CN104388169A - Preparation method of wire-drawing mould lubricating agent - Google Patents
Preparation method of wire-drawing mould lubricating agent Download PDFInfo
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- CN104388169A CN104388169A CN201410595918.5A CN201410595918A CN104388169A CN 104388169 A CN104388169 A CN 104388169A CN 201410595918 A CN201410595918 A CN 201410595918A CN 104388169 A CN104388169 A CN 104388169A
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Abstract
The invention discloses a preparation method of a wire-drawing mould lubricating agent. The preparation method comprises the following steps of: (a) selecting a material for later use; (b) preparing plant base oil; (c) mixing in sections; (d) carrying out post-processing on the lubricating agent. The invention discloses the preparation method of the wire-drawing mould lubricating agent. The preparation method disclosed by the invention has the advantages of reasonable procedure arrangement and moderate cost and can be simple to implement. The prepared lubricating agent has good cooling function, antirust function and cleaning function, especially has outstanding anti-abrasion property and anti-attrition property and is especially suitable for the drawing production of copper wires and aluminum wires.
Description
Technical field
The present invention relates to a kind of preparation method of wortle lubricant, particularly relate to the preparation method of the wortle lubricant that a kind of wear-resistant, Wear vesistance is given prominence to, belong to technology of die manufacturing field.
Background technology
Wortle is the instrument carrying out metal wire (rod) material extending, and its body is primarily of steel bushing and core rod composition, and steel bushing is selected as stainless steel usually, and core rod can select the materials such as Wimet, steel alloy, natural diamond or artificial diamond.In drawing process implementation process, External Force Acting makes metallic substance be forced through die core of wire-drawing die, and the cross-sectional area of metallic substance is compressed, to obtain required cross-sectional area shape and size.Copper cash, aluminum steel are the prevailing transmission wires of power industry conveying electricity, are usually obtained by drawing process.
When metallic substance is forced through die core of wire-drawing die, larger frictional force, heat and racking stress can be produced, therefore, must make with lubricator, to guarantee to realize cooling, lubrication, cleaning and the object such as antirust.At present, there is the problem that range of product is few, result of use is undesirable and production cost is high in the lubricant for wire drawing on market, and this situation have impact on the development of drawn wire product.
Summary of the invention
For the demand, the invention provides a kind of preparation method of wortle lubricant, this preparation method's procedure arrangement is reasonable, be easy to implement, moderate cost, obtained lubricant is except having good cooling, antirust and cleaning function, and it is wear-resistant, Wear vesistance is particularly outstanding, is particularly suitable for using in the drawing of copper, aluminum steel is produced.
The present invention is a kind of preparation method of wortle lubricant, and this preparation method comprises the steps: that a) selection is got the raw materials ready, and b) prepares plant base oil, c) segmentation batch mixing, d) lubricant aftertreatment.
In a preferred embodiment of the present invention, in described step a), the main component of lubricant is: plant base oil, viscosifying agent, additive and water; Plant base oil is the mixture of sulfurized castor oil and rape oil; The one in Polyanionic Cellulose, Natvosol, methyl hydroxyethylcellulose, Type 3U selected by viscosifying agent; Petroleum sodium sulfonate selected by rust-preventive agent in additive, and extreme-pressure additive selects olefine sulfide or ZDDP, and alkylbenzene sulfonate selected by emulsifying agent, thermally coupled distillation columns selected by tensio-active agent or aliphatic alcohol polyoxyvinethene phosphate.
In a preferred embodiment of the present invention, in described step b), first formulating vulcanization Viscotrol C, then prepares plant base oil; The process for preparation of sulfurized castor oil is as follows: first, pours the Viscotrol C of 100 parts into reactor, and adds 5-6 part vulcanizing agent sulfur dichloride; Then, uniform stirring 2.5-3 hour at the temperature of 35 DEG C-40 DEG C; Then, mixed solution is sent into centrifugal blender, and add the ammonium sulfide solution of 8-10 part and the reduced iron powder of 4-5 part, stir 1-1.5 hour; Finally, get supernatant liquid and filter, obtained sulfurized castor oil; The process for preparation of plant base oil is as follows: first, and sulfurized castor oil and rape oil are quantitatively added into stirrer barrel, and both adding proportions are about: 1%-2.5%:97.5%-99%; Then, control barrel temperature at 40 DEG C-45 DEG C, stirrer rotating speed controls at 900-950r/min, high-speed stirring 3-3.5 hour; Finally, filter, obtained plant base oil.
