CN104436116A - Rosemary foot bath powder and preparation method thereof - Google Patents
Rosemary foot bath powder and preparation method thereof Download PDFInfo
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- CN104436116A CN104436116A CN201410652569.6A CN201410652569A CN104436116A CN 104436116 A CN104436116 A CN 104436116A CN 201410652569 A CN201410652569 A CN 201410652569A CN 104436116 A CN104436116 A CN 104436116A
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- A61K36/18—Magnoliophyta (angiosperms)
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Abstract
The invention discloses rosemary foot bath powder and a preparation method thereof. The rosemary foot bath powder disclosed by the invention comprises the following components in parts by weight: 10-25 parts of rosemary, 3-10 parts of geranium, 3-8 parts of pogostemon cablin, 4-9 parts of folium cortex eucommiae, 1-3 parts of grape pip, 1-5 parts of rose, and 2-6 parts of ginger powder. The preparation method disclosed by the invention comprises the steps of removing impurities, air-drying, fermenting, sterilizing, carrying out enzymolysis, drying, compounding and crushing. The rosemary foot bath powder disclosed by the invention is rapid to take effect and has much soluble substances; and the rosemary foot bath powder can have a better health effect without being soaked for a long time and is short in use period and low in cost.
Description
Technical field
The invention belongs to Chinese medicine health care product technical field, be specifically related to a kind of Herba Rosmarini Officinalis lavipeditum powder and preparation method thereof.
Background technology
In the traditional Chinese medical science, foot bath is one of method of disease therapy, belongs to the one of inner disease outer treat, and it comes from China's ancient times, is the experience that China working people sums up out in long-term practice.Song dynasty Soviet Union and Eastern Europe is said on slope " heating bath foot method, its effect is not just very felt, but accumulates over one hundred day, and function can not be measured, and takes medicine than it, and it imitates Radix Achyranthis Bidentatae ".Often some Chinese medicine ingredients with health role are added in hot water in foot bath process, by warm-heat effect, mechanism, the chemical action of water and smoke the therapeutical effect washed by medicine steam and medicinal liquid, can dredge and give reason, loose wind cooling, thoroughly reach muscles and bones, regulate the flow of vital energy and blood, thus reach the object strengthening cardiovascular and cerebrovascular vessel function, improving water flood, allaying tiredness.
Current lavipeditum powder comprises Chinese medicinal foot bath powder and chemical synthetic drug lavipeditum powder.Chemical synthetic drug lavipeditum powder is mainly used in skin diseases such as treatment beriberi, tinea pedis etc., Chinese herbal medicine lavipeditum powder is the lavipeditum powder kind that current field of health care products generally uses and accepted extensively by consumer, annual use amount is large, price is high, and life-time service can reach the conditioning health-care effect of corresponding Chinese herbal medicine.Chinese herbal medicine is carried out drying by traditional Chinese herbal medicine lavipeditum powder usually, the rear directly aseptic packaging of pulverizing becomes lavipeditum powder, medicinal herb components carries out simple pulverizing can not destroy plant cell wall completely, effective ingredient stripping quantity in Chinese medicine is few, the higher water temperature long period is needed to soak ability stripping part Effective Component of Chinese Medicine in use procedure, take effect slow, life cycle is long, and cost is high.
Summary of the invention
For solving the problems of the technologies described above, the present invention aims to provide a kind of instant effect, and leachable is more, soaks the lavipeditum powder product that can reach better effects without the need to the long period; This product life cycle is short and cost is low.
The present invention is achieved through the following technical solutions.
A kind of Herba Rosmarini Officinalis lavipeditum powder, comprises the material composition of following weight portion: Herba Rosmarini Officinalis 10-25 part; Flos Pelargonii 3-10 part; Herba Pogostemonis 3-8 part; Folium Eucommiae 4-9 part; Semen Vitis viniferae 1-3 part; Flos Rosae Rugosae 1-5 part; Rhizoma Zingiberis Recens powder 2-6 part.
