为25℃;所述第一预设厚度为50μm,所述第二预设厚度为26μm。Embodiment 3: the concentration of the first hydrofluoric acid solution is 20.7mol/L, and the concentration of the second hydrofluoric acid solution is 13.5mol/L; the first temperature is 65°C, and the second temperature 25°C; the first preset thickness is 50 μm, and the second preset thickness is 26 μm.

通过计算可以得知,所述快速刻蚀速率v1为3.64μm/min,所述慢速刻蚀速率v2为0.5μm/min。It can be known through calculation that the fast etching rate v1 is 3.64 μm/min, and the slow etching rate v2 is 0.5 μm/min.

在上述条件下,快速刻蚀过程中达到第一预设厚度所消耗的时间t1为184min,慢速刻蚀过程中达到第二预设厚度所消耗的时间t2为48min。将厚度为720μm的石英摆片挠性梁酸刻蚀至26μm,总消耗的时间为232min。Under the above conditions, the time t1 taken to reach the first preset thickness during the fast etching process is 184 minutes, and the time t2 taken to reach the second preset thickness during the slow etching process is 48 minutes. The flexible beam of the quartz pendulum with a thickness of 720 μm is acid-etched to 26 μm, and the total time consumed is 232 minutes.

从而,我们可以清楚的看到,本发明所公开的一种酸刻蚀石英摆片挠性梁的成形方法,将厚度为720μm的石英摆片挠性梁酸刻蚀至26μm,所消耗的时间为210min~350min。远远小于通过“一步法”进行酸刻蚀同样厚度的石英摆片挠性梁所消耗的时间。Therefore, we can clearly see that the acid etching of the flexible beam of the quartz pendulum plate with a thickness of 720 μm to 26 μm in the forming method of acid etching the flexible beam of the quartz pendulum plate disclosed in the present invention takes It is 210min~350min. It is far less than the time consumed by acid etching the flexible beam of the quartz pendulum with the same thickness by the "one-step method".

本发明所公开的一种酸刻蚀石英摆片挠性梁的成形方法,慢速刻蚀速率较慢,所以比较容易控制所述慢速刻蚀步骤中,达到第二预设厚度的时间。能够将所述石英摆片挠性梁的厚度控制精度提高至±1μm。The slow etching rate of the acid-etched quartz pendulum flexible beam disclosed in the present invention is relatively slow, so it is relatively easy to control the time for reaching the second predetermined thickness in the slow etching step. The thickness control accuracy of the quartz pendulum flexible beam can be improved to ±1 μm.

并且在所述第一氢氟酸溶液中反应的时间较短,从而能够避免橡胶掩膜酸溶造成的石英摆片挠性梁厚度不均和玻璃边缘毛刺。And the reaction time in the first hydrofluoric acid solution is relatively short, so that the uneven thickness of the flexible beam of the quartz pendulum plate and the burr on the edge of the glass caused by the acid dissolution of the rubber mask can be avoided.

本发明中的通过光纤进行测量的设备为在线厚度测量装置(具体请参见图3),所述光纤光谱测厚装置包括光纤光谱仪6、光源5、模具固定底座和光纤测量探头3,所述光纤光谱仪6和光源分别经光纤4与所述光纤测量探头3连接,所述模具固定底座用于固定所述石英摆片绕性梁1,所述光纤测量探头3垂直设置在固定在所述模具固定底座上的所述石英摆片绕性梁1的一侧。所述石英摆片挠性梁1前后两面均反射光源,反射信号经所述光纤4传导至所述光纤光谱仪6,经过计算处理便可得所述石英摆片挠性梁1的厚度,其值显示并储存于所述计算机中,输入所述酸刻蚀速率便可计算第一预设时间和第二预设时间。The equipment for measuring by optical fiber in the present invention is an online thickness measuring device (see Fig. 3 for details), and the optical fiber spectrum thickness measuring device includes an optical fiber spectrometer 6, a light source 5, a mold fixing base and an optical fiber measuring probe 3, and the optical fiber The spectrometer 6 and the light source are respectively connected to the optical fiber measuring probe 3 via the optical fiber 4, the mold fixing base is used to fix the quartz pendulum plate winding beam 1, and the optical fiber measuring probe 3 is vertically arranged on the mold fixed The quartz pendulum on the base is wound around one side of the beam 1 . The front and rear sides of the quartz pendulum flexible beam 1 all reflect the light source, and the reflected signal is transmitted to the optical fiber spectrometer 6 through the optical fiber 4, and the thickness of the quartz pendulum flexible beam 1 can be obtained through calculation and processing, and its value Displayed and stored in the computer, the first preset time and the second preset time can be calculated by inputting the acid etching rate.