In a preferred embodiment of the present invention, in described step c), mixed preparing process is as follows: first, and plant base oil, viscosifying agent, emulsifying agent, tensio-active agent and water are added into reactor; Then, control temperature of reaction kettle in 75 DEG C-80 DEG C, fully stir 20-25 minute; Then, add rust-preventive agent, continue to stir 35-40 minute; Finally, add extreme-pressure additive, agitation vat rotating speed controls at 800-850 r/min, stirs 70-75 minute.
Present invention is disclosed a kind of preparation method of wortle lubricant, this preparation method's procedure arrangement is reasonable, be easy to implement, moderate cost, obtained lubricant is except having good cooling, antirust and cleaning function, it is wear-resistant, Wear vesistance is particularly outstanding, is particularly suitable for using in the drawing of copper, aluminum steel is produced.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the present invention is further detailed explanation:
Fig. 1 is the process figure of the preparation method of embodiment of the present invention wortle lubricant.
Embodiment
Below in conjunction with accompanying drawing, preferred embodiment of the present invention is described in detail, can be easier to make advantages and features of the invention be readily appreciated by one skilled in the art, thus more explicit defining is made to protection scope of the present invention.
Fig. 1 is the process figure of the preparation method of embodiment of the present invention wortle lubricant; This preparation method comprises the steps: that a) selection is got the raw materials ready, and b) prepares plant base oil, c) segmentation batch mixing, d) lubricant aftertreatment.
Embodiment 1
The concrete preparation process of the preparation method of the wortle lubricant that the present invention mentions is as follows:
A) selection is got the raw materials ready, and the main component of lubricant and ratio of quality and the number of copies thereof are: plant base oil 22 parts, viscosifying agent 4 parts, additive 8 parts, 950 parts, water; Plant base oil is the mixture of sulfurized castor oil and rape oil; Polyanionic Cellulose selected by viscosifying agent; Petroleum sodium sulfonate selected by rust-preventive agent in additive, and olefine sulfide selected by extreme-pressure additive, and alkylbenzene sulfonate selected by emulsifying agent, thermally coupled distillation columns selected by tensio-active agent;
B) plant base oil is prepared, first formulating vulcanization Viscotrol C, rear preparation plant base oil;
The process for preparation of sulfurized castor oil is as follows: first, pours the Viscotrol C of 100 parts into reactor, and adds 5 parts of vulcanizing agent sulfur dichloride; Then, uniform stirring 3 hours at the temperature of 35 DEG C; Then, mixed solution is sent into centrifugal blender, and add the ammonium sulfide solution of 8 parts and the reduced iron powder of 4 parts, stir 1.5 hours; Finally, get supernatant liquid and filter, obtained sulfurized castor oil;
The process for preparation of plant base oil is as follows: first, and sulfurized castor oil and rape oil are quantitatively added into stirrer barrel, and both adding proportions are about: 2%:98%; Then, control barrel temperature at 40 DEG C, stirrer rotating speed controls at 950r/min, high-speed stirring 3 hours; Finally, obtained plant base oil is filtered;
C) segmentation batch mixing, first, is added into reactor by plant base oil, viscosifying agent, emulsifying agent, tensio-active agent and water; Then, control temperature of reaction kettle in 75 DEG C, fully stir 25 minutes; Then, add rust-preventive agent, continue stirring 35 minutes; Finally, add extreme-pressure additive, agitation vat rotating speed controls at 800 r/min, stirs 75 minutes;
D) lubricant aftertreatment, aftertreatment technology mainly comprise lubricant filtration, filling, packaging and store stack etc.