One of preferably, the weight portion of each material consists of: Herba Rosmarini Officinalis 15-22 part; Flos Pelargonii 5-8 part; Herba Pogostemonis 5-7 part; Folium Eucommiae 5-8 part; Semen Vitis viniferae 1-2 part; Flos Rosae Rugosae 2-4 part; Rhizoma Zingiberis Recens powder 3-5 part.
Preferably two, the weight portion of each material consists of: Herba Rosmarini Officinalis 15 parts; Flos Pelargonii 5 parts; Herba Pogostemonis 5 parts; Folium Eucommiae 5 parts; Semen Vitis viniferae 1 part; Flos Rosae Rugosae 2 parts; Rhizoma Zingiberis Recens powder 3 parts.
Preferably three, the weight portion of each material consists of: Herba Rosmarini Officinalis 20 parts; Flos Pelargonii 6 parts; Herba Pogostemonis 6 parts; Folium Eucommiae 7 parts; Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts.
The preparation method of Herba Rosmarini Officinalis lavipeditum powder, comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.
Described concrete steps are as follows:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity, Flos Pelargonii, Herba Pogostemonis, Folium Eucommiae press formula proportion mix homogeneously, be crushed to 10-20 order, spray sterilized water, adjustment moisture is to 25%-35%, 0.05%-0.15% accesses EM microbial inoculum in mass ratio, constant temperature and humidity fermentation 10-20h;
(4) sterilizing: by the material sterilizing 10-30min fermented in step (3), for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, 30-35 DEG C of enzymolysis 2-5h, enzyme denaturing, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying or hot air drying, being dried to moisture is that less than 10% stopping is dry;
(7) composite: the Semen Vitis viniferae of dried material and formula proportion, Flos Rosae Rugosae, Rhizoma Zingiberis Recens powder are mixed homogeneously, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 200-300 order.
Concrete, the sterilizing methods described in step (3) is microwave sterilizating, and sterilising temp is 50-100 DEG C.
Concrete, the microwave drying condition described in step (6) is microwave dose 0.027-0.033kw/kg, baking temperature 65-80 DEG C.
Concrete, the microwave drying described in step (6) is intermittent pulse microwave drying, and microwave dose is 0.027-0.033kw/kg, and baking temperature is 45-55 DEG C, and microwave effective time accounts for the 50%-70% of total contribution time.
The present invention for base material, is equipped with Flos Pelargonii, Herba Pogostemonis, Folium Eucommiae with Herba Rosmarini Officinalis, through remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverize after composite with Semen Vitis viniferae, Flos Rosae Rugosae, Rhizoma Zingiberis Recens powder.Herba Rosmarini Officinalis is the plant of a kind of high antioxidant of generally acknowledging at present, is rich in the compositions such as carnosic acid, carnosol, rosmanol, ursolic acid, rosmarinic acid, effectively can removes interior free yl, has anti-swollen effect such as antiinflammatory, antitumor.Herba Rosmarini Officinalis bases substance contained in Herba Rosmarini Officinalis strengthens corticocerebral process always anticonvulsant effect, and the volatile essential oil in Herba Rosmarini Officinalis has significant antibacterial action to staphylococcus aureus, escherichia coli, cholera bacilli etc.Therefore, adopting Herba Rosmarini Officinalis to do base material can effectively suppress foot bacterial reproduction, has good effect to the beriberi, tinea pedis etc. that antibacterial, fungus etc. cause.Herba Pogostemonis has another name called extra large Herba Pogostemonis, being the dry aerial parts of labiate Herba Pogostemonis, is famous and precious plant perfume, is again common Chinese crude drug, there is eliminating turbid pathogen with aromatics, the preventing or arresting vomiting that whets the appetite, deliver effect of expelling summer-heat, be usually used in treatment turbid damp obstructing in middle-JIAO, heat-damp in summer asthenia, uncomfortable in chestly do not relax, stomachache tells diseases such as letting out.Flos Pelargonii has another name called fish pelargonium, has strong fragrance, is the plant that a kind of essential oil content is higher, and wherein extracted quintessence oil is a kind of emotion balance agent preferably, and energy is allaying tiredness preferably, has the functions such as resisting oxidation and delaying senility.Folium Eucommiae is the leaf of the Eucommiaceae plant Cortex Eucommiae, be the distinctive economic tree of China, Folium Eucommiae is a kind of traditional Chinese medicine, and research finds that Folium Eucommiae extract can the synthesis Sum decomposition of protein collagen in effect on human body skeleton and muscle, there is promotion metabolism, the function of prevention of osteoporosis.Containing higher chlorogenic acid in Folium Eucommiae, there is function of gallbladder promoting, blood pressure lowering, the effect such as antibacterial, there is higher antioxidant activity simultaneously, be applied in the antioxidation of food.The present invention by Herba Rosmarini Officinalis, Herba Pogostemonis, Flos Pelargonii, Folium Eucommiae mix, the antioxidant activity of extractum can be increased, better reach sterilization, antiinflammatory, antioxidative effect, be rich in various plants derived essential oil in the present invention simultaneously and can promote that Skin Cell regenerates, make skin more smooth, fine and smooth, prevent xerosis cutis from chapping.
