CN104473857B - 一种炫彩啫喱及其制备方法 - Google Patents

一种炫彩啫喱及其制备方法 Download PDF

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CN104473857B
CN104473857B CN201410682711.1A CN201410682711A CN104473857B CN 104473857 B CN104473857 B CN 104473857B CN 201410682711 A CN201410682711 A CN 201410682711A CN 104473857 B CN104473857 B CN 104473857B
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邓伟健
罗平
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GUANGZHOU SHENCAI COSMETICS Co Ltd
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Abstract

本发明提供了一种炫彩啫喱及其制备方法，其包括以下重量百分比的组分：甘油20.0％～25.0％，丙二醇20.0％～25.0％，海藻提取物1.0％，EDTA‑二钠0.05％，尿囊素0.06％，透明质酸钠0.05％，环五聚二甲基硅氧烷20.0％～30.0％，聚二甲基硅氧烷5.0％～10.0％，丙烯酸钠/丙烯酰二甲基牛磺酸钠共聚物0.5％～1.0％，异十六烷0.25％～0.5％，聚山梨醇酯‑800.2％～0.4％，可溶性胶原1.5％，辛甘醇0.5％，水余量。本发明还提供了该炫彩啫哩的制备方法。本发明的炫彩啫哩保湿性能优异，能够持续滋润肌肤，安全健康。

Description

一种炫彩啫喱及其制备方法
技术领域
本发明属于化妆品领域，具体涉及一种炫彩护肤啫喱，以及该炫彩护肤啫喱的制备方法。
背景技术
目前市场上销售的透明啫喱主要有两大类，一类是水性啫喱，以水溶性高分子材料作为增稠剂，配合各种水溶性成分配制而成的；另一类是油性凝胶啫喱，它以油性的原料为主要成分。这两种啫喱存在以下的缺陷：(1)水性啫喱只能添加水溶性的原料，油性凝胶啫喱只能添加油性的成分，这样配方的成分选择会受到很大的限制；(2)水性啫喱只能添加水溶性的成分，所以滋润度比较差，油性凝胶啫喱只能添加油性的成分，存在肤感粘腻、堵塞毛孔的问题；(3)一般情况下都需要添加防腐剂来确保产品不被污染；(4)需要添加有机色素或者无机色素才能达到彩色的效果。
发明内容
本发明的一个目的是针对以上要解决的技术问题，提供一种外观炫彩、保湿性能好、油分含量高、不含防腐剂的透明护肤啫喱。
本发明的另一个目的是提供上述炫彩啫喱的制备方法。
为达到以上目的，本发明提供了一种炫彩啫哩，其由以下重量百分比的组分组成：甘油20.0％～25.0％，丙二醇20.0％～25.0％，海藻提取物1.0％，EDTA-二钠0.05％，尿囊素0.06％，透明质酸钠0.05％，环五聚二甲基硅氧烷20.0％～30.0％，聚二甲基硅氧烷5.0％～10.0％，丙烯酸钠/丙烯酰二甲基牛磺酸钠共聚物0.5％～1.0％，异十六烷0.25％～0.5％，聚山梨醇酯-800.2％～0.4％，可溶性胶原1.5％，辛甘醇0.5％，水余量。
本发明还提供了所述炫彩啫喱的制备方法，其步骤如下：
(1)将透明质酸钠用丙二醇润湿，然后加入水相锅中，开启搅拌，依次加入水、甘油、海藻提取物、EDTA-二钠、尿囊素，升温至80℃，保温10分钟；
(2)将聚二甲基硅氧烷和部分环五聚二甲基硅氧烷依次加入乳化锅中，开启搅拌，混合均匀，并升温至70℃；
(3)将剩下的环五聚二甲基硅氧烷、丙烯酸钠/丙烯酰二甲基牛磺酸钠共聚物、异十六烷和聚山梨醇酯-80混合均匀，然后加入乳化锅中，搅拌均匀；
(4)乳化锅的搅拌速度保持在300转/分钟，将步骤(1)的混合物通过真空吸入，保持 真空，均质5分钟；
(5)搅拌降温至45℃以下时，加入辛甘醇和可溶性胶原，均质并搅拌均匀；降至38℃时出料。
优选地，步骤(2)所用的环五聚二甲基硅氧烷占全部环五聚二甲基硅氧烷的重量百分比为95～97％。
与现有技术相比，本发明的护肤啫喱克服了传统啫喱的种种缺点，采用先进的凝胶配方体系，通过调整水相和油相的折光率，呈现淡紫色，美观时尚；本发明同时含有大量滋润油脂，能够结合长效和短效的双重高效保湿成分，保湿性能优异(24小时持续保湿)，显著增加肌肤角质层含水量。此外，本发明配合特殊的增稠乳化体系，产品质感爽滑，具有丝绒般的肤感，且不含防腐剂，安全环保。
具体实施方式
下面结合具体实施例对本发明的技术方案做进一步的详述，但本发明的保护范围并不仅限于以下实施例。
按照以下重量百分比称量各组分，以下各组分均可通过商业渠道购买获得。
制作实施例1～3的炫彩护肤啫喱，其步骤如下：
(1)将A组分中的透明质酸钠用丙二醇润湿，然后加入水相锅中，开启搅拌，依次加入其它余下的A组分，升温至80℃，保温10分钟；
(2)将B组分的原料依次加入乳化锅中，开启搅拌，混合均匀，并升温至70℃；
(3)将C组分混合均匀，然后加入乳化锅中，搅拌均匀；
(4)乳化锅的搅拌速度保持在300转/分钟，将A组分通过真空吸入，保持真空，均质5分钟；
(5)搅拌降温至45℃以下时，加入D组分，均质并搅拌均匀；降至38℃时出料。
(6)检验合格，出料灌装。产物外观透明、呈现浅紫色。
测试效果实施例：
1.保湿性能测试：根据QB/T 4256-2011《化妆品保湿功效评价指南》的方法，对实施例1～3的炫彩啫哩进行“人体功效试验8小时保湿”测试，测试结果如下：
说明：统计方法：“*”为单因素方差分析；“**”为独立样本t检验，P值<0.05，则有显著性差异。
2.刺激性评估(人体皮肤斑贴试验结果)
(1)受试物：本发明实施例1～3的炫彩啫哩化妆品终产品。
(2)阴性对照：空白对照。
(3)受试者：共25人，男12人，女13人，年龄18～30岁，符合受试者志愿入选标准。
(4)斑试方法：选用合格的斑试器，以封闭式斑贴试验方法，将受试物约0.02ml～0.025ml涂于斑试器内，外用专用胶带贴敷于受试者前臂曲侧，24小时后去除受试物，于去除受试物斑试器后30min，待压痕消失后观察皮肤反应，按《化妆品卫生规范》(2007年版)中皮肤反应分级标准记录其结果。
(5)结果评价：按下表(皮肤不良反应分级标准)记录反应结果。
(6)试验结果见下表：
以上结果显示：实施例1、2、3中，25名受试者皮肤全部呈阴性反应(评分等级：0级)。依据《化妆品卫生规范》(2007年版)人体皮肤班贴试验判断标准，样品对人体无皮肤不良反应。
由以上测试结果可见，本发明实施例1～2的炫彩护肤啫喱外观透明，通过调整水相和油相的折光率，呈现淡紫色，美观时尚，同时含有大量滋润油脂，结合长效和短效的双重高效保湿成分，保湿性能优异，此外，本发明配合特殊的增稠乳化体系，产品质感爽滑，且不含防腐剂，安全环保。