具体地,连接所述光纤光谱仪6和所述光纤测量探头3的光纤4为第一光纤,连接所述光源5和所述光纤测量探头3的光纤4为第二光纤,所述第二光纤为导光光纤,从而,能够将所述光源5发出的光传递到所述光纤测量探头3处。所述光纤测量探头3处的光照射在所述石英摆片绕性梁1上时,一部分经所述石英摆片绕性梁1的第一面反射,所述反射信息传递给所述光纤测量探头3,然后经第一光纤传递给光纤光谱仪6,一部分经所述石英摆片绕性梁1的第二面反射,所述反射信息也经第一光纤传递给光纤光谱仪6,然后传递给计算机7,计算机7根据上述反射信息计算所述石英摆片绕性梁1的厚度。Specifically, the optical fiber 4 connecting the optical fiber spectrometer 6 and the optical fiber measuring probe 3 is a first optical fiber, the optical fiber 4 connecting the light source 5 and the optical fiber measuring probe 3 is a second optical fiber, and the second optical fiber is The light-guiding optical fiber can transmit the light emitted by the light source 5 to the optical fiber measuring probe 3 . When the light at the optical fiber measuring probe 3 is irradiated on the quartz pendulum plate winding beam 1, part of it is reflected by the first surface of the quartz pendulum plate winding beam 1, and the reflection information is transmitted to the optical fiber measurement The probe 3 is then transmitted to the fiber optic spectrometer 6 through the first optical fiber, and a part is reflected by the second surface of the quartz pendulum around the beam 1, and the reflection information is also transmitted to the fiber optic spectrometer 6 through the first optical fiber, and then transmitted to the computer 7. The computer 7 calculates the thickness of the quartz pendulum piece around the flexible beam 1 according to the above reflection information.

通过所述光纤测厚装置的设置,能够对所述石英摆片绕性梁1的厚度进行实施测量,能够将所述石英摆片绕性梁1的厚度测量精度提高至±1μm。Through the arrangement of the optical fiber thickness measuring device, the thickness of the quartz pendulum plate winding beam 1 can be measured, and the thickness measurement accuracy of the quartz pendulum plate winding beam 1 can be improved to ±1 μm.

以上所述,仅是本发明的较佳实施例而已,并非对本发明作任何形式上的限制,依据本发明的技术实质对以上实施例所作的任何简单修改、等同变化与修饰,均仍属于本发明技术方案的范围内。The above are only preferred embodiments of the present invention, and are not intended to limit the present invention in any form. Any simple modifications, equivalent changes and modifications made to the above embodiments according to the technical essence of the present invention still belong to the present invention. within the scope of the technical solution of the invention.

Claims (10)