The present invention by Herba Rosmarini Officinalis, Flos Pelargonii, Herba Pogostemonis, to ferment after Folium Eucommiae combination drying, sweat adjustment moisture is 25%-35%, too much juice is avoided to take away effective ingredient in product, produce some humic acid materials in sweat, effectively increase the effect of product bactericidal antiphlogistic.Adopt cellulase after material sterilizing after having fermented, protease composite enzyme system carries out enzymolysis, macromole cellulose, protein etc. in raw material are carried out enzymolysis, produce the compositions such as multiple micromolecule polypeptide, aminoacid, vegetable polysaccharides, effectively can increase the dissolving of product effective ingredient, while ensureing drug effect, increase the skin care effect of product of the present invention.
Semen Vitis viniferae, Flos Rosae Rugosae, Rhizoma Zingiberis Recens powder add after other fermenting raw materials, ensure that the original character of this type of raw material, reach the object of invigorating blood circulation, dispeling cold.
For verifying effect of the present invention, applicant measures water extraction content of the present invention, inhibition zone size, antiphlogistic effects, free radical scavenging activity, measuring method and measurement result as follows:
One, lavipeditum powder water extraction assay of the present invention
The lavipeditum powder prepared using the present invention as test group, not enzymolysis as a control group 1, azymic as a control group 2, enzymolysis, azymic are not matched group 3, and all matched groups all adopt formula of the present invention, and other technique is identical with present invention process; Adopt weight method to measure water extraction content, get 3g trial target respectively, add boiling water 200mL, soak 45min, filter, weigh filtering residue weight, calculate extract content, measurement result is as shown in table 1 below.
Table 1 the present invention and controlled trial water extraction content
| Test group | Matched group 1 | Matched group 2 | Matched group 3 | |
| Extract content (%) | 42.1 | 34.2 | 30.1 | 22.7 |
As shown in Table 1, in lavipeditum powder immersion process prepared by the present invention, water extraction content is apparently higher than other 3 groups of control sample, pulverize merely, enzymolysis, azymous matched group 3 sample water extract content are not minimum, it can thus be appreciated that carried out by lavipeditum powder fermenting, enzymolysis can effectively increase water extraction content, and apparently higher than only carrying out the lavipeditum powder product of physical pulverization.
Two, lavipeditum powder antibacterial tests of the present invention
The lavipeditum powder prepared using the present invention as test group, not enzymolysis as a control group 1, azymic as a control group 2, enzymolysis, azymic are not matched group 3, and all matched groups all adopt formula of the present invention, and other technique is identical with present invention process; Detect the inhibition zone size of each group of lavipeditum powder to different mushroom, measure antibacterial circle diameter size as a result, measurement result is as shown in table 2.