Claims (3)

1.一种炫彩啫喱，其特征在于包括以下重量百分比的组分：甘油20.0％～25.0％，丙二醇20.0％～25.0％，海藻提取物1.0％，EDTA-二钠0.05％，尿囊素0.06％，透明质酸钠0.05％，环五聚二甲基硅氧烷20.0％～30.0％，聚二甲基硅氧烷5.0％～10.0％，丙烯酸钠/丙烯酰二甲基牛磺酸钠共聚物0.5％～1.0％，异十六烷0.25％～0.5％，聚山梨醇酯-800.2％～0.4％，可溶性胶原1.5％，辛甘醇0.5％，水 余量。
2.权利要求1所述炫彩啫喱的制备方法，其步骤如下：
(1)将透明质酸钠用丙二醇润湿，然后加入水相锅中，开启搅拌，依次加入水、甘油、海藻提取物、EDTA-二钠、尿囊素，升温至80℃，保温10分钟；
(2)将聚二甲基硅氧烷和部分环五聚二甲基硅氧烷依次加入乳化锅中，开启搅拌，混合均匀，并升温至70℃；
(3)将剩下的环五聚二甲基硅氧烷、丙烯酸钠/丙烯酰二甲基牛磺酸钠共聚物、异十六烷和聚山梨醇酯-80混合均匀，然后加入乳化锅中，搅拌均匀；
(4)乳化锅的搅拌速度保持在300转/分钟，将步骤(1)的混合物通过真空吸入，保持真空，均质5分钟；
(5)搅拌降温至45℃以下时，加入辛甘醇和可溶性胶原，均质并搅拌均匀；降至38℃时出料。
3.根据权利要求2所述的方法，其特征在于：步骤(2)所用的环五聚二甲基硅氧烷占全部环五聚二甲基硅氧烷的重量百分比为95～97％。
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CN105726394A (zh) * 2016-03-02 2016-07-06 佛山市万盈化妆品有限公司 一种含骨胶原的面部啫喱
CN105726395A (zh) * 2016-03-02 2016-07-06 佛山市万盈化妆品有限公司 一种含骨胶原的面部啫喱的制备方法
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