1.一种酸刻蚀石英摆片挠性梁的成形方法,其特征在于,包括以下步骤:1. a forming method of acid etching quartz pendulum plate flexible beam, is characterized in that, comprises the following steps: 第一步:将工装好的石英摆片挠性梁放入第一氢氟酸溶液中,在第一温度条件下,进行快速刻蚀,直至所述石英摆片挠性梁达到第一预设厚度;The first step: Put the flexible beam of the quartz pendulum plate into the first hydrofluoric acid solution, and perform rapid etching under the first temperature condition until the flexible beam of the quartz pendulum plate reaches the first preset value. thickness; 第二步:将所述第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中,在第二温度条件下,进行慢速刻蚀,直至所述石英摆片挠性梁达到第二预设厚度;Step 2: Put the flexible beam of the quartz pendulum plate with the first preset thickness into the second hydrofluoric acid solution, and perform slow etching under the second temperature condition until the quartz pendulum plate is flexible. the beam reaches a second preset thickness; 其中:所述第一氢氟酸溶液的浓度大于所述第二氢氟酸溶液的浓度,所述第一氢氟酸溶液的浓度小于22mol/L;Wherein: the concentration of the first hydrofluoric acid solution is greater than the concentration of the second hydrofluoric acid solution, and the concentration of the first hydrofluoric acid solution is less than 22mol/L; 所述第一温度高于所述第二温度。The first temperature is higher than the second temperature. 2.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,2. the forming method of acid etching quartz pendulum piece flexible beam according to claim 1, is characterized in that, 所述第一氢氟酸溶液的浓度的18~22mol/L;18-22mol/L of the concentration of the first hydrofluoric acid solution; 所述第二氢氟酸溶液的浓度为10~15mol/L。The concentration of the second hydrofluoric acid solution is 10-15 mol/L. 3.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,3. the forming method of acid etching quartz pendulum piece flexible beam according to claim 1, is characterized in that, 所述第一温度为50~70℃;The first temperature is 50-70°C; 所述第二温度为20~30℃。The second temperature is 20-30°C. 4.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,4. the forming method of acid etching quartz pendulum piece flexible beam according to claim 1, is characterized in that, 在所述快速刻蚀过程中,在所述第一氢氟酸溶液中放入第一玻璃陪片,通过计算所述第一玻璃陪片在所述第一氢氟酸溶液中的第一酸刻蚀速率,进行估算测试所述第一预设厚度的第一预设时间;In the rapid etching process, the first glass companion is placed in the first hydrofluoric acid solution, and the first acid of the first glass companion in the first hydrofluoric acid solution is calculated Etching rate, the first preset time for estimating and testing the first preset thickness; 在所述慢速刻蚀过程中,在所述第二氢氟酸溶液中放入第二玻璃陪片,通过计算所述第二玻璃陪片在所述第二氢氟酸溶液中的第二酸刻蚀速率,进行估算测试所述第二预设厚度的第二预设时间。In the slow etching process, put a second glass companion in the second hydrofluoric acid solution, by calculating the second glass companion in the second hydrofluoric acid solution The acid etching rate is estimated and tested for a second preset time for the second preset thickness. 5.根据权利要求4所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,5. the forming method of acid etching quartz pendulum piece flexible beam according to claim 4, is characterized in that, 所述第一预设时间为180~300min;The first preset time is 180-300 minutes; 所述第二预设时间为30~50min。The second preset time is 30-50 minutes. 6.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,6. the forming method of acid etching quartz pendulum plate flexible beam according to claim 1, is characterized in that, 通过光纤光谱测厚装置,测量所述石英摆片挠性梁的第一预设厚度和第二预设厚度;Measuring the first preset thickness and the second preset thickness of the quartz pendulum flexible beam through an optical fiber spectroscopic thickness measuring device; 所述光纤光谱测厚装置包括光纤光谱仪、光源、模具固定底座和光纤测量探头,所述光纤光谱仪和光源分别经光纤与所述光纤测量探头连接,所述模具固定底座用于固定所述石英摆片绕性梁,所述光纤测量探头垂直设置在固定在所述模具固定底座上的所述石英摆片绕性梁的一侧。The optical fiber spectrum thickness measuring device includes a fiber optic spectrometer, a light source, a mold fixing base and an optical fiber measuring probe, the fiber optic spectrometer and the light source are respectively connected to the optical fiber measuring probe through an optical fiber, and the mold fixing base is used to fix the quartz pendulum A sheet-wound beam, the optical fiber measuring probe is vertically arranged on one side of the quartz pendulum sheet-wound beam fixed on the mold fixing base. 7.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,7. the forming method of acid etching quartz pendulum plate flexible beam according to claim 1, is characterized in that, 所述第一预设厚度为40~60μm;The first preset thickness is 40-60 μm; 所述第二预设厚度为24~28μm。The second preset thickness is 24-28 μm. 8.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,8. the forming method of acid etching quartz pendulum plate flexible beam according to claim 1, is characterized in that, 通过氟硅橡胶掩膜将所述石英摆片挠性梁装模,形成工装好的石英摆片挠性梁。The flexible beam of the quartz pendulum plate is molded through a fluorosilicone rubber mask to form the flexible beam of the quartz pendulum plate that has been tooled. 9.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,9. the forming method of acid etching quartz pendulum plate flexible beam according to claim 1, is characterized in that, 将第一预设厚度的石英摆片挠性梁放入第二氢氟酸溶液中时,使用去离子水冲洗残留酸液,并用无尘布吸干石英摆片挠性梁表面水分。When putting the flexible beam of the quartz pendulum plate with the first predetermined thickness into the second hydrofluoric acid solution, rinse the residual acid solution with deionized water, and dry the surface moisture of the flexible beam of the quartz pendulum plate with a dust-free cloth. 10.根据权利要求1所述的酸刻蚀石英摆片挠性梁的成形方法,其特征在于,10. the forming method of acid etching quartz pendulum plate flexible beam according to claim 1, is characterized in that, 在进行快速刻蚀时,所述石英摆片挠性梁竖直放置在所述第一氢氟酸溶液中;When performing rapid etching, the flexible beam of the quartz pendulum plate is vertically placed in the first hydrofluoric acid solution; 在进行慢速刻蚀时,所述石英摆片挠性梁竖直放置在所述第二氢氟酸溶液中。When performing slow etching, the flexible beam of the quartz pendulum is vertically placed in the second hydrofluoric acid solution.
CN201410689983.4A 2014-11-25 2014-11-25 Method for forming acid-etching quartz pendulous reed flexible beam Pending CN104478224A (en)

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