Table 2 difference group lavipeditum powder inhibition zone size
As shown in Table 2, test group lavipeditum powder all has obvious Developing restraint effect to surveyed various mushroom, and test group product antibacterial circle diameter is maximum, and the lavipeditum powder of matched group 3 is only pulverized, inhibition zone is less, though there is fungistatic effect, but effect is poor, through lavipeditum powder of the present invention and the test group of enzymolysis, fermentation procedure, have good fungistatic effect, inhibition zone is maximum.It can thus be appreciated that, the bactericidal effect that the present invention has had.Result shows: lavipeditum powder of the present invention all has good bacteriostasis to staphylococcus aureus, escherichia coli, trichophyton, candidiasis, Trichophyton floccosum, can be applicable to the auxiliary treatment of tinea pedis, beriberi, tinea unguium, skin pruritus etc.
Three, lavipeditum powder antiphlogistic effects of the present invention
The lavipeditum powder that anti-inflammation test is prepared using the present invention as test group, not enzymolysis as a control group 1, azymic as a control group 2, enzymolysis, azymic are not matched group 3, and all matched groups all adopt formula of the present invention, and other technique is identical with present invention process; Measure different product to the impact of mouse ear swelling test small mouse inhibitory rate of intumesce, test shows that four groups of samples all obviously can suppress the ear thickness of mouse ear swelling test small mouse, and test group suppression ratio is apparently higher than other three matched group products, and minimum with matched group 3 suppression ratio.Result of the test is as shown in table 3.
Table 3 difference group lavipeditum powder is on the impact of mouse ear swelling test
Note: " * * " shows and to compare with model control group, P<0.01.
Four, lavipeditum powder of the present invention is to free radical scavenging activity effect test
The lavipeditum powder that free radical scavenging activity test is prepared using the present invention is as test group, not enzymolysis as a control group 1, azymic as a control group 2, enzymolysis, azymic are not matched group 3, all matched groups all adopt formula of the present invention, and other technique is identical with present invention process; Checking lavipeditum powder is on the impact of hydroxyl radical free radical, DPPH, superoxide radical clearance rate, and testing result is as shown in table 4.
Table 4 difference group lavipeditum powder is to the comparison of free radical scavenging efficiency
| Free radical | Test group | Matched group 1 | Matched group 2 | Matched group 3 |
| Hydroxyl radical free radical clearance rate (%) | 34.00 | 21.00 | 24.00 | 17.00 |
| DPPH clearance rate (%) | 80.62 | 64.84 | 58.61 | 44.50 |
| Superoxide anion clearance rate (%) | 78.91 | 56.72 | 60.17 | 40.55 |
Four groups of lavipeditum powder products can remove hydroxyl radical free radical, DPPH free radical, ultra-oxygen anion free radical preferably as shown in Table 4, and test group free radical scavenging effect is best, and minimum with contrast 3 free radical scavenging activity pulverized merely without enzymolysis, thing fermentation, effect is the poorest.It can thus be appreciated that the present invention has good Scavenging ability, can effective delay skin aging, there is good antioxidant effect.
Five, Clinical practice compliance test result
The lavipeditum powder prepared using the present invention as test group, not enzymolysis as a control group 1, azymic as a control group 2, enzymolysis, azymic are not matched group 3, and all matched groups all adopt formula of the present invention, and other technique is identical with present invention process; Use four kinds of product foot bath, with clear water foot bath for blank, detect the result of use of lavipeditum powder of the present invention.
Foot is selected to have blister, skin pruritus, the vitamin B1 deficiency patient that fungal detection is positive is subjects, each 5 people of test group men and women, each 5 people of blank group men and women, adopt each group of sample 20g, selecting same size foot bath, adding 2L water to not having ankle, continuous foot bath 2 weeks, foot bath time every day is 20-30min, off-test detects pedal skin character, and detect fungal content, testing result is as shown in table 5 below.
Table 5 clinical trial testing result
As shown in Table 5, the present invention can treat preferably due to fungus-caused vitamin B1 deficiency, and effectively can improve skin symptom, and life-time service not only has the effect for the treatment of beriberi, has simultaneously and improves skin quality, skincare effect.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention will be further described, but protection scope of the present invention is not limited in this, and all those skilled in the art all fall into protection scope of the present invention with the change of spirit of the present invention to the equivalence that the present invention does.