Embodiment 2
The concrete preparation process of the preparation method of the wortle lubricant that the present invention mentions is as follows:
A) selection is got the raw materials ready, and the main component of lubricant and ratio of quality and the number of copies thereof are: plant base oil 23 parts, viscosifying agent 5 parts, additive 8 parts, 980 parts, water; Plant base oil is the mixture of sulfurized castor oil and rape oil; Methyl hydroxyethylcellulose selected by viscosifying agent; Petroleum sodium sulfonate selected by rust-preventive agent in additive, and ZDDP selected by extreme-pressure additive, and alkylbenzene sulfonate selected by emulsifying agent, aliphatic alcohol polyoxyvinethene phosphate selected by tensio-active agent;
B) plant base oil is prepared, first formulating vulcanization Viscotrol C, rear preparation plant base oil;
The process for preparation of sulfurized castor oil is as follows: first, pours the Viscotrol C of 100 parts into reactor, and adds 6 parts of vulcanizing agent sulfur dichloride; Then, uniform stirring 2.5 hours at the temperature of 40 DEG C; Then, mixed solution is sent into centrifugal blender, and add the ammonium sulfide solution of 9 parts and the reduced iron powder of 5 parts, stir 12 hours; Finally, get supernatant liquid and filter, obtained sulfurized castor oil;
The process for preparation of plant base oil is as follows: first, and sulfurized castor oil and rape oil are quantitatively added into stirrer barrel, and both adding proportions are about: 2.5%:97.5%; Then, control barrel temperature at 45 DEG C, stirrer rotating speed controls at 900r/min, high-speed stirring 3.5 hours; Finally, obtained plant base oil is filtered;
C) segmentation batch mixing, first, is added into reactor by plant base oil, viscosifying agent, emulsifying agent, tensio-active agent and water; Then, control temperature of reaction kettle in 80 DEG C, fully stir 20 minutes; Then, add rust-preventive agent, continue stirring 40 minutes; Finally, add extreme-pressure additive, agitation vat rotating speed controls at 850 r/min, stirs 70 minutes;
D) lubricant aftertreatment, aftertreatment technology mainly comprise lubricant filtration, filling, packaging and store stack etc.
Present invention is disclosed a kind of preparation method of wortle lubricant, be characterized in: this preparation method's procedure arrangement is reasonable, be easy to implement, moderate cost, obtained lubricant is except having good cooling, antirust and cleaning function, it is wear-resistant, Wear vesistance is particularly outstanding, is particularly suitable for using in the drawing of copper, aluminum steel is produced.
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.
Claims (4)
1. a preparation method for wortle lubricant, is characterized in that, this preparation method comprises the steps: that a) selection is got the raw materials ready, and b) prepares plant base oil, c) segmentation batch mixing, d) lubricant aftertreatment.
2. the preparation method of wortle lubricant according to claim 1, is characterized in that, in described step a), the main component of lubricant is: plant base oil, viscosifying agent, additive and water; Plant base oil is the mixture of sulfurized castor oil and rape oil; The one in Polyanionic Cellulose, Natvosol, methyl hydroxyethylcellulose, Type 3U selected by viscosifying agent; Petroleum sodium sulfonate selected by rust-preventive agent in additive, and extreme-pressure additive selects olefine sulfide or ZDDP, and alkylbenzene sulfonate selected by emulsifying agent, thermally coupled distillation columns selected by tensio-active agent or aliphatic alcohol polyoxyvinethene phosphate.
3. the preparation method of wortle lubricant according to claim 1, is characterized in that, in described step b), first formulating vulcanization Viscotrol C, then prepares plant base oil; The process for preparation of sulfurized castor oil is as follows: first, pours the Viscotrol C of 100 parts into reactor, and adds 5-6 part vulcanizing agent sulfur dichloride; Then, uniform stirring 2.5-3 hour at the temperature of 35 DEG C-40 DEG C; Then, mixed solution is sent into centrifugal blender, and add the ammonium sulfide solution of 8-10 part and the reduced iron powder of 4-5 part, stir 1-1.5 hour; Finally, get supernatant liquid and filter, obtained sulfurized castor oil; The process for preparation of plant base oil is as follows: first, and sulfurized castor oil and rape oil are quantitatively added into stirrer barrel, and both adding proportions are about: 1%-2.5%:97.5%-99%; Then, control barrel temperature at 40 DEG C-45 DEG C, stirrer rotating speed controls at 900-950r/min, high-speed stirring 3-3.5 hour; Finally, filter, obtained plant base oil.