Embodiment 1
Herba Rosmarini Officinalis lavipeditum powder, comprises Herba Rosmarini Officinalis 10 parts; Flos Pelargonii 3 parts; Herba Pogostemonis 3 parts; Folium Eucommiae 4 parts; Semen Vitis viniferae 1 part; Flos Rosae Rugosae 1 part; Rhizoma Zingiberis Recens powder 2 parts.
Its preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.Concrete operation method is:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity 10 parts, Flos Pelargonii 3 parts, Herba Pogostemonis 3 parts, Folium Eucommiae 4 parts of mix homogeneously, be crushed to 10 orders, spray sterilized water, adjustment moisture to 25%, in mass ratio 0.05% access EM microbial inoculum, constant temperature and humidity fermentation 10h;
(4) sterilizing: by the material microwave sterilizating 10min fermented in step (3), sterilising temp is 100 DEG C, for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, enzyme denaturing after 30 DEG C of enzymolysis 5h, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying, microwave dose 0.027kw/kg, baking temperature 80 DEG C, being dried to moisture is that less than 10% stopping is dry;
(7) composite: the Semen Vitis viniferae of dried material and formula proportion, Flos Rosae Rugosae, Rhizoma Zingiberis Recens powder are mixed homogeneously, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 200 orders.
The present embodiment lavipeditum powder hydrotrope stripping quantity is high, have sterilization go beriberi, circumcise calm the nerves, the function such as improving water flood, health-care and skin-care, product indices meets; Its indices meets the standard of QB/T 1859-2004.
Embodiment 2
Herba Rosmarini Officinalis lavipeditum powder, comprises Herba Rosmarini Officinalis 25 parts; Flos Pelargonii 10 parts; Herba Pogostemonis 8 parts; Folium Eucommiae 9 parts; Semen Vitis viniferae 3 parts; Flos Rosae Rugosae 5 parts; Rhizoma Zingiberis Recens powder 6 parts.
Its preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.Concrete operation method is:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity 25 parts, Flos Pelargonii 10 parts, Herba Pogostemonis 8 parts, Folium Eucommiae 9 parts of mix homogeneously, be crushed to 20 orders, spray sterilized water, adjustment moisture to 35%, in mass ratio 0.15% access EM microbial inoculum, constant temperature and humidity fermentation 20h;
(4) sterilizing: by the material microwave sterilizating 30min fermented in step (3), sterilising temp is 50 DEG C, for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, enzyme denaturing after 30 DEG C of enzymolysis 2h, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying, microwave dose 0.033kw/kg, baking temperature 65 DEG C, being dried to moisture is that less than 10% stopping is dry;
(7) composite: dried material is mixed homogeneously with Semen Vitis viniferae 3 parts, Flos Rosae Rugosae 5 parts, Rhizoma Zingiberis Recens powder 6 parts, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 300 orders.
The present embodiment lavipeditum powder hydrotrope stripping quantity is high, have sterilization go beriberi, circumcise calm the nerves, the function such as improving water flood, health-care and skin-care, product indices meets; Its indices meets the standard of QB/T 1859-2004.
Embodiment 3
Herba Rosmarini Officinalis lavipeditum powder, comprises fan's Herba Rosmarini Officinalis 15 parts; Flos Pelargonii 5 parts; Herba Pogostemonis 5 parts; Folium Eucommiae 5 parts; Semen Vitis viniferae 1 part; Flos Rosae Rugosae 2 parts; Rhizoma Zingiberis Recens powder 3 parts.
Its preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.Concrete operation method is:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity 20 parts; Flos Pelargonii 6 parts; Herba Pogostemonis 6 parts; Folium Eucommiae 7 parts of mix homogeneously, are crushed to 20 orders, spray sterilized water, adjustment moisture to 30%, in mass ratio 0.10% access EM microbial inoculum, constant temperature and humidity fermentation 15h;
(4) sterilizing: by the material microwave sterilizating 15min fermented in step (3), sterilising temp is 60 DEG C, for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, 32 DEG C of enzymolysis 3h, enzyme denaturing, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying, and microwave dose is 0.033kw/kg, and baking temperature is 45 DEG C, and microwave effective time accounts for 70% of the total contribution time, being dried to moisture is that less than 10% stopping is dry;
(7) composite: dried material and Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts of mix homogeneously, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 300 orders.
The present embodiment lavipeditum powder hydrotrope stripping quantity is high, have sterilization go beriberi, circumcise calm the nerves, the function such as improving water flood, health-care and skin-care, product indices meets; Its indices meets the standard of QB/T 1859-2004.
Embodiment 4
Herba Rosmarini Officinalis lavipeditum powder, comprises Herba Rosmarini Officinalis 20 parts; Flos Pelargonii 6 parts; Herba Pogostemonis 6 parts; Folium Eucommiae 7 parts; Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts.
Its preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.Concrete operation method is:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity 20 parts, Flos Pelargonii 6 parts, Herba Pogostemonis 6 parts, Folium Eucommiae 7 parts of mix homogeneously, be crushed to 20 orders, spray sterilized water, adjustment moisture to 25%, in mass ratio 0.15% access EM microbial inoculum, constant temperature and humidity fermentation 10h;
(4) sterilizing: by the material microwave sterilizating 20min fermented in step (3), sterilising temp is 70 DEG C, for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, enzyme denaturing after 30 DEG C of enzymolysis 5h, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts hot air drying to moisture to be that less than 10% stopping is dry;
(7) composite: dried material and Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts of mix homogeneously, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 200 orders.
The present embodiment lavipeditum powder hydrotrope stripping quantity is high, have sterilization go beriberi, circumcise calm the nerves, the function such as improving water flood, health-care and skin-care, product indices meets; Its indices meets the standard of QB/T 1859-2004.
Embodiment 5
Herba Rosmarini Officinalis lavipeditum powder, comprises fan's Herba Rosmarini Officinalis 22 parts; Flos Pelargonii 8 parts; Herba Pogostemonis 7 parts; Folium Eucommiae 8 parts; Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 4 parts; Rhizoma Zingiberis Recens powder 5 parts.
Its preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.Concrete operation method is:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity 20 parts; Flos Pelargonii 6 parts; Herba Pogostemonis 6 parts; Folium Eucommiae 7 parts of mix homogeneously, are crushed to 20 orders, spray sterilized water, adjustment moisture to 30%, in mass ratio 0.10% access EM microbial inoculum, constant temperature and humidity fermentation 15h;
(4) sterilizing: by the material microwave sterilizating 25min fermented in step (3), sterilising temp is 90 DEG C, for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, 32 DEG C of enzymolysis 3h, enzyme denaturing, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying, and microwave dose is 0.027kw/kg, and baking temperature is 55 DEG C, and microwave effective time accounts for 50% of the total contribution time, being dried to moisture is that less than 10% stopping is dry;
(7) composite: dried material and Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts of mix homogeneously, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, namely obtains Herba Rosmarini Officinalis lavipeditum powder after being crushed to 300 orders.
The present embodiment lavipeditum powder hydrotrope stripping quantity is high, have sterilization go beriberi, circumcise calm the nerves, the function such as improving water flood, health-care and skin-care, product indices meets; Its indices meets the standard of QB/T 1859-2004.
Claims (9)
1. a Herba Rosmarini Officinalis lavipeditum powder, is characterized in that, comprises the material composition of following weight portion: Herba Rosmarini Officinalis 10-25 part; Flos Pelargonii 3-10 part; Herba Pogostemonis 3-8 part; Folium Eucommiae 4-9 part; Semen Vitis viniferae 1-3 part; Flos Rosae Rugosae 1-5 part; Rhizoma Zingiberis Recens powder 2-6 part.