4. the preparation method of wortle lubricant according to claim 1, is characterized in that, in described step c), mixed preparing process is as follows: first, and plant base oil, viscosifying agent, emulsifying agent, tensio-active agent and water are added into reactor; Then, control temperature of reaction kettle in 75 DEG C-80 DEG C, fully stir 20-25 minute; Then, add rust-preventive agent, continue to stir 35-40 minute; Finally, add extreme-pressure additive, agitation vat rotating speed controls at 800-850 r/min, stirs 70-75 minute.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410595918.5A CN104388169A (en) | 2014-10-30 | 2014-10-30 | Preparation method of wire-drawing mould lubricating agent |
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| CN201410595918.5A CN104388169A (en) | 2014-10-30 | 2014-10-30 | Preparation method of wire-drawing mould lubricating agent |
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| CN104388169A true CN104388169A (en) | 2015-03-04 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883915A (en) * | 2017-03-22 | 2017-06-23 | 合肥浦尔菲电线科技有限公司 | A kind of wire drawing oil of electric wire copper wire processing and preparation method thereof |
| CN108017202A (en) * | 2017-12-12 | 2018-05-11 | 西北大学 | A kind for the treatment of for reuse technique of copper drawing fluid waste liquid |
| CN108033602A (en) * | 2017-12-12 | 2018-05-15 | 西北大学 | A kind of copper drawing fluid liquid waste treating apparatus |
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| RO79729A2 (en) * | 1980-07-19 | 1982-08-17 | Institutul De Cercetare Si Proiectare Pentru Sistematizarea Locuinte Si Gospodarie Comunala,Ro | PROCESS AND INSTALLATION FOR THE DISTILLATION OF ACVIFIERS AND RECOVERY OF NON-DISPOSABLE PRODUCTS |
| CN101353607A (en) * | 2007-07-26 | 2009-01-28 | 颜克绳 | Manufacturing method of biomass environment-protective lubricant oil |
| CN104164283A (en) * | 2014-08-19 | 2014-11-26 | 清华大学 | Microemulsion metal cutting fluid |
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2014
- 2014-10-30 CN CN201410595918.5A patent/CN104388169A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RO79729A2 (en) * | 1980-07-19 | 1982-08-17 | Institutul De Cercetare Si Proiectare Pentru Sistematizarea Locuinte Si Gospodarie Comunala,Ro | PROCESS AND INSTALLATION FOR THE DISTILLATION OF ACVIFIERS AND RECOVERY OF NON-DISPOSABLE PRODUCTS |
| CN101353607A (en) * | 2007-07-26 | 2009-01-28 | 颜克绳 | Manufacturing method of biomass environment-protective lubricant oil |
| CN104164283A (en) * | 2014-08-19 | 2014-11-26 | 清华大学 | Microemulsion metal cutting fluid |
Non-Patent Citations (2)
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| 方建华等: "硫化润滑油添加剂在菜籽油基础油中的摩擦学性能", 《石油炼制与化工》 * |
| 芮斌等: "新型铜线拉丝润滑剂的研制", 《润滑与密封》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883915A (en) * | 2017-03-22 | 2017-06-23 | 合肥浦尔菲电线科技有限公司 | A kind of wire drawing oil of electric wire copper wire processing and preparation method thereof |
| CN108017202A (en) * | 2017-12-12 | 2018-05-11 | 西北大学 | A kind for the treatment of for reuse technique of copper drawing fluid waste liquid |
| CN108033602A (en) * | 2017-12-12 | 2018-05-15 | 西北大学 | A kind of copper drawing fluid liquid waste treating apparatus |
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