2. a kind of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 1, is characterized in that, comprises the material composition of following weight portion: Herba Rosmarini Officinalis 15-22 part; Flos Pelargonii 5-8 part; Herba Pogostemonis 5-7 part; Folium Eucommiae 5-8 part; Semen Vitis viniferae 1-2 part; Flos Rosae Rugosae 2-4 part; Rhizoma Zingiberis Recens powder 3-5 part.
3. a kind of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 1, is characterized in that, comprises the material composition of following weight portion: Herba Rosmarini Officinalis 15 parts; Flos Pelargonii 5 parts; Herba Pogostemonis 5 parts; Folium Eucommiae 5 parts; Semen Vitis viniferae 1 part; Flos Rosae Rugosae 2 parts; Rhizoma Zingiberis Recens powder 3 parts.
4. a kind of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 1, is characterized in that, comprises the material composition of following weight portion: Herba Rosmarini Officinalis 20 parts; Flos Pelargonii 6 parts; Herba Pogostemonis 6 parts; Folium Eucommiae 7 parts; Semen Vitis viniferae 2 parts; Flos Rosae Rugosae 3 parts; Rhizoma Zingiberis Recens powder 4 parts.
5. the preparation method of the Herba Rosmarini Officinalis lavipeditum powder as described in as arbitrary in claim 1-4, is characterized in that, described preparation method comprises remove impurity, air-dry, fermentation, sterilizing, enzymolysis, drying, composite, pulverising step.
6. the preparation method of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 5, it is characterized in that, described step is specific as follows:
(1) remove impurity: the impurity such as raw material removing branch, weeds, leaves, clean water is clean, for subsequent use;
(2) air-dry: by air-dry for needed raw material to water content be less than 10%;
(3) ferment: the Herba Rosmarini Officinalis after remove impurity, Flos Pelargonii, Herba Pogostemonis, Folium Eucommiae press formula proportion mix homogeneously, be crushed to 10-20 order, spray sterilized water, adjustment moisture is to 25%-35%, 0.05%-0.15% accesses EM microbial inoculum in mass ratio, constant temperature and humidity fermentation 10-20h;
(4) sterilizing: by the material sterilizing 10-30min fermented in step (3), for subsequent use;
(5) enzymolysis: regulate pH to neutral by after material complete for sterilizing cooling, add cellulase, neutral protease, 30-35 DEG C of enzymolysis 2-5h, enzyme denaturing, for subsequent use;
(6) dry: the material after being completed by enzymolysis adopts microwave drying or hot air drying, being dried to moisture is that less than 10% stopping is dry;
(7) composite: dried material is mixed homogeneously with Semen Vitis viniferae, Flos Rosae Rugosae, Rhizoma Zingiberis Recens powder, for subsequent use;
(8) pulverize: the material after composite is placed in pulverizer, after being crushed to 200-300 order, namely obtains Herba Rosmarini Officinalis lavipeditum powder.
7. the preparation method of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 6, it is characterized in that, the sterilizing methods described in step (3) is microwave sterilizating, and sterilising temp is 50-100 DEG C.
8. the preparation method of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 6, it is characterized in that, the microwave drying condition described in step (6) is microwave dose 0.027-0.033kw/kg, baking temperature 65-80 DEG C.
9. the preparation method of Herba Rosmarini Officinalis lavipeditum powder as claimed in claim 6, it is characterized in that, microwave drying described in step (6) is intermittent pulse microwave drying, microwave dose is 0.027-0.033kw/kg, baking temperature is 45-55 DEG C, and microwave effective time accounts for the 50%-70% of total contribution time.
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| CN105079097A (en) * | 2015-08-20 | 2015-11-25 | 黔南龙海特种植物开发有限公司 | Rosemary foot-bathing powder and manufacture method thereof |
| CN105233227A (en) * | 2015-11-13 | 2016-01-13 | 韦慧芳 | Bacteriostatic foot bath powder and preparation method thereof |
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| CN105079097A (en) * | 2015-08-20 | 2015-11-25 | 黔南龙海特种植物开发有限公司 | Rosemary foot-bathing powder and manufacture method thereof |
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| CN104436116B (en) | 2017-10-31 